UV Filters: TiO 2 encapsulated Silica Bead

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1 Cosmetic Raw Material Presentation SJ Presentation_3.2_UV_TiO2 encapsulates_ver1.0 UV Filters: TiO 2 encapsulated Silica Bead For more information, please visit our home page: or sales@sunjinchem.co.kr or call office tel: (300) or call mobile: CHEMICAL R&D CENTER

2 UV Encapsulates - Overview Why do you mix UV filters & Spherical Beads SEPARATELY in your formulation? Micro Bead Mixed + Inorganic UV Filter Encapsulated

3 SUNSIL T in 40: TiO 2 Encapsulated Silica Bead TiO 2 30~40% 5um Silica Bead With 12nm TiO 2 40% TiO 2 is encapsulated in 5um silica bead The crystal size of TiO 2 is on average 12nm and is perfectly encapsulated within the silica bead Due to encapsulation, surface characteristics, e.g. rough touch & feel, of TiO 2 are not present. As nano-sized TiO 2 is well dispersed within the silica beads, transparency of T in 40 is exceptionally good. As the surface of T in 40 is silica, T in 40 exhibits the excellent dispersion properties of silica in both oil and water media. The manufacturing process is easier and formulation stability is more reliable compared to the use of common nano-sized TiO 2. Synergistic SPF boost shown with TiO 2.

4 SUNSIL T in 40(Silica/TiO 2 composites): advantages TiO 2 30~40% Silica 60~70% TiO2 (3) Easy to disperse T in TiO 2 T in TiO 2 (1) Excellent Transparency Same TiO2 content 0.2mg/cm 2 SPF 13.8 SPF 8.7 (2) Excellent Feel TiO2 Silica It s SPHERICAL! 24hrs later (4) Synergistic SPF boost See in the next page

5 Reference Formular: W/S cream type No Ingredients % INCI Name 1 water 45.1 water 2 DPG 4.6 dipropylene glycol 3 1,3-BG 5.8 butylene glycol 4 Magnesium sulfate 0.6 magnesium sulfate 5 Methyl paraben 0.2 methyl paraben 6 Germall imidazolidinyl urea 7 D-pantenol 0.6 panthenol 8 Kak-HL 3.5 hexyl laurate 9 KF cyclomethicone 10 DC KSG UV filters 11.6 dimethicone and dimethicone cross polymer dimethicone vinyldimethicone cross polymer and dimethicone 14 Sunsil-130SC 0.6 silica and dimethicone 15 SunPMMA 0.6 polymethyl Methacrylate 16 KF PEG-10 dimethicone 17 Abil EM cetyl PEG/PPG-10/1 dimethicone 18 Benton quaternium-18 hectorite 19 Propyl paraben 0.1 propyl paraben 20 Fragrance 0.3 fragrance Tested Mineral UV filters Mineral UV filters 1. Sunclear-T40 2. Sunclear-Z50 3. Sunsil-ZnO-AS 4. SUNZNO-NAS 5. ZnO-303S(Tayca) 6. Z-Cote HP-1(BASF) 7. Sunsil-TZin50-AS 8. Sunsil-Tin40 9. Sunsil-Tin Sunsil TinUVAB 11. UV-capsule MT100TV(Tayca)

6 Tin40, SPF booster: unit SPF 0.2/% ** Inorganic UV-filter (11.6%) SPF Whiteness Sensory Feel(Panel test) Avg. SPF/% BW #1 #2 avg. 1 Sunclear-T Sunclear-Z Sunsil-ZnO-AS SUNZNO-NAS ZnO-303S(Tayca) Z-Cote HP-1(BASF) Sunsil-TZin50-AS Sunsil-Tin Sunsil-Tin Sunsil TinUVAB UV-capsule MT100TV(Tayca) Organic(8.7%) Parsol Parsol MCX Benzophenone Tinsorb-M

7 But good synergistic SPF boost when properly used Formulation New Past New Past T in 40 TiO2 ZnO OMC UV filter Oil base Water base Net TiO2 Content SPF Spread Touch Transparency Good bad Good bad Good bad New = 7.5*40% = = 5.5 Past = = 10

8 Synergistic SPF study of UV filters What would be SPF synergy between different UV filters when used together? 4 major UV Filters tested: T40C: 40% TiO2 dispersion in Silicone oil SUNZNO-NAS: 40nm Zinc Oxide 5um Silica Bead With 12nm TiO2 inside by 35% OMC: Parsol MCX from DSM TiO 2 30~40% W/S formulation prepared In vitro SPF measurement Combinations tested Alone Double Triple All together September 2006

9 Chemical Filter Free 30.0 SPF Chemical filter free Good SPF synergy SPF 0.8 Tin40 4% 4.2 NAS 3% 5.2 SPF boost = 0.2 NAS 3% Tin40 4% SPF SPF boost = SPF boost = 5.7 Tin40 4% NAS 3% T40C 7% T40C 7% NAS 3% Tin40 4% Tin40 4% T40C 7% T40C 7% Tin40 4%

10 Chemical Filter Free Chemical filter free Tin40 is low SPF by itself But when used together with TiO2 & ZnO, this combination has very good complementary SPF boost Moreover, Tin40 has spherical silica bead so provides silky spread Tin40 4% NAS 3% T40C 7% T40C 7% NAS 3% Tin40 2% T40C 7% NAS 3% Tin40 4% So TiO2, ZnO and Tin40 combination is very good for Chemical filter free formulation For more detail, please refer to SJ_3.0_UVfilters_SPF synergy file

11 Maybelline SuperStay Foundation

12 COVER GIRL OUTLAST LIQUID FOUNDATION Foundation's new way to last through the day: STEP 1 The face base preps the skin, minimizes the appearance of fine lines, smoothes out pores and helps prevent shine. STEP 2 The make-up glides on and stays fresh with a natural coverage that lasts up to 10 hours. Hi Sung-Ho: Maybelline calls the uncolored side the "silky coverage extender". The two parts become one product during application. I think this is a marketing ploy to compete with P&G's foundation that has a white side and a colored side. In the case of P&G, the two products look like one package, but have two caps and are dispensed separately, and each has a different function. If this is not enough info, let me know. Diane

13 SPF data in W/O sun screen lotion type formulation Case 1 Case 2 Case 3 Case 4 Case 5 UV filter OMC Octyl methoxy cinnamate, DSM Tin40 TiO2 composited silica bead, TiO2 15nm TiO2,Tayca ZnO 100nm ZnO, T40 40% TiO2 dispersion, Total Oil Phase A.B Alkyl Benzoate Silicone D5 cyclomethicone KF6017 Silicone emulsifier Total Water Phase Water Bentonite Total Evaluation SPF UVA/UVB ratio Boots Star Rating Erythermal UVA PF Critical wavelength Best transparency Best Feel Highest SPF 1:1 substitute with TiO 2

14 Formulation, SJS-001 Transparent Sun Cream, W/O type SPF36, PA++ T in 40 provides excellent transparency and soft spread and good sensory N o Ingredients % INCI Name 1 Water To 100 Aqua 2 Glycerin 98% 4.0 Glycerin 3 1,3 BG 2.0 Butylene glycol 4 NaCl 0.5 Sodium chloride 5 Mehtyl paraben 0.2 Methyl paraben 6 Phenoxy ethanol 0.3 Phenoxy ethanol In Vivo Tested Formula Procedure 1) Heat the components 1-7 up to 75 2) Heat the components 8-9, and up to 75 3) Disperse the components 10,11 into part 2 4) Add slowly 1) into the 3) during mixing with homo mixer. 5) Mix with homo mixer at 3500rpm for 20 min. 6) Cool down to 50 and add the component 21, then mix with homo mixer at 3500rpm for 10 min. 7) Cool down to EDTA-2Na 0.0 Disodium EDTA 8 KF Cyclomethicone 9 Uvinul MC Octylmethoxy cinnamate 10 SUNSIL-Tin Silica & Titanium dioxide 11 SUNZNO-NAS 5.0 Zinc oxide & alkyl silane 12 Tegosoft DEC 5.0 Diethylhexyl carbonate 13 Finsolv-TN 4.0 C12-15 Alkyl benzoate 14 Abil EM Cetyl PEG/PPG-10/1 dimethicone 15 Normcort HK-G 1.0 Glyceryl behenate/eicosadioate 16 Stearic acid 0.5 Stearic acid 17 Bentone Quaternium-18 hectorite 18 KSG Arlacel Sorbitan sesquioleate 20 Tocopheryl acetate 0.1 Tocopheryl acetate Dimethicone vinyldimethicone crosspolymer and dimethicone 21 Fragrance 0.3 Fragrance

15 스캐더 (SCADDER) Plastic 70% TiO2 24% ZnO 6% 태평양에서개발하여, IR52 장영실상을받은태평양전용원료입니다. Hydrophobic PMMA shell이우수한상용성및사용감을부여합니다. Recommended for Skin care products with daily UV protection

16 SUMMARY composition size Spec UV Evaluation Recomm endation Remarks SUNZNO-NAS UV Capsule 60 SUNSIL Tin40 SUNSIL-TZin50AS TiO2-50~60 30~40 16~25 ZnO 97 min ~24 Silica - 40~50 60~70 45~67 Alkyl Silane 3 max 5 max - 6 max Primary(nm) Secondary( μm ) Apparent Density 0.75(g/cc) BET (m2/g) Oil Absorption(cc/g) 0.2(cc/g) SPF efficiency 1 SPF unit/g UVA protection Photostability Transparency Dispersibility Sensory feeling Make-up Skin care Sun Care For transparent & mild UV protection Avobenzone compatible TiO2 For transparent & silky premium sun care TiO 2 12/ZnO 40nm Good to achieve PA+++ in makeups SUNSIL-TinUVAB 30~40-60~70 - TiO 2 200nm Substitute pigmentary TiO2 in make-ups

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