Certificate of Analysis
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1 5420 Mainway Drive, Unit 5, Burlington ON, L7L 6A4 Phone: , FAX: Certificate of Analysis ALS Project Contact: Steve Kennedy Client Name: ISKY Chemicals Co Ltd ALS Project ID: SKY300 Client Address: Kimhonda Building No. ALS WO#: L Furong oad(m) Date of Sample eceipt 7-Aug-3 Changsha, Hunan 40005, China Date of eport Client Contact: Gary Tang Client Project ID: COMMENTS: Toxic PCDD/F and PCB Congeners by GC/HMS Marker PCB Congeners by GC/MS GC/HMS for PCDD/F and PCB congeners was from an eluant fraction from carbon column clean-up The balance of the PCB congeners were determined via GC/LMS on a separate carbon column eluant fraction eporting units of are equivalent to ng/kg eporting units of ng/g are equivalent to µg/kg Target analyte data are reported on an as-received basis. Certified by: esults in this certificate relate only to the samples as submitted to the laboratory. This report shall not be reproduced, except in full, without the written permission of ALS Canada Ltd. Steve Kennedy Laboratory Manager ALS Canada Ltd L Page of 7
2 ALS Environmental Sample Analysis Summary eport Method Blank ZINC SULPHATE MONOHYDATE BATCH NO.: 4300FA MANGANESE SULPHATE MONOHYDATE BATCH NO.: FEOUS SULPHATE MONOHYDATE BATCH NO.: 4300FA ALS Sample ID WG7232- L L L WG Sample Size Sample units grams grams grams grams Moisture Content 0.00% 0.0%.30% Matrix qc solid solid solid qc -an-3 5-ul-3 5-May-3 Extraction Date LCS Polychlorinated Dibenzo(p)dioxins % ec 2,3,7,8-TCDD < <0.00 < < ,2,3,7,8-PeCDD < <0.00 < < ,2,3,4,7,8-HxCDD < <0.08 < < ,2,3,6,7,8-HxCDD < <0.02 < < ,2,3,7,8,9-HxCDD < <0.02 < < ,2,3,4,6,7,8-HpCDD < < OCDD <0.03 <0.078 <0.036 < Polychlorinated Dibenzofurans 2,3,7,8-TCDF < < < < ,2,3,7,8-PeCDF < <0.08 < < ,3,4,7,8-PeCDF < <0.04 < ,2,3,4,7,8-HxCDF < < ,2,3,6,7,8-HxCDF < < < ,3,4,6,7,8-HxCDF < <0.04 < < ,2,3,7,8,9-HxCDF < <0.07 <0.00 <0.0 97,2,3,4,6,7,8-HpCDF < <0.02 < < ,2,3,4,7,8,9-HpCDF < <0.0 <0.008 < OCDF <0.02 <0.035 <0.02 < Dioxin-like Polychlorinated Biphenyls PCB-8 < < PCB-77 < <0.042 < PCB-23 <0.030 < < PCB-8 < < PCB-4 <0.0 <0.00 < < PCB-05 < < PCB-26 <0.0 < < < PCB-67 <0.00 <0.09 < PCB-56 <0.0 <0.020 <0.06 < PCB-57 <0.0 <0.020 <0.02 < PCB-69 <0.00 <0.08 <0.0 < PCB-89 < < <0.007 < Lower Bound TEQ - PCDD/F Upper Bound TEQ - PCDD/F Lower Bound TEQ - PCB Upper Bound TEQ - PCB Lower Bound TEQ - TOTAL Upper Bound TEQ - TOTAL Marker Polychlorinated Biphenyls ng/g ng/g ng/g ng/g % PCB PCB-52 <0.02 <0.02 <0.02 < PCB-0 <0.02 <0.02 <0.02 < PCB-53 <0.02 <0.02 <0.02 < PCB-38 <0.02 <0.02 <0.02 < PCB-80 <0.02 <0.02 <0.02 < Upper Bound Sum of Marker PCBs ALS Canada Ltd L Page 2 of 7
3 ALS Environmental Laboratory Method Blank Analysis eport Method Blank ALS Sample ID WG7232- Extraction Date Analysis Method Mod. 63B/668A Sample Size grams Analysis Type Blank Percent Moisture Sample Matrix qc Split atio --e-signature-- Filename A S: D 4-Aug-3 2:34 3-Aug-3 6:32 Analysis Units et. Conc. EDL TEF et. Conc. Target Analytes Time Flags WHO (2005) Time. 2,3,7,8-TCDD NotFnd < U,2,3,7,8-PeCDD NotFnd < U,2,3,4,7,8-HxCDD NotFnd < U 0.,2,3,6,7,8-HxCDD NotFnd < U 0.,2,3,7,8,9-HxCDD NotFnd < U 0.,2,3,4,6,7,8-HpCDD 4:0 < OCDD 5:46 < ,3,7,8-TCDF NotFnd < U 0.,2,3,7,8-PeCDF NotFnd < U ,3,4,7,8-PeCDF NotFnd < U 0.3,2,3,4,7,8-HxCDF 2: ,2,3,6,7,8-HxCDF 2:06 < ,3,4,6,7,8-HxCDF NotFnd < U 0.,2,3,7,8,9-HxCDF NotFnd < U 0.,2,3,4,6,7,8-HpCDF NotFnd < U 0.0,2,3,4,7,8,9-HpCDF NotFnd < U 0.0 OCDF 5:52 < PCB-28 5: M PCB-52 NotFnd <2 M U PCB-8 7:30 < M U PCB-77 7:42 < M PCB-23 8:02 < PCB-8 8:08 < PCB-4 NotFnd < U PCB-05 8:38 < PCB-26 NotFnd < U 0. PCB-53 NotFnd <2 M U PCB-38 NotFnd <2 M U PCB-67 NotFnd < U PCB-56 NotFnd < U PCB-57 NotFnd < U PCB-69 NotFnd < U 0.03 PCB-89 :33 < C2-2,3,7,8-TCDD 9: C2-,2,3,7,8-PeCDD 0: C2-,2,3,4,7,8-HxCDD 2: C2-,2,3,6,7,8-HxCDD 2: C2-,2,3,7,8,9-HxCDD 2: C2-,2,3,4,6,7,8-HpCDD 4: C2-OCDD 5: C2-2,3,7,8-TCDF 8: C2-,2,3,7,8-PeCDF 0: C2-2,3,4,7,8-PeCDF 0: C2-,2,3,4,7,8-HxCDF 2: C2-,2,3,6,7,8-HxCDF 2: C2-2,3,4,6,7,8-HxCDF 2: C2-,2,3,7,8,9-HxCDF 2: C2-,2,3,4,6,7,8-HpCDF 3: C2-,2,3,4,7,8,9-HpCDF 4: C2-OCDF 5: C2-PCB-28 m 5: C2-PCB-52 m C2-PCB-8 t 7: C2-PCB-77 t 7: C2-PCB-0 m C2-PCB-23 t 8: C2-PCB-8 t,m 8: C2-PCB-4 t 8: C2-PCB-05 t 8: C2-PCB-26 t 9: C2-PCB-53 m C2-PCB-38 m C2-PCB-67 t 9: C2-PCB-56 t 0: C2-PCB-57 t 0: C2-PCB-69 t 0: C2-PCB-80 m C2-PCB-89 t : Upper Bound Sum of Marker PCBs 05 Lower Bound TEQ - PCDD/F Upper Bound TEQ - PCDD/F Lower Bound TEQ - PCB 0.00 Upper Bound TEQ - PCB Lower Bound TEQ - TOTAL Upper Bound TEQ - TOTAL U Indicates that this compound was not detected above the EDL. indicates that a target analyte was detected below the calibrated range but above the EDL. ALS Canada Ltd L Page 3 of 7
4 ZINC SULPHATE MONOHYDATE BATCH NO.: 4300FA an-3 ALS Sample ID L Extraction Date Analysis Method Mod. 63B/668A Sample Size grams Analysis Type Sample Percent Moisture 0.0% --e-signature-- Sample Matrix solid Split atio Filename A S: D 4-Aug-3 3:54 3-Aug-3 7:27 Analysis Units et. Conc. EDL TEF et. Conc. Target Analytes Time Flags WHO (2005) Time. 2,3,7,8-TCDD NotFnd < U,2,3,7,8-PeCDD NotFnd < U,2,3,4,7,8-HxCDD NotFnd < U 0.,2,3,6,7,8-HxCDD NotFnd < U 0.,2,3,7,8,9-HxCDD NotFnd < U 0.,2,3,4,6,7,8-HpCDD 4: OCDD 5:46 < ,3,7,8-TCDF NotFnd < U 0.,2,3,7,8-PeCDF 0:9 < ,3,4,7,8-PeCDF 0: ,2,3,4,7,8-HxCDF 2: B 0.,2,3,6,7,8-HxCDF 2: ,3,4,6,7,8-HxCDF NotFnd < U 0.,2,3,7,8,9-HxCDF NotFnd < U 0.,2,3,4,6,7,8-HpCDF 3:36 < ,2,3,4,7,8,9-HpCDF 4:28 < OCDF 5:52 < PCB-28 5: B PCB-52 NotFnd <2 M U PCB-8 7: M PCB-77 7: PCB-23 8:02 < PCB-8 8: PCB-4 NotFnd < U PCB-05 8: PCB-26 NotFnd < U 0. PCB-53 NotFnd <2 M U PCB-38 NotFnd <2 M U PCB-67 NotFnd < U PCB-56 NotFnd < U PCB-57 NotFnd < U PCB-69 NotFnd < U 0.03 PCB-89 NotFnd < U C2-2,3,7,8-TCDD 9: C2-,2,3,7,8-PeCDD 0: C2-,2,3,4,7,8-HxCDD 2: C2-,2,3,6,7,8-HxCDD 2: C2-,2,3,7,8,9-HxCDD 2: C2-,2,3,4,6,7,8-HpCDD 4: C2-OCDD 5: C2-2,3,7,8-TCDF 8: C2-,2,3,7,8-PeCDF 0: C2-2,3,4,7,8-PeCDF 0: C2-,2,3,4,7,8-HxCDF 2: C2-,2,3,6,7,8-HxCDF 2: C2-2,3,4,6,7,8-HxCDF 2: C2-,2,3,7,8,9-HxCDF 2: C2-,2,3,4,6,7,8-HpCDF 3: C2-,2,3,4,7,8,9-HpCDF 4: C2-OCDF 5: ALS Environmental Sample Analysis eport 3C2-PCB-28 m 5: C2-PCB-52 m C2-PCB-8 t 7: C2-PCB-77 t 7: C2-PCB-0 m C2-PCB-23 t 8: C2-PCB-8 t,m 8: C2-PCB-4 t 8: C2-PCB-05 t 8: C2-PCB-26 t 9: C2-PCB-53 m C2-PCB-38 m C2-PCB-67 t 9: C2-PCB-56 t 0: C2-PCB-57 t 0: C2-PCB-69 t 0: C2-PCB-80 m C2-PCB-89 t : Upper Bound Sum of Marker PCBs 08 Lower Bound TEQ - PCDD/F 0.07 Upper Bound TEQ - PCDD/F Lower Bound TEQ - PCB Upper Bound TEQ - PCB Lower Bound TEQ - TOTAL 0.07 Upper Bound TEQ - TOTAL U Indicates that this compound was not detected above the EDL. B indicates that a target analyte was detected below the calibrated range but above the EDL. Indicates that this compound was detected in the method blank at greater than 0% of the sample concentration. ALS Canada Ltd L Page 4 of 7
5 MANGANESE SULPHATE MONOHYDATE BATCH NO.: ul-3 ALS Sample ID L Extraction Date Analysis Method Mod. 63B/668A Sample Size grams Analysis Type Sample Percent Moisture 0.% --e-signature-- Sample Matrix solid Split atio Filename A S: D 4-Aug-3 4:4 3-Aug-3 7:46 Analysis Units et. Conc. EDL TEF et. Conc. Target Analytes Time Flags WHO (2005) Time. 2,3,7,8-TCDD NotFnd < U,2,3,7,8-PeCDD NotFnd < U,2,3,4,7,8-HxCDD NotFnd < U 0.,2,3,6,7,8-HxCDD NotFnd < U 0.,2,3,7,8,9-HxCDD NotFnd < U 0.,2,3,4,6,7,8-HpCDD 4: OCDD 5:46 < ,3,7,8-TCDF NotFnd < U 0.,2,3,7,8-PeCDF NotFnd < U ,3,4,7,8-PeCDF 0:4 < M 0.3,2,3,4,7,8-HxCDF NotFnd < U 0.,2,3,6,7,8-HxCDF NotFnd < U 0. 2,3,4,6,7,8-HxCDF NotFnd < U 0.,2,3,7,8,9-HxCDF NotFnd < U 0.,2,3,4,6,7,8-HpCDF NotFnd < U 0.0,2,3,4,7,8,9-HpCDF 4:27 < OCDF NotFnd < U PCB-28 5: B PCB-52 NotFnd <2 M U PCB-8 NotFnd < U PCB-77 7:42 < M PCB-23 8: PCB-8 8: PCB-4 NotFnd < U PCB-05 8: PCB-26 NotFnd < U 0. PCB-53 NotFnd <2 M U PCB-38 NotFnd <2 M U PCB-67 NotFnd < U PCB-56 0:03 < PCB-57 NotFnd < U PCB-69 NotFnd < U 0.03 PCB-89 NotFnd < U C2-2,3,7,8-TCDD 9: C2-,2,3,7,8-PeCDD 0: C2-,2,3,4,7,8-HxCDD 2: C2-,2,3,6,7,8-HxCDD 2: C2-,2,3,7,8,9-HxCDD 2: C2-,2,3,4,6,7,8-HpCDD 4: C2-OCDD 5: C2-2,3,7,8-TCDF 8: C2-,2,3,7,8-PeCDF 0: C2-2,3,4,7,8-PeCDF 0: C2-,2,3,4,7,8-HxCDF 2: C2-,2,3,6,7,8-HxCDF 2: C2-2,3,4,6,7,8-HxCDF 2: C2-,2,3,7,8,9-HxCDF 2: C2-,2,3,4,6,7,8-HpCDF 3: C2-,2,3,4,7,8,9-HpCDF 4: C2-OCDF 5: ALS Environmental Sample Analysis eport 3C2-PCB-28 m 5: C2-PCB-52 m C2-PCB-8 t 7: C2-PCB-77 t 7: C2-PCB-0 m C2-PCB-23 t 8: C2-PCB-8 t,m 8: C2-PCB-4 t 8: C2-PCB-05 t 8: C2-PCB-26 t 9: C2-PCB-53 m C2-PCB-38 m C2-PCB-67 t 9: C2-PCB-56 t 0: C2-PCB-57 t 0: C2-PCB-69 t 0: C2-PCB-80 m C2-PCB-89 t : Upper Bound Sum of Marker PCBs 06 Lower Bound TEQ - PCDD/F Upper Bound TEQ - PCDD/F Lower Bound TEQ - PCB Upper Bound TEQ - PCB Lower Bound TEQ - TOTAL Upper Bound TEQ - TOTAL U Indicates that this compound was not detected above the EDL. B indicates that a target analyte was detected below the calibrated range but above the EDL. Indicates that this compound was detected in the method blank at greater than 0% of the sample concentration. ALS Canada Ltd L Page 5 of 7
6 FEOUS SULPHATE MONOHYDATE BATCH NO.: 4300FA May-3 ALS Sample ID L Extraction Date Analysis Method Mod. 63B/668A Sample Size grams Analysis Type Sample Percent Moisture.3% --e-signature-- Sample Matrix solid Split atio Filename A S: D 4-Aug-3 4:34 3-Aug-3 8:04 Analysis Units et. Conc. EDL TEF et. Conc. Target Analytes Time Flags WHO (2005) Time. 2,3,7,8-TCDD NotFnd < U,2,3,7,8-PeCDD NotFnd < U,2,3,4,7,8-HxCDD NotFnd < U 0.,2,3,6,7,8-HxCDD NotFnd < U 0.,2,3,7,8,9-HxCDD NotFnd < U 0.,2,3,4,6,7,8-HpCDD 4: < M 0.0 OCDD 5:46 < ,3,7,8-TCDF NotFnd < U 0.,2,3,7,8-PeCDF NotFnd < U ,3,4,7,8-PeCDF NotFnd < U 0.3,2,3,4,7,8-HxCDF NotFnd < U 0.,2,3,6,7,8-HxCDF NotFnd < U 0. 2,3,4,6,7,8-HxCDF NotFnd < U 0.,2,3,7,8,9-HxCDF 2:48 < ,2,3,4,6,7,8-HpCDF NotFnd < U 0.0,2,3,4,7,8,9-HpCDF NotFnd < U 0.0 OCDF 5:53 < U PCB-28 5: B PCB-52 NotFnd <2 U PCB-8 7: PCB-77 7:42 < PCB-23 8:03 < PCB-8 8:08 < PCB-4 8:20 < PCB-05 8:36 < PCB-26 9:5 < PCB-53 NotFnd <2 M U PCB-38 NotFnd <2 M U PCB-67 9: PCB-56 0:02 < PCB-57 0:08 < PCB-69 NotFnd < U 0.03 PCB-89 NotFnd < U C2-2,3,7,8-TCDD 9: C2-,2,3,7,8-PeCDD 0: C2-,2,3,4,7,8-HxCDD 2: C2-,2,3,6,7,8-HxCDD 2: C2-,2,3,7,8,9-HxCDD 2: C2-,2,3,4,6,7,8-HpCDD 4: C2-OCDD 5: C2-2,3,7,8-TCDF 8: C2-,2,3,7,8-PeCDF 0: C2-2,3,4,7,8-PeCDF 0: C2-,2,3,4,7,8-HxCDF 2: C2-,2,3,6,7,8-HxCDF 2: C2-2,3,4,6,7,8-HxCDF 2: C2-,2,3,7,8,9-HxCDF 2: C2-,2,3,4,6,7,8-HpCDF 3: C2-,2,3,4,7,8,9-HpCDF 4: C2-OCDF 5: ALS Environmental Sample Analysis eport 3C2-PCB-28 m 5: C2-PCB-52 m M 3C2-PCB-8 t 7: C2-PCB-77 t 7: C2-PCB-0 m C2-PCB-23 t 8: C2-PCB-8 t,m 8: C2-PCB-4 t 8: C2-PCB-05 t 8: C2-PCB-26 t 9: C2-PCB-53 m C2-PCB-38 m M 3C2-PCB-67 t 9: C2-PCB-56 t 0: C2-PCB-57 t 0: C2-PCB-69 t 0: C2-PCB-80 m C2-PCB-89 t : Upper Bound Sum of Marker PCBs 09 Lower Bound TEQ - PCDD/F 0.00 Upper Bound TEQ - PCDD/F Lower Bound TEQ - PCB Upper Bound TEQ - PCB Lower Bound TEQ - TOTAL Upper Bound TEQ - TOTAL U Indicates that this compound was not detected above the EDL B indicates that a target analyte was detected below the calibrated range but above the EDL Indicates that this compound was detected in the method blank at greater than 0% of the sample concentration. ALS Canada Ltd L Page 6 of 7
7 ALS Environmental Laboratory Control Sample Analysis eport LCS ALS Sample ID WG Extraction Date Analysis Method Mod. 63B/668A Sample Size Analysis Type LCS Percent Moisture --e-signature-- Sample Matrix qc Split atio Filename A S: D 4-Aug-3 :34 3-Aug-3 5:56 Analysis Units % % et. et. Target Analytes Time % ec Flags Limits Time. % ec 2,3,7,8-TCDD 9: ,2,3,7,8-PeCDD 0: ,2,3,4,7,8-HxCDD 2: ,2,3,6,7,8-HxCDD 2: ,2,3,7,8,9-HxCDD 2: ,2,3,4,6,7,8-HpCDD 4: OCDD 5: ,3,7,8-TCDF 8: ,2,3,7,8-PeCDF 0: ,3,4,7,8-PeCDF 0: ,2,3,4,7,8-HxCDF 2: ,2,3,6,7,8-HxCDF 2: ,3,4,6,7,8-HxCDF 2: ,2,3,7,8,9-HxCDF 2: ,2,3,4,6,7,8-HpCDF 3: ,2,3,4,7,8,9-HpCDF 4: OCDF 5: PCB-28 5: PCB M PCB-8 7: PCB-77 7: PCB PCB-23 8: PCB-8 8: PCB-4 8: PCB-05 8: PCB-26 9: PCB M PCB PCB-67 9: PCB-56 0: PCB-57 0: PCB-69 0: PCB PCB-89 : C2-2,3,7,8-TCDD 9: C2-,2,3,7,8-PeCDD 0: C2-,2,3,4,7,8-HxCDD 2:28 62 M C2-,2,3,6,7,8-HxCDD 2:3 58 M C2-,2,3,7,8,9-HxCDD 2: C2-,2,3,4,6,7,8-HpCDD 4: C2-OCDD 5: C2-2,3,7,8-TCDF 8: C2-,2,3,7,8-PeCDF 0: C2-2,3,4,7,8-PeCDF 0: C2-,2,3,4,7,8-HxCDF 2: C2-,2,3,6,7,8-HxCDF 2: C2-2,3,4,6,7,8-HxCDF 2: C2-,2,3,7,8,9-HxCDF 2: C2-,2,3,4,6,7,8-HpCDF 3: C2-,2,3,4,7,8,9-HpCDF 4: C2-OCDF 5: C2-PCB-28 m 5: C2-PCB-52 m C2-PCB-8 t 7: C2-PCB-77 t 7: C2-PCB-0 m C2-PCB-23 t 8: C2-PCB-8 t,m 8: C2-PCB-4 t 8: C2-PCB-05 t 8: C2-PCB-26 t 9: C2-PCB-53 m C2-PCB-38 m C2-PCB-67 t 9: C2-PCB-56 t 0: C2-PCB-57 t 0: C2-PCB-69 t 0: C2-PCB-80 m C2-PCB-89 t : ALS Canada Ltd L Page 7 of 7
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