SAMPLE IDENTIFICATION ANALYSIS. Date : January 19, 2017
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1 Date : January 19, 2017 SAMPLE IDENTIFICATION Internal code : 17A03-TOB24-1-DM Customer identification : Geranium BP Type : Essential Oil Source : Pelargonium graveolens Customer : Serene Living ANALYSIS Method : PC-PA E06, "Analysis of the composition of a liquid essential oil by GC-FID" (in French). Analyst : Sylvain Mercier, M. Sc., chimiste Analysis date : Checked and approved by : Alexis St-Gelais, M. Sc., chimiste Note: This report may not be published, including online, without the written consent from Laboratoire PhytoChemia. This report is digitally signed, it is only considered valid if the digital signature is intact. Page 1 of 7
2 IDENTIFIED COMPOUNDS Identification Column: BP5 Column: WAX R.T. R.I. % % R.I. R.T. Molecular Class 3-Methylpentanol Aliphatic alcohol cis-hex-3-en-1-ol Aliphatic alcohol Heptanal Aliphatic aldehyde α-pinene Monoterpene Geranic oxide Monoterp. ether β-pinene Monoterpene Myrcene Monoterpene 6-Methyl-5-hepten-2-one Aliphatic ketone α-phellandrene 4.69* Monoterpene Δ3-Carene 4.69* 1008 [0.08] Monoterpene α-terpinene Monoterpene para-cymene Monoterpene Limonene Monoterpene β-phellandrene * Monoterpene 1,8-Cineole [0.05] * Monoterp. ether cis-β-ocimene Monoterpene trans-β-ocimene Monoterpene γ-terpinene Monoterpene cis-linalool oxide (fur.) Monoterp. alcohol Terpinolene Monoterpene trans-linalool oxide (fur.) Monoterp. alcohol para-cymenene Monoterpene 6,7-Epoxymyrcene Monoterp. ether Linalool 6.73* * Monoterp. alcohol cis-rose oxide 6.73* 1109 [6.93] Monoterp. ether trans-rose oxide Monoterp. ether Isopulegol [6.06] * Monoterp. alcohol Menthone 7.95* Monoterp. ketone Citronellal 7.95* 1154 [2.14] Monoterp. aldehyde Isomenthone Monoterp. ketone Terpinen-4-ol Monoterp. alcohol Menthol Monoterp. alcohol α-terpineol * Monoterp. alcohol Nerol Monoterp. alcohol Citronellol 11.21* Monoterp. alcohol Neral 11.21* 1244 [32.50] * Monoterp. aldehyde cis-isogeraniol Monoterp. alcohol Geraniol Monoterp. alcohol Citronellyl formate 12.72* * Monoterp. ester Geranial 12.72* 1277 [7.68] Monoterp. aldehyde Neryl formate Monoterp. ester Page 2 of 7
3 Geranyl formate * Monoterp. ester α-cubebene Sesquiterpene Citronellyl acetate [0.32] * Monoterp. ester α-copaene Sesquiterpene β-bourbonene Sesquiterpene β-elemene Sesquiterpene Geranyl acetate Monoterp. ester α-gurjunene Sesquiterpene Isocaryophyllene Sesquiterpene β-caryophyllene 20.35* * Sesquiterpene Geranic acid 20.35* 1398 [1.18] Monoterp. acid β-copaene [1.19] * Sesquiterpene Aromadendrene Sesquiterpene Seychellene 22.76* Sesquiterpene 6,9-Guaiadiene 22.76* 1427 [0.43] Sesquiterpene α-humulene Sesquiterpene allo-aromadendrene [7.28] * Sesquiterpene Citronellyl propionate Monoterp. ester Neryl propionate Monoterp. ester Germacrene D Sesquiterpene γ-muurolene Sesquiterpene β-selinene [0.46] * Sesquiterpene Viridiflorene Sesquiterpene Geranyl propionate Monoterp. ester α-selinene 26.56* [3.42] * Sesquiterpene Bicyclogermacrene 26.56* 1472 [0.35] [3.42] * Sesquiterpene Eremophilene Sesquiterpene α-muurolene Sesquiterpene γ-cadinene * Sesquiterpene δ-cadinene Sesquiterpene Zonarene [0.67] * Sesquiterpene trans-calamenene Sesquiterpene Geranyl isobutyrate Monoterp. ester trans-γ-bisabolene Sesquiterpene α-agarofuran Sesquiterp. ether Citronellyl butyrate Monoterp. ester Geranyl butyrate Monoterp. ester Spathulenol 33.90* Sesquiterp. alcohol Caryophyllene oxide 33.90* 1570 [0.17] Sesquiterp. ether Phenylethyl tiglate Phenolic ester 10-epi-γ-Eudesmol Sesquiterp. alcohol 1,10-diepi-Cubenol * Sesquiterp. alcohol 1-epi-Cubenol Sesquiterp. alcohol γ-eudesmol 37.02* Sesquiterp. alcohol Page 3 of 7
4 Hinesol 37.02* 1627 [0.16] Sesquiterp. alcohol Cubenol [0.17] * Sesquiterp. alcohol τ-cadinol Sesquiterp. alcohol τ-muurolol Sesquiterp. alcohol α-muurolol 37.79* Sesquiterp. alcohol β-eudesmol 37.79* 1646 [0.58] Sesquiterp. alcohol α-eudesmol 37.79* 1646 [0.58] Sesquiterp. alcohol α-cadinol Sesquiterp. alcohol Geranyl valerate Monoterp. ester Citronellyl tiglate Monoterp. ester Geranyl tiglate * Monoterp. ester Geranyl caproate isomer Monoterp. ester Geranyl caproate [0.92] * Monoterp. ester Geranyl caprylate Monoterp. ester Total identified 96.97% 97.01% *: Two or more compounds are coeluting on this column [xx]: Duplicate percentage due to coelutions, not taken account in the identified total Note: no correction factor was applied Page 4 of 7
5 OTHER DATA Physical aspect : Yellow liquid Refractive index : ± (20 C) COMPLIANCE WITH ISO 4731:2011(PELARGONIUM X, NORTH AFRICAN TYPE) Compound North Africa Min. % Max. % Observed % Complies? cis-rose oxide Yes trans-rose oxide Yes Menthone Yes Isomenthone Yes Linalool Yes 6,9-Guaiadiene Yes Citronellyl formate Yes α-terpineol Yes Geranyl formate Yes Citronellol Yes Geraniol Yes Geranyl butyrate Yes 10-epi-γ-Eudesmol Yes Geranyl tiglate Yes Phenylethyl tiglate Yes Refractive index Yes CONCLUSION No adulterant, contaminant or diluent were detected using this method. The oil complies with the ISO norm. Page 5 of 7
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