Discipline Chemical Testing Issue Date Certificate Number T-1435 Valid Until Last Amended on - Page 1 of 18
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1 Last Amended on - Page 1 of 18 I. DRUGS & PHARMACEUTICALS A. Natural Drugs (Medicinal Plant Preparations) 1. Asava and Arista AFI (Abhayarishta, Amritarishta, okarishta, Asvagandharishta, Kanakasava, Kutajarishta, Kumaryasava, Khadirarishta, Chandanasava, Dasamularishta, Draksharishta, Jirakarishta, Balarishta, Punarnavasava, Lohasava) ph IP. Vol. I, 2014; p. 169 (WI/SOP/:CSMDRIA/CL/001) Specific gravity IP. Vol. I, 2014; p. 208 (WI/SOP/:CSMDRIA/CL/002) Total solids IP. Vol. I, 2014; p. 277 (WI/SOP/:CSMDRIA/CL/003) Alcohol content IP. Vol. I, 2014; p. 116 (WI/SOP/:CSMDRIA/CL/004) Reducing sugar AOAC International, 2005, Ch. 44, p.9 and table Appendix C P.37. (WI/SOP/:CSMDRIA/CL/005) Total sugar AOAC International, 2005, Ch. 44,p.9 and table Appendix C P.37. (WI/SOP/:CSMDRIA/CL/005) 2.5 to to to 45 % 1.5 to 12 % 2.0 to 56.0 % 2.0 to 62.0 % Test for methanol Laboratory manual of Organic Chemistry, 1957, p.54. (WI/SOP/:CSMDRIA/CL/006)
2 Last Amended on - Page 2 of 18 Asava and Arista AFI Photo documentation of Single drug/ formulations by TLC Plant drug Analysis, 1996, p.364. (WI/SOP/:CSMDRIA/CL/007) Finger print of Single drug/ formulations by HPTLC HPTLC Quantitative analysis of Pharmaceutical formulations, 1996, p (WI/SOP/:CSMDRIA/CL/008) 2. Arka (AFI ) (Ajamodarka, Karpuradyarka, Satapushparka) Dravaka (AFI ) Sankhadravaka ph IP. Vol. I, 2014; p. 169 (WI/SOP/:CSMDRIA/CL/001) Specific gravity IP. Vol. I, 2014; p. 208 (WI/SOP/:CSMDRIA/CL/002) 2.5 to to 1.55 Tinir, (SFI) (Comput Tinir, Omat Tinir) Tiravakam (SFI) Cankatiravakam Volatile matter /Oil 4. Photo documentation of Single drug/ formulations by TLC Medicinal Plant Materials, WHO, 1998, p (WI/SOP/:CSMDRIA/CL/009) Plant drug Analysis, 1996, p.364. (WI/SOP/:CSMDRIA/CL/007) 0.2 to 5 % 5. Finger print of Single drug/ formulations by HPTLC HPTLC Quantitative analysis of Pharmaceutical formulations, 1996, p (WI/SOP/: CSMDRIA/CL/008)
3 Last Amended on - Page 3 of Avaleha, Rasayana, Paka (AFI) (Agastyaharitaki, rasayana, wagandhadi lehya, Cyavanaprasa, Kusmandaka rasayana, Kutajavaleha, Dasamulaharitaki lehya, Draksavaleha, Bilvadileha, Brahma rasayana, Vasavaleha) Modaka (AFI) Eladya modaka Loss on drying at 105 C Fat content (WI/SOP/: CSMDRIA/CL/010) AOAC International, 2005, ch , p.10. (WI/SOP/: CSMDRIA/CL/013) 0.5 to 15% 0.2 to 2.0 % 0.2 to 20 % 0.5 to 20 % Iracayanam (SFI) (Parankip pattai, Iracayanam, Tippili Iracayanam) Ilakam, (SFI) (Maka Vallati Ilakam, Nellikkai Ilakam, Vilvati Ilakam) ph IP. Vol. I, 2010; p (WI/SOP/:CSMDRIA/CL/001) Reducing sugar AOAC International, 2005, Ch. 44,p.9 and table Appendix C p.37. (WI/SOP/:CSMDRIA/CL/005) 2.5 to to 65 %
4 Last Amended on - Page 4 of 18 Manappaku (SFI) (Atatotai, Manappaku, Matulai, Manappaku) Total sugar AOAC International, 2005, Ch. 44, p.9 and table Appendix C p.37. (WI/SOP/:CSMDRIA/CL/005) 5 to 75 % Meluku (SFI) (Iraca kanti Meluku, Iti Vallati Nava Uppu Meluku) Water-soluble extractive Alcohol-soluble Extractive (WI/SOP/:CSMDRIA/CL/014) (WI/SOP/:CSMDRIA/CL/015) 10 to 75 % 5 to 50 % Photo documentation of Single drug/ formulations by TLC Plant drug Analysis, 1996, p.364. (WI/SOP/:CSMDRIA/CL/007) Finger print of Single drug/ formulations by HPTLC HPTLC Quantitative analysis of Pharmaceutical formulations, 1996, p (WI/SOP/: CSMDRIA/CL/008)
5 Last Amended on - Page 5 of Bhasma, (AFI) (Kasisabhasma, Pravalabhasma, Mukthabhasma, Yasadabhasma, Lauhabhasma, Sankhabhasma) Kupipakva Rasayana, (AFI) (Makaradhvaja, Rasasinndura, Samirapanna- Garasa) Pisti, (AFI) (Pravalapisti, Muktapisti) Parpati (AFI) (Pancarmrita parpati) Patankam(SFI) Parpam (SFI) (Canku Parpam, Cempu Parpam, Kunkiliya Parpam) Centuram (SFI) (Tamra Centuram) Loss on drying at 105 C Assay for Calcium (Titrimetric method) Assay for Copper (Titrimetric Method) (WI/SOP/: CSMDRIA/CL/010) Analytical uses of Ethylenediamine tetra acetic acid, 1965, p (WI/SOP/: CSMDRIA/CL/016) A Text Book of Quantitative Inorganic analysis, 1961, p.348 and 358. (WI/SOP/: CSMDRIA/CL/017) 1 to 99 % 0.2 to 80 % 0.2 to 2 % 10 to 45 % 5 to 65 %
6 Last Amended on - Page 6 of 18 Karuppu (SFI) (Civanar Amirtam, Pancha lavana, Karuppu, Gandhaka, Karuppu) Assay for Iron (Titrimetric method) A Text Book of Quantitative Inorganic analysis, 1961, p (WI/SOP/: CSMDRIA/CL/018) 5 to 50 % 5. Curna (AFI) (Eladicurna, Avipattikaracurna, Talisadyacurna, Trikatucurna, Triphalacurna, Nimbadicurna, Nyagrodhadicurna, Pushyanugacurna, Balacaturbhadrika Curna, Sitotaladicurna) Kvatha Curna (AFI) (Amritottara kvatha curna, Dasamulakatutraya kvatha curna, Trayantyadi kvatha curna) Curanam, (SFI) (Tirikatukacurana m, Tiriphalacuranam, Eladicuranam) Fineness of particle IP. Vol. I, 2014; p (WI/SOP/:CSMDRIA/CL/021) Water-soluble Extractive Alcohol-soluble Extractive WHO, 1998, Pp.28. (WI/SOP/:CSMDRIA/CL/010) (WI/SOP/:CSMDRIA/CL/014) (WI/SOP/:CSMDRIA/CL/015) 0.2 to 70 % 0.2 to 50 % 3 to 75 % 3 to 45%
7 Last Amended on - Page 7 of 18 Kutinir (SFI) (Nilavembu Kutinir) Loss on drying at 105 C 1 to 12 % 6. Taila (AFI) (Balataila Narayanataila MahaVisagarbha Taila, Laksaditaila Balaashwagandha laksaditaila Pindataila) Ghrita (AFI) (Jatyadighrita, Triphalaghrita, Dadimadighrita, 4Indukantaghrita) Ney (SFI) (Biraminey, Vallarainey) Tailam (Noccit tailam, Pindatailam, Civanarvembukulit ailam, VellaiEennai) Loss on drying at 105 C Refractive index IP. Vol. I, 2014; p (WI/SOP/:CSMDRIA/CL/022) Acid value IP. Vol. I, 2014; p WI/SOP/: CSMDRIA/CL/023 Saponification value IP. Vol. I, 2014; p.109. (WI/SOP/:CSMDRIA/CL/024) Iodine value IP. Vol. I, 2014; p Method A (WI/SOP/:CSMDRIA/CL/025) Fat content AOAC International, 2005, ch , p.10. (WI/SOP/:CSMDRIA/CL/013) 0.2 to 10 % 1.33 to to to to to 25 %
8 Last Amended on - Page 8 of 18 Taila (AFI) (Balataila Narayanataila MahaVisagarbha Taila, Laksaditaila Balaashwagandha laksaditaila Pindataila) Ghrita (AFI) (Jatyadighrita, Triphalaghrita, Dadimadighrita, 4Indukantaghrita) Ney (SFI) (Biraminey, Vallarainey) Peroxide value Rancidity. Photo documentation of Single drug/ formulations by TLC Finger print of Single drug/ formulations by HPTLC IP. Vol. I, 2014; p.109. (WI/SOP/:CSMDRIA/CL/026) The Chemical Analysis of Foods, 1962, p411. (WI/SOP/:CSMDRIA/CL/027) Plant drug Analysis, 1996, p.364. (WI/SOP/:CSMDRIA/CL/007) HPTLC Quantitative analysis of Pharmaceutical formulations, 1996, p (WI/SOP/: CSMDRIA/CL/008) 0.2 to 30 Tailam (Noccit tailam, Pindatailam, Civanarvembukulit ailam, VellaiEennai) 7. Guggulu (AFl ) (Triphalaguggulu, Kancanaraguggulu Yagarajaguggulu, Goksuradiguggulu, Laksaguggulu) (WI/SOP/:CSMDRIA/CL/010.) 0.2 to 50 %
9 Last Amended on - Page 9 of 18 Guggulu (AFl ) (Triphalaguggulu, Kancanaraguggulu Yagarajaguggulu, Goksuradiguggulu, Laksaguggulu) Water-soluble extractive (WI/SOP/:CSMDRIA/CL/014) 0.2 to 36 % 15 to 50 % Alcohol-soluble extractive (WI/SOP/:CSMDRIA/CL/015) 8 to 35 % Loss on drying at 105 C 8 to 24 % Resin content AOAC International, 2005, ch. 43, p.5. (WI/SOP/: CSMDRIA/CL/028) 3 to 15 % Photo documentation of Single drug/ formulations by TLC Plant drug Analysis, 1996, p.364. (WI/SOP/:CSMDRIA/CL/007)
10 Last Amended on - Page 10 of 18 Guggulu (AFl ) (Triphalaguggulu, Kancanaraguggulu Yagarajaguggulu, Goksuradiguggulu, Laksaguggulu) Finger print of Single drug/ formulations by HPTLC HPTLC Quantitative analysis of Pharmaceutical formulations, 1996, p (WI/SOP/: CSMDRIA/CL/008) 8. Ksara (AFI) (Apamargaksara, Palasaksara, Yavaksara) Lavana (AFI) (Arka lavana, Narikela lavana) ph IP. Vol. I, 2014; p (WI/SOP/:CSMDRIA/CL/001) Assay for Sodium (Flame Photometric Method) AOAC International, 2005, Ch. 3, p.10. (WI/SOP/:CSMDRIA/CL/020 ) 2.5 to to 100 ppm 0.1 to 40 % Assay for Potassium (Flame Photometric Method) AOAC International, 2005, Ch. 3, p.10. (WI/SOP/:CSMDRIA/CL/019 ) 1 to 100 ppm 0.1 to 40 % 9. Lauha (AFI) (Dhatrilauha, Saptamritalauha) Mandura (AFI) (Punarnavadi mandura) Karpam (SFI) (Pavanakatukai) Loss on drying at 105 C (WI/SOP/:CSMDRIA/CL/010) 1 to 5 % 1 to 70 %
11 Last Amended on - Page 11 of 18 Cunnam (SFI) (Vetiyuppue cunnum) 0.2 to 25 % Assay for Iron (Titrimetric Method) A Text Book of Quantitative Inorganic analysis, 1961, p (WI/SOP/:CSMDRIA/CL/018) 5 to 55 % 5. Photo documentation of Single drug/ formulations by TLC Plant drug Analysis, 1996, p.364. (WI/SOP/:CSMDRIA/CL/007) 6. Finger print of Single drug/ formulations by HPTLC HPTLC Quantitative analysis of Pharmaceutical formulations, 1996, p (WI/SOP/: CSMDRIA/CL/008) 10. Lepa (AFI) (Dasangalepa, Sothaghnalepa, Grihadhumadi lepa, Avalgujadilepa, Sinduradilepa) ph IP. Vol. I, 2014; p (WI/SOP/:CSMDRIA/CL/001) WHO, 1998p.28. (WI/SOP/: CSMDRIA/CL/010) 2.5 to to 25 %
12 Last Amended on - Page 12 of 18 Venney (Amirta venney, Kunkiliya venney) Kulampu, Pura maruntukal (SFI) (Akasthiyar, kulampu Ilanir kulambu) Loss on drying at C 0.2 to 10 % 2 to 10 % Photo documentation of Single drug/ formulations by TLC (WI/SOP/:CSMDRIA/CL/007) Finger print of Single drug/ formulations by HPTLC (WI/SOP/: CSMDRIA/CL/008) 11. Rasa yoga (AFI) (Anandabhairava rasa, Karpurarasa asantakusumakar Arasa, Brihatgarbhacinta manirasa, Sutasekhararasa) (WI/SOP/: CSMDRIA/CL/010) 3 to 99 % 0.2 to 45 % Loss on drying at C 1 to 10 %
13 Last Amended on - Page 13 of 18 Rasa yoga (AFI) (Anandabhairava rasa, Karpurarasa asantakusumakar Arasa, Brihatgarbhacinta manirasa, Sutasekhararasa) Water-soluble extractive Alcohol-soluble extractive (WI/SOP/:CSMDRIA/CL/014) (WI/SOP/:CSMDRIA/CL/015) 5 to 80 % 1 to 45 % 12. Sattva (AFI) (Guduci sattva) (WI/SOP/:CSMDRIA/CL/010) 0.2 to 10 % (WI/SOP/:CSMDRIA/CL/011) 0.2 to 10 % Loss on drying at C (WI/SOP/:CSMDRIA/CL/012) 1 to 10 % Water-soluble extractive (WI/SOP/:CSMDRIA/CL/014) 5 to 65 %
14 Last Amended on - Page 14 of Vartti, Anjana, Netra Bindu (AFI) (Candrodayavartti Elanir Kuzhambu) (WI/SOP/: CSMDRIA/CL/010) 0.5 to 55 % 0.2 to 6 % ph IP. Vol. I, 2014; p (WI/SOP/:CSMDRIA/CL/001) 5.0 to 10.0 Photo documentation of Single drug/ formulations by TLC Plant drug Analysis, 1996, p.364. (WI/SOP/:CSMDRIA/CL/007) Finger print of Single drug/ formulations by HPTLC HPTLC Quantitative analysis of Pharmaceutical formulations, 1996, p (WI/SOP/:CSMDRIA/CL/008) 14. Vati and Gutika (AFI) (Eladigutika SanjivanivatiCitra kadigutika Chandraprabhavati Gandhakavati) Loss on drying at 105 C 1 to 15 %
15 Last Amended on - Page 15 of 18 Mattirai, (SFI) (Ilavankati mattirai Kasturi mattirai) Vatakam (SFI) (Inci vatakam, Pirandai vatakam, Talicati vatakam) (WI/SOP/: CSMDRIA/CL/010) 0.2 to 80 % 0.2 to 20 % Disintegration test IP. Vol. I, 2014, p.251. (WI/SOP/: CSMDRIA/CL/029) Uniformity of weight IP. Vol. I, 2014, p.256. (WI/SOP/: CSMDRIA/CL/030) 15. Plant Materials (Root/Stolen Root bark Rhizome Root tuber /corm Stem Stem bark Leaf Flower/Flower bud/stamen Fruit/pericarp/pulp Seed) (WI/SOP/: CSMDRIA/CL/010) 0.1 to 15 % 0.2 to 5 %
16 Last Amended on - Page 16 of 18 Exudate/Gum Whole plant Aerial parts Heart wood Water-soluble extractive (WI/SOP/:CSMDRIA/CL/014) 1 to 75 % Alcohol-soluble extractive (WI/SOP/:CSMDRIA/CL/015) 1 to 50 % Loss on drying at 105 C WHO, 1998,p to 12 % Photo documentation of Single plant material/ formulations by TLC Plant drug Analysis, 1996, p.364. (WI/SOP/:CSMDRIA/CL/007) Finger print of Single plant materials / formulations by HPTLC HPTLC Quantitative analysis of Pharmaceutical formulations, 1996, p (WI/SOP/:CSMDRIA/CL/008)
17 Last Amended on - Page 17 of Metal/ Mineral drugs IRON (Aya Centuram Arumuka Centuram Aya Centuram Aya Kantac Centuram Anna Peti Centuram) COPPER (Cempu Parpam (Tamira Parpam) Tamirac Centuram Cempuc Centuram Mayilaragathi chooranam) CALCIUM (Pavala Parpam Palagarai Parpam Muttu Cippi Parpam) POTASSIUM (Vediuppu chunnam) SODIUM (Astavargachooranam Kunmakudrimezhugu) Loss on drying at C Assay for Calcium (Titrimetric Method) Assay for Copper (Titrimetric Method) Assay for Iron (Titrimetric Method) Assay for Potassium (Flame Photometric Method) Assay for Sodium (Flame Photometric Method) (WI/SOP/: CSMDRIA/CL/010) (WI/SOP/:CSMDRIA/CL/016). (WI/SOPCSMDRIA/CL/017). (WI/SOP/:CSMDRIA/CL/018). (WI/SOP/:CSMDRIA/CL/019 ) (WI/SOP/:CSMDRIA/CL/020) 1 to 99 % 0.2 to 60 % 0.2 to 10 % 5 to 60 % 5 to 65 % 5 to 60 % 1 to 100 ppm 0.1 to 40 % 1 to 100 ppm 0.1 to 40 %
18 Last Amended on - Page 18 of Herbal and Herbomineral Drugs Cadmium WHO, 1998, p (WI/SOP/:CSMDRIA/CL/031) 0.1 to 20 ppm Lead WHO, 1998, p (WI/SOP/:CSMDRIA/CL/031) 0.1 to 20 ppm -X-X-X-X-X-X-X-X-X-X-X-X-X-X-
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