GRUPO ANALIZA CALIDAD. International Workshop UBU 2013 Silvia Raliegos Martín

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1 GRUPO ANALIZA CALIDAD International Workshop UBU 2013 Silvia Raliegos Martín

2 GRUPO ANALIZA CALIDAD Group of companies that aims to provide comprehensive support to companies in different sectors such as: Agriculture Animal feed Human food Environmental Industrial

3 Our companies 1. ANALIZA CONTROL DE CALIDAD S.L. (BURGOS) 2. ANALIZA CALIDAD MADRID S.L. 3. ANALIZA CALIDAD BARCELONA S.L. 4. ANALIZA CALIDAD VALLADOLID S.L. 5. SANILAB CALIDAD S.L. (ZAMORA) 6. HIDROMANTE S.L. (CACERES) 7. AUDITAR ALIMENTARIA S.L. (MADRID) 8. GARANTIZA/FORMEAM (VALLADOLID) 9. AKLABS CALIDAD S.L. (CASTELLÓN) 10. LABNOVA DISTRIBUCIONES ALIMENTARIAS S.L. (BURGOS)

4 Our analysis o Microbiology o Bromatology o Additives o Mycotoxines o Drinking water o Waste water o Soil o Pathogenic micro-organisms identification o And so on

5 Microbiological Analysis o Indicator parameters (both in food and water): Aerobic mesophilic Enterobacteria Molds and yeasts Coliforms Fecal coliforms Sporulated microorganisms psicotrophics Lactic acid bacteria Aerobic thermophilic Anaerobic Anaerobic sulfite reducing Streptococcus

6 Microbiological Analysis o Pathogenic micro-organisms Bacillus cereus Clostridium perfringens Escherichia coli Staphylococcus aureus Salmonella Listeria monocytogenes Pseudomona aeruginosa Legionella pneumophila...

7 Bromatologic Analysis o Nutritional facts: Moisture, fat, protein, carbohydrates, etc. o Fat: Saturated fatty acids, unsaturated fatty acids, cholesterol, sterols... o Minerals: Iron, calcium, magnesium. o Vitamins

8 Pollutants o In compliance with Regulation 1886/2006: Nitrates Heavy Metals Mycotoxines Dioxins and PCBs

9 Allergens o Gluten o Lactose o Sulphites o Soya o Egg o Nuts

10 Drinking water o Microbiological analysis o Phisico-chemical parameters: Nitrites Nitrates Chloride Sulphate o Metals: Sodium, calcium, magnesium Heavy metals as lead, cadmium, mercury, arsenic o Another contaminants Pesticides, hydrocarbons

11 Industrial water o Ultrapure water Low detection limits for many substances, as TOC (Total Organic Carbon), under the limit set by the Real Farmacopea Española o Tower water Phisico-chemical and microbiological control, including Legionella Pneumophyla o Sewages Control of industrial waste water in order to compliance the legal requeriments Automatic sampler, to make a representative sample during all the working day Collaborative with the Hidroghaphic Confederation

12 Enviromental Analysis o Sewages o Muds Controlling their adequation to be used in agriculture

13 Agriculture o Soil Texture, ph, organic materia, calcic carbonate, etc. To know the adequation of the soil for a crop, and to choose the fertilizing it needs o Fertilizers Total NPK amount Another nutrients like calcium and magnesium

14 Instrumental Analysis o GC o GC-MS o HPLC o LC-MS/MS

15 GC and GC-MS o Gas cromatography: Fatty acids profile Sterols Alcohols o GC-MS: Pesticide residues Hydrocarbons Phenols PAH s VOC s

16 HPLC o Amino-acids: complete aminogram, lysine, methionine, tryptophan o Organic acids (fumaric, lactic) o Veterinary medicinal products: tetracyclines, sulfonamides, tiamulin, trimethoprim, amoxicilin, lincomycin, tylosin, salinomycin, monensin o Vitamines: A, D, E, vitamin B group (both in animal and human feed)

17 HPLC o Preservatives: sorbic acid, propionic acid o Antioxidants: BHT, BHA, ethoxiquin o Dyes o Sugars o Sweeteners

18 HPLC Our Instrumental Departament we have three HPLC equipments

19 LC-MS/MS o Mycotoxines o Medicine residues o Pesticide residues

20 ISO 17025:2005 Three current acreditations: o Dossier 552/LE1333 Human food and animal feed Microbiology and phisic-chemical o Dossier 552/LE1225 Drinking water, continental water and waste water Microbiology and phisic-chemical (Including Legionella) o Dossier 1013/LE1770 Animal feed (antibiotics) and human food (preservatives) HPLC methods

21 ISO 17025: targets: o Heavy metals o More preservatives o Mycotoxines (LC-MS/MS) o Alergens

22 THANK YOU

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