POLIMERSAN A.S. Orta Mahalle Universite Cd. 29 Orhanli-Tuzla Istanbul (EE)
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1 FOOD PACKAGING MATERIALS FOOD CONTACTS 04\FPM\FDC\14_3 Rev. 1 1/05/ POLIMERSAN A.S. Orta Mahalle Universite Cd. 2 Orhanli-Tuzla 3456 Istanbul (EE) D.P.R. 777 dated 23/08/182, D.L. 108 dated 25/01/12, D.M.34 dated 21/3/73 European Directives: 82/711/EEC GUCEE L 27 dated 23/10/82, 85/572/EEC GUCEE L 372 dated 31/12/185, 3/8/EEC GU L0 dated 14/04/13, 7/48/EC GUCE L 222 dated 12/8/7. Regulations 135/2004/EC GUCE L 338 dated 13/11/04 and 185/2005/EC GUCE L 302 dated 1/11/2005. Regulation 10/2011/EU, GUUE L 12 del 15/01/2011, and subsequent updatings. UNI EN :2003. POLIMERSAN A.S. Mr. Umut Korkmaz Copy to Division Head
2 04\FPM\FDC\14_3 Rev. 1 1/05/ GENERALITIES - Sample receiving date: 11/04/ Analysis start date: 22/04/ Analysis end date: 15/05/ Deviation from test methods: NO SAMPLE DESCRIPTION SAMPLING The initial sampling has been done by the customer. The sampling for the test has been done drawing casually part of the sample in our possession. DECLARATION The test results of the present report are related exclusively to the tested sample. The present test report cannot be partially reproduced without the authorization of CSI managing Director. The uncertainties are estimated as extended obtained multiplying the standard by the coverage factor k corresponding to a confidence level of about 5%. Normally, this factor = 2. (*)Not under ACCREDIA accreditation. PERFORMED DETERMINATIONS 1) DETERMINATION OF THE OVERALL MIGRATION D.P.R. 777 dated 23/08/182, D.L. 108 dated 25/01/12, D.M.34 dated 21/3/73 European Directives: 82/711/EEC GUCEE L 27 dated 23/10/82, 85/572/EEC GUCEE L 372 dated 31/12/185, 3/8/EEC GU L0 dated 14/04/13, 7/48/EC GUCE L 222 dated 12/8/7. Regulations 135/2004/EC GUCE L 338 dated 13/11/04 and 185/2005/EC GUCE L 302 dated 1/11/2005. Regulations 10/2011/EU, 321/2011/EU and 1282/2011/EU. UNI EN :2003. UNI EN :2003, UNI EN :2003 e UNI EN :2003. This test report delates ad replaces Test report N 04\FPM\FDC\14 issued on 16/05/2014
3 04\FPM\FDC\14_3 Rev. 1 1/05/ Food simulant Contact condition Acetic acid in aqueous solution 3% w/v 2 hours at 100 C Ethanol 10% v/v 2 hours at 100 C Rectified olive oil 2 hours at 100 C Migration test was carried out by TOTAL IMMERSION. LOD (limit of detection): 1 mg/dm 2. 2) SPECIFIC MIGRATION OF BA, CO, MN, ZN, CU, FE, LI(*) Determination of the specific migration of Ba, Co, Mn, Zn, Cu, Fe, Li according to Reg. EU 10/2011 from the tested material into the simulants by ICP (Inductively Coupled Plasma) technique. The quantitative evaluation was carried out by external calibration of the elements in the same liquid simulants. Ba - SML: 1 mg/kg; LOD: 0.02 mg/kg Co - SML: 0.05 mg/kg; LOD: 0.02 mg/kg Mn - SML: 0.6 mg/kg; LOD: 0.02 mg/kg Li - SML: 0.6 mg/kg; LOD: 0.02 mg/kg Zn - SML: 25 mg/kg; LOD: 1 mg/kg Cu - SML: 5 mg/kg; LOD: 1 mg/kg Fe - SML: 48 mg/kg; LOD: 1 mg/kg 3) QUANTITATIVE DETERMINATION OF PRIMARY AROMATIC AMINES: METHOD L (LMBG 35) The procedure used to quantify the primary aromatic amines was a spectrophotometer method, based on the colour complex formed by a diazotization and a coupletization reaction. The solution was further concentred and eluted on a solid phase column. The final solution was photometrically detected at 550 nm (Method BGVV 64 LFGB, L dated 15, updated 2002) LOD: 0.2 µg /100 ml or LOD: mg/kg or LOD: mg/dm2 (the limit is originally expressed in mg/kg; it is possible to convert the measure unit by dividing for the factor 6 to express them in mg/dm2.) This test report delates ad replaces Test report N 04\FPM\FDC\14 issued on 16/05/2014
4 04\FPM\FDC\14_3 Rev. 1 1/05/ ) SPECIFIC MIGRATION OF NOT DECLARABLE COMPOUND N.1 (*) Determination of the specific migration of Not Declarable Compound n.1 from the tested material into the simulant, by GC-MS analysis. The quantitative evaluation was carried out by external calibration of Not Declarable Compound N.1 in the same liquid simulants. LMS: YES not declarable LOD: 1.0 mg/kg 5) OLFACTORY ORGANOLEPTIC TEST (*) The olfactory scoring test is a evaluation of the odor, measured with a 5 point scale. Each judge is asked to smell a series of coded dark flasks containing the samples. They are then asked to give a mark to each flask: 0: no perceivable smell 1: little perceivable smell, very difficult to define; 2: weak but identifiable smell; 3: strong smell; 4: very strong smell The final result is expressed with the average value of the scores given by each judge, coupled with the standard deviation. Testing conditions: time of conditioning : 18 ore temperature of conditioning : 55 ± 1 C n judges : 6 quantity of sample: 10 g volume of jar: 500 ml A potential organoleptic impact is to be acknowledged to the sample if the average score plus one time the standard deviation is 3. This test report delates ad replaces Test report N 04\FPM\FDC\14 issued on 16/05/2014
5 04\FPM\FDC\14_3 Rev. 1 1/05/ RESULTS 1) DETERMINATION OF THE OVERALL MIGRATION Food simulant: Acetic acid in aqueous solution 3% w/v Measured unit: mg/dm 2 Measured value Average value ± 2 Food simulant: Ethanol 10% v/v Measured unit: mg/dm 2 Measured value Average value ± 2 measured value average value Food simulant: Rectified olive oil Measured unit: mg/dm 2 To be subtracted from replications average if >2 Replications average volatiles average Limit value < ± 3 This test report delates ad replaces Test report N 04\FPM\FDC\14 issued on 16/05/2014
6 04\FPM\FDC\14_3 Rev. 1 1/05/ ) SPECIFIC MIGRATION OF BA, CO, MN, ZN, CU, FE, LI (*) Metals Food simulant: Acetic acid in aqueous solution 3% w/v Average value (According to Reg. EU 10/2011) Ba < Co < Mn < Zn - 25 Cu - 5 Fe - 48 Li < Metals Food simulant: Ethanol 10% v/v Average value (According to Reg. EU 10/2011) Ba < Co < Mn < Zn - 25 Cu - 5 Fe - 48 Li < This test report delates ad replaces Test report N 04\FPM\FDC\14 issued on 16/05/2014
7 04\FPM\FDC\14_3 Rev. 1 1/05/ Metals Food simulant: Rectified olive oil Average value (According to Reg. EU 10/2011) Ba < Co < Mn < Zn - 25 Cu - 5 Fe - 48 Li < ) QUANTITATIVE DETERMINATION OF PRIMARY AROMATIC AMINES: METHOD L (LMBG 35) Food simulant: Acetic acid in aqueous solution 3% w/v Measured unit: mg/kg measured value average value standard deviation limit value 10/2011) < < < mg/kg This test report delates ad replaces Test report N 04\FPM\FDC\14 issued on 16/05/2014
8 04\FPM\FDC\14_3 Rev. 1 1/05/ ) SPECIFIC MIGRATION OF NOT DECLARABLE COMPOUND N.1 (*) Food simulant: Acetic acid in aqueous solution 3% w/v measured value average value < SML --- YES Food simulant: Ethanol 10% v/v measured value average value < SML --- YES Food simulant: Rectified olive oil measured value average value < SML --- YES This test report delates ad replaces Test report N 04\FPM\FDC\14 issued on 16/05/2014
9 04\FPM\FDC\14_3 Rev. 1 1/05/2014 5) OLFACTORY ORGANOLEPTIC TEST (*) The average scores and the standard deviation obtained from the test are reported in the following table: Sample Average score Standard deviation Opinions and interpretations - not object of ACCREDIA accreditation. CONCLUSIONS In the chosen test condition the sample is suitable to be used in contact with aqueous, acidic and oily or fatty foodstuffs for which simulants A, B, and D2 are used. The sample tested by this Laboratory are therefore suitable to come in contact with foodstuff mentioned above on condition that they have been produced employing the monomers, additives and technical support agents according to in force legislation, specific migrations are respected and they do not induce any organoleptic modification on foodstuff. Date Division Head Managing Director 1/05/2014 Alberto Taffurelli Pasqualino Cau This test report delates ad replaces Test report N 04\FPM\FDC\14 issued on 16/05/2014
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