STANDARD DI CARNI NIST CARNI <<

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1 CARNI << STANDARD DI CARNI NIST SRM577b RM844 Malerial Bovine liver Bovine muscle powder (beef) 50 g x5 g Concentrations* (mg/kg, unless otherwise stated) Aluminium (3),7 Antimony (0,003) (0,0) Arsenic (0,05) 0,009 Barium (0,05) Boron 0,6 Bromine (9,7), Cadmium 0,50 0,03 Caesium (0,05) Calcium 6 45 Chlorine 0,78 Wt% 880 Chromium 0,07 Cobalt (0,5) 0,007 Copper 60,84 Fluorine (0,) Iodine 0,035 Iron 84 7, Lead 0,9 0,38 Magnesium Manganese 0,5 0,37 Mercury (0,003) 0,005 Molybdenum 3,5 0,08 Niclkel 0,05 Nitrogen Phosphorus,O Wt% 8360 Potassium 0,994 Wt% 570 Rubidium 3,7 8,7 Selenium 0,73 0,076 Silver 0,039 Sodium 0,4 Wt% 00 Strontium 0,36 0,05 Sulphur 0,785 Wt% 7950 Vanadium (0,3) (0,005) Zinc 7 4 * Values in brackets are noncertified values given for information only. The other values regarding RM844 are noncertified reference values provided with associated uncertainties, which may not include all sources of uncertainty or may reflect a lack of sufficient statistical agreement among multiple analytical methods. 3

2 >> CARNI NIST SRM546 Meat homogenate 4x85 g Certified Value* (g/kg, unless otherwise stated) Octanoic acid (C 8:0) (0,04) Decanoic acid (C 0:0) 0,7 Dodecanoic acid (C :0) 0,33 Tetradecanoic acid (C 4:4),53 Hexadecanoic acid (C 6:0) 45,6 9 - Hexadecanoic acid (C 6:) (6,83) Octadecanoic acid (C 8:0),7 (Z) Octadecenoic acid (C 8:) 8,0 9, - Octadienoic acid (C 8:) (9,6) 9,,5 - Octadecatrienoic acid (C 8:3) (,4) Eicosanoic acid (C 0:0) 0,35 -Eicosenoic acid (C 0:) (,56) 5,8,,4 - Eicosatetraenoic acid (C 0:4) (0,56) Boron (0,8) mg/kg Calcium 33 mg/kg Copper (0,93) mg/kg Iodine (0,4) mg/kg Iron,4 mg/kg Magnesium (65) mg/kg Manganese (0,9) mg/kg Phosphorus (540) mg/kg Potassium (460) mg/kg Sodium 9990 mg/kg Sulphur (900) mg/kg Zinc (8,5) mg/kg Chloride (500) mg/kg Vitamin B HC (,6) mg/kg Vitamin B (,00) mg/kg Vitamin B 6 (,30) mg/kg Vitamin B (0,006) mg/kg Niacin (36,3) mg/kg Pantothenic acid (5,76) mg/kg Biotin (0,036) mg/kg Solids (40,5)% Ash (3,)% Extractable fat (,0)% Fat as sum of fatty acids (9,7)% Protein (4,9)% Carbohydrates (,77)% Calories (5) kcal/00g Cholesterol 0,750 Sucrose (7,7) Folic acid (0,0) mg/kg Choline (ion) (580) mg/kg Inositol (30) mg/kg 3 * Values in brackets are noncertified reference values provided for analytes for which: ) the results have not been confirmed by an independent analytical technique as required for certification; ) the disagreement among the methods was greater than expected for certified values, and/or; 3) analyses have not been performed at NIST.

3 CARNI << IRMM, EUROPEAN COMMISSION Catalogue Number BCR-84 BCR-85R BCR-86 Bovine muscle Bovine liver Pig kidney 5 g (powder) 5 g (powder) 5 g (powder) Concentrations* (µg/kg, unless otherwise started) Arsenic Cadmium Calcium (50) mg/kg (95) mg/kg Chlorine (,0) g/kg (9,4) g/kg Chromium Copper,36 mg/kg 77 mg/kg 3,9 mg/kg lodine (40) (45) Iron 79 mg/kg 99 mg/kg Lead Magnesium (00) mg/kg (89) mg/kg Manganese 334 mg/kg,07 mg/kg 8,5 mg/kg Mercury,6 970 Nickel (70) (40) Phosphorus (8,3) g/kg (,) g/kg Potassium (6,6) g/kg (,6) g/kg Selenium Sodium (,0) g/kg (7,) g/kg Zinc 66 mg/kg 38,6 mg/kg 8 mg/kg * Values in brackets are not certified. VITAMINS* BCR-487 Pig s liver 5 g Certified Value (mg/kg) B (thiamin) 8,6 B (riboflavin) 06,8 B 6 (total pyridoxine) 9,3 B, Folate (total) 3,3 * Vitamins: information on nutritional composition of foods is essential for studies investigating the relascionship between diet and health or disease. The importance of realiable food composition data in the European Union is reflected in the issuing of Council Directive 90/496/Cee on the Nutritional Labelling of Foodstuffs. 33

4 >> CARNI IRMM, EUROPEAN COMMISSION METHYL ESTER OF BCR-63 Beef-Pork fat oil blend x5 ml Mass fraction* FATTY ACID METHYL ESTER/ TOTAL FATTY ACID METHYL ESTER (g/00 g) 4:0 n-tetradecanoic acid,9 4: ω5 (0,3) 5:0 (0,3) 6:0 n-hexadecanoic acid 5,96 6: n-hexadecenoic acid,58 6: ω9 (0,3) 7:0 () 7: (0,4) 8:0 n-octadecanoic acid 8,9 8: n-octadecenoic acid 38,34 8: ω7 (-3) 8: trans (0,5) 8: n-octadecadienoic acid 7,05 8: trans (0,5) 8: conj. (0,4) 8:3 n-octadecatrienoic acid 0,86 8:3 trans (0,5) 0:0 (0,3) 0: (0,8) 0: (0 3) 0:3 (0,3) :0 (0,5) STEROLS MASS FRACTION IN FAT (mg/00 g) Cholesterol 33,6 * Values in brackets are not certified. The fatty acid (methyl ester) profile was determined by capillary and packed gas chromatography. Although the entire profile is characterised, certified values are only given for the major components (> %) whereas indicative values are given for all minor components detected. BCR-444 BCR-445 Lyophilised porcine muscle Lyophilised porcine muscle x7,5 g (powder) x7,5 g (powder) Certified Value (µg/kg) Chloramphenicol <0, (Blank) 0,9 (Positive) Corresponding to approximately x5 g of fresh muscle. Determined by GC-MS, GC-ECD, HPLC-MS, HPLC-UV. 34

5 CARNI << IRMM, EUROPEAN COMMISSION BCR-384 Pork muscle 50 g (powder) Certified Value* (g/00 g, unless otherwise stated) Kjeldahl Nitrogen 3,7 Fat 0,8 Ash at 550 C 4,6 Calcium (0,) g/kg Chlorine (3,0) g/kg Magnesium,00 g/kg Phosphorus (8,5) g/kg Potassium 5,5 g/kg Sodium,8 g/kg * Values in brackets are not certified. Cat.No. IRMM-444 IRMM-445 IRMM-446 BCR-430 Pork fat Pork fat Pork fat Pork fat 5 g 5 g 5 g 3 g Concentrations* (ng/g) PCB CONGENER BLANK VERY LOW LEVEL LOW LEVEL PCB No.8 < 4,8 9,6 PCB No.5 <,9 5,5 PCB No.0 <,5 30,0 PCB No.8 <,7 30, PCB No.38 < 4,6 3,0 PCB No.53 < 3, 30,8 PCB No.80 <,6 9,8 Sum of the above PCBs <4 93, 07 Lindane (5,7) (5,6) (4,6) 4,4 -Tetrabromodiphenylether (3,7) (3,9) (6,) HCB 39 α-hch 40 β-hch 59 γ-hch 500 β-hepo 09 p,p -DDE 80 Dieldrin 4 Eldrin 0 p,p -DDT 3400 p,p -TDE (766) * Values in brackets are not certified and are only indicative values. 35

6 >> CARNI IRMM, EUROPEAN COMMISSION BCR-648 BCR-649 Lyophilised bovine liver Lyophilised bovine liver 0 g (powder) 0 g (powder) Certified Value* (µg/kg) Clenbuterol <0,5 (Blank) * Determined by RIA and GC-MS of TMS derivatives. BCR-4 BCR-4 Lyophilised bovine muscle Lyophilised bovine muscle,5 g (powder),5 g (powder) Certified Value (µg/l) Diethylstilboestrol <0, >0,5 Equivalent to 5,0 g of fresh bovine muscle tissue. Determined by GC-MS, after addition of 3,6 ml of distilled water. BCR-474 BCR-475 Lyophilised bovine liver Lyophilised bovine,8 g (powder),8 g (powder) Certified Value (µg/kg) 7α-Trenbolone <0,5 7,60 Equivalent to 0 g of fresh liver. Determined by RIA and GC-MS of MO-TMS derivatives. KEURINGSDIENST VAN WAREN KVW-PS7 Canned meat product (pork and chicken) 50 g Certified Value* (g/00 g) Moisture Starch Crude fat Ash Glutamic acid * At this moment the exact values of the constituents are not known, since this reference material is still in preparation. 36

7 CARNI << LGC PROMOCHEM LGC7000 LGC700 Beef/pork meat Pork meat 3 00 g 00 g Certified Values (g/00 g, unless otherwise stated) Ash 0,78 0,90 Chloride Fat,4 7,8 Moisture 66,5 68,6 Nitrogen,96,97 Calcium 53 mg/kg 39 mg/kg Potassium 590 mg/kg 860 mg/kg Sodium 360 mg/kg 50 mg/kg Zinc 4, mg/kg, mg/kg Values in brackets are not certified. Composed of 45% beef, 0% pork, 0% rusk, 4% fat, 0,5% emulsifier. Made up to 00% with water. 3 Composed of 50% pork leg, % rusk, 4% chicken fat, 0,5% emulsifier. Made up to 00% with water. LCG7 Pig liver paste 50 g Concentration (mg/kg) Aluminium () Cadmium 0,5 Calcium 49,9 Cobalt 0,06 Copper 7 Lead (0,) Magnesium 67 Manganese 3,04 Molybdenum (7) Phosphorus 3430 Potassium 770 Selenium 0,9 Sodium 8 Vanadium (0,0) Zinc 43,0 Values in brackets are not certified. Composed of 99,5% pig s liver and 0,5% stabiliser. 37

8 >> CARNI LGC PROMOCHEM LGC750 LGC75 LGC75 Pig liver paste Processed meat Processed pork meat Unit or Issue 5x50 g 5x50 g 5x50 g Assessed Values (g/00g) Moisture 65,3 63,6 6,0 Nitrate 0,085 Nitrogen,78,93,38 Salt 4,3 Casein (0,3) Hydroxyproline 0,7 Soya Protein (0,3) Ash 3,37 5,8 4,67 Total Fat 5,0 4,6 5,0 Values in bracked are indicative and given for information only. The salt content has been calculated from the cloride content of the material. LGC700 LGC70 LGC70 LGC703 LGC704 Beef meat, Beef meat, Lamb meat, Lamb meat, Pork meat, raw cooked raw cooked raw 3 Unit or Issue 30 g 30 g 30 g 30 g 30 g Certified meat species Assessed Content Beef meat 00% 00% Lamb meat 00% 00% Pork meat 00% Rump steak from Scottish Aberdeen Angus cattle, aged 0 months, purchased from an organic farm. The cattle had been fed grass rich in clover. Suffolk-cross leg of lamb, aged 9 months, was purchased from an organic meat supplier. 3 Free range Land Race/Large white cross pork leg steak, aged approximately 5 months at slaughter, was purchased from an organic meat supplier. LGC705 LGC706 LGC707 LGC708 LGC709 Pork meat, Chicken meat, Chicken meat, Turkey meat, Turkey meat, cooked raw cooked raw 3 cooked 3 Unit or Issue 30 g 30 g 30 g 30 g 30 g Certified meat species Assessed Content Pork meat 00% Chicken meat 00% 00% Turkey meat 00% 00% Free range Land Race/Large white cross pork leg steak, aged approximately 5 months at slaughter, was purchased from an organic meat supplier. Free range Ross whole chickens, aged 4 to 45 days at slaughter, were purchased from an organic meat supplier. 3 Organic turkeys were purchased from a local butcher's shop. 38

9 CARNI << NRCCRM GBW0855 GBW0855 Pork liver Pork muscle 5 g 0 g Concentrations* (µg/g, unless otherwise stated) Arsenic 0,044 Barium (0,39) Bromine 6, Cadmium 0,067 Caesium (0,4) Calcium Chlorine 0,87% Chromium (0,0) (0,39) Cobalt (0,00) (0,03) Copper 7, 3,88 Iron 0,05 % 43,6 Lead 0,54 (0,0) Magnesium Manganese 8,3 0,48 Mercury (0,03) Molybdenum 3,8 (0,055) Nitrogen 0,86%,7% Phosphorus (,3)% 0,83% Potassium,5%,40% Rubidium 4,7 Selenium 0,94 0,49 Sodium 0,33% 0,0% Strontium (0,8) Zinc 7 94, * Values in brackets are not certified. 39

10 >> CARNI SWEDISH MEAT RESEARCH INSTITUTE SMRD000 Meat 90 g Certified Value* (g/00 g, unless otherwise stated) Moisture 68,8 Ash,65 Fat 4,3 Nitrogen, N,63 Hydroxyproline 0,33 Starch 3,85 Salt, NaCl,9 Calcium 70,3 mg/kg Iron 6,33 mg/kg Phosphorus 075 mg/kg Potassium 859 mg/kg Sodium 8533 mg/kg Standard non inclusi nel catalogo sono disponibili su richiesta. Contattateci! 30