High Resolution Mass Spectrometry Lab
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1 1 st Workshop on Multi-User-Equipment and Facilities High Resolution Mass Spectrometry Lab IQSC-USP-São Carlos Principal Investigator and Presenter: Emanuel Carrilho
2 HRMS LTQ Orbitrap Velos
3 EMU PROC No. 2009/
4 Original Proponents - IQSC/USP Coordenador: Emanuel Carrilho Pesquisadores Associados: André Luiz Meleiro Porto Antonio Carlos Bender Burtoloso Eny Maria Vieira Daniel Rodrigues Cardoso Júlio Cesar Borges Pesquisadores Colaboradores: Agnieszka Joanna Pawlicka Maule Benedito dos Santos Lima Neto Douglas Wagner Franco Janete Harumi Yariwake Marcos Roberto de Vasconcelos Lanza Roberto Gomes de Souza Berlinck Ubirajara Pereira Rodrigues Filho Vitor Marcelo DeMlon
5 Steering Committee Emanuel Carrilho (IQSC) Edson Rodrigues Filho (UFSCar) Daniel Rodrigues Cardoso (IQSC)
6 USER s Committee Antonio Carlos Bender Burtoloso (IQSC) João Batista Fernandes (UFSCar) Quézia Bezerra Cass (UFSCar) Janete Harumi Yariwake (IQSC) Maria de Fátima G. F. da Silva (UFSCar) Regina Vincenzi Oliveira (UFSCar)
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10 High Resolution Mass Spectrometer LTQ Orbitrap Velos Ionization sources: electrospray ionization (ESI) nanoelectrospray (nanoesi) atmospheric pressure chemical ionization (APCI) desorption electrospray ionization (DESI) Separation units: ultra-performance liquid chromatography (UPLC) Accela High Speed LC (Thermo Scientifc) nano-lc EASY-nLc II (Thermo Scientific) Sample Prep Accessories: Akta Prime GE (preparative scale sample prep) Liophilizer Alpha 2-4 LDplus Christ Concentrator model RVC 2-33IR CD Plus Christ.
11 Location & Installations
12 Location & Installations
13 Location & Installations
14 Location & Installations
15 Location & Installations
16 Equipment
17 Supplies
18 UFSCar
19 UFSCar
20 Separations Units
21 Separations Units
22 Ionization Sources
23 Ionization Sources - DESI
24 Ionization Sources - NanoMate CAPES - Pro-Equipamentos
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26 RT#Expenditure# training' so*ware' reagent' infra' consumables' accessory'
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30 Scheduling & Usage!! 5!! 10!! 15!! 20!! 25!! 30!! 35!! Taicia!Pacheco!Fill!/!Edson!Rodrigues!Filho!UFSCar! Emanuel!Carrilho!IQSC/USP! Vitor!Marcel!Faça!FMRP/USP! Undergraduate!Classes!IQSC/USP! Leadro!ArriveG!/!Daniel!Rodrigues!Cardoso!IQSC/USP! Roberto!GS!Berlinck!IQSC/USP! Daniel!Rodrigues!Cardoso!IQSC/USP! Edson!Rodrigues!Filho!UFSCar! Janete!Harumi!Yariwake! Natalia!EC!Almerida!/!Daniel!Rodrigues!Cardoso!IQSC/USP! Carlos!Galinaro!/!Eny!Maria!Vieira!IQSC/USP! Antonio!Carlos!B!Burtoloso! Lívia!S!Medeiros!/!Edison!Rodrigues!Filho!UFSCar! Arlene!Gonçalves!Corrêa!UFSCar! Helio!JA!Franco!/!Emanuel!Carrilho! José!Cesar!Rosa!FMRP/USP! Carlos!Alberto!Montanari!IQSC/USP! Ana!Rita!A!Nogueira!EMBRAPA! Alberto!Grossi!KU! Fernanda!F!Anibal!UFSCar! Marcols!RV!Lanza!IQSC/USP! Beatriz!NM!Miranda!/!Emanuel!Carrilho!IQSC/USP! Nilson!A!Assunção!UNIFESP! Adriano!Aquino!/!Emanuel!Carrilho!IQSC/USP! Juliana!Vieira!Alberice!/!Emanuel!Carrilho!IQSC/USP! Germano!Tremiliosi!Fo.!IQSC/USP! Eny!Maria!Vieira!IQSC/USP! Frank!N.!Crespilho!IQSC/USP! Pedro!Berci!IQSC/USP! Willy!Glen!Santos!/!Daniel!Rodrigues!Cardoso!IQSC/USP! Hong!Tran!/!Roberto!GS!Berlinck!IQSC/USP! André!LM!Porto!IQSC/USP! Tanare!CR!Ferreira!/!Alvaro!J!Santos!Neto! Timothy!J!Brockton!UFSCar! Magali!Monteiro!Silva!FCFAR!UNESP! Andrei!Leitão!IQSC/USP! Kleber!Thiago!de!Oliveira!UFSCar! Barbara!Bernardim!/!Antonio!Carlos!B!Burtoloso!IQSC/USP! Francisco!ER!Gomes!/!Germano!Tremiliosi!Fo.!IQSC/USP! Antonio!Gilberto!Ferreira!UFSCar! Carla!S!Cavalheiro!IQSC/USP! Victor!Deflon!IQSC/USP! Ubirajara!Rodrigues!Pereira!IQSC/USP! 165$$ 61$$ 23$$ 5$$ 5$$ 4$$2$$ iqsc$ ufscar$ fmrp$ embrapa$ exterior$ unifesp$ unesp$
31 Future Charges - After Final Report Direct Infusion - per Sample $ (IQSC & UFSCar) $ (Academic) $ (Industry) NanoLC and UHPLC MS $ 75.00/day (IQSC & UFSCar) $ /day (Academic) $ /sample (Industry)
32 100% Granted EMU 2004: CE-MS (w/ Marina FM Tavares IQ/USP and Adelia R Amaya, UNICAMP) 2004: LC-QToF (Fernando M Lanças and Douglas W Franco, IQSC and Edson Rodrigues Fo, UFSCar) 2009: HRMS LTQ Orbitrap Velos (w/ Edson Rodrigues Fo, UFSCar) 2014/2015: Tribrid Orbitrap Fusion; MALDI/ToF Imaging; SEM-FEG; GCxGC/MS
33 Thanks
SCS Mass Spectrometry Laboratory
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