the new dna of high strength glass ceramics
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1 the new dna of high strength glass ceramics 1
2 the new dna of high strength glass ceramics Together with the Fraunhofer Institute and VITA, DENTSPLY has developed a new class of materials for high-strength glass-ceramic from zirconia-reinforced lithium silicate: ZLS. zls ZLS has a unique microstructure compared with traditional glass ceramics. It comprises three distinct properites. Properties of ZLS High glass content High translucency, opalescence, fluorescence 10% zirconia High mean flexural strength Very small lithium silicate crystals Ultra-fine microstructure Microstructures compared ZLS LS 2 The inclusion of 10% zirconia within ZLS results in lithium silicate crystals four times smaller than lithium disilicate. The result is an ultra-fine microstructure which combines high average flexural strength with a high glass content. Glass with completely dissolved zirconia Lithium silicate crystals, nm Glass Lithium disilicate crystals, nm 2
3 Clinical benefits of ZLS Aesthetic Chameleon effect and opalescence Strong For safety and long-term stability Fast Efficient, rapid processing DENTSPLY took ZLS as the starting point for the development of a new high-strength all ceramic system, to allow dental surgeries and laboratories to tap into these benefits. 3
4 AEsthetic, STRONG, FAST CELTRA owes its specific properties to its threefold functional microstructure. CELTRA contains lithium metasilicate, lithium disilicate and lithium phosphate crystals. CELTRA stands for successful all-ceramic restorations: with exceptional aesthetics... with outstanding strength Increased glass content visibly improves aesthetics by facilitating in-depth opalescence and fluorescence. This leads to a dynamic colour play that affects the aesthetic appearance of the entire tooth. The dissolution of zirconia reinforces the glass matrix without clouding the glass. This combined with the presence of the glass-ceramic crystals, results in very high strength. Opalescence Load at fracture, anterior crowns Transillumination Direct incident light MEDIAN LOAD AT FRACTURE [N] CELTRA e.max Vita Mark II Before artificial ageing After artificial ageing Thermal cycling (5 C 55 C), 6000 cycles, followed by 1.2 million chewing cycles at 70 N. 4 Data on file.
5 3... in minimal time Compatible with Sirona Equipment The very small glass-ceramic crystals are less than 1 µm in size and allow the material to be finished and polished in its final crystallised, tooth-coloured state. No additional crystallisation is required. CELTRA DUO is compatible with Sirona CEREC and Sirona inlab wet grinding machines, and others. If you have an MCXL or similar you are on your way to producing a new breed of glass ceramic. A ceramic glass furnace will add staining and glazing options. No extra hardware investment Easy processing No extra software investment The excellent aesthetic appearance of CELTRA can be enhanced with staining, and the strength of the restoration can be increased with a glaze-firing cycle. CEREC and inlab are not registered trademarks of DENTSPLY International Inc. 5
6 CELTRA : THE SYSTEM AT A GLANCE CELTRA for the dental laboratory Customisation options of 360 veneers: - Cut-back technique - Simple staining 6
7 CELTRA for production Crystallised, high strength (210 MPa; 370 MPa after glaze-firing). CELTRA DUO CAD/CAM workflow CAD CAM CAD/CAM-BLOCK CEREC AC CEREC MC XL or CELTRA DUO inlab MC XL CEREC AC, CEREC MC XL and inlab MC XL are not registered trademarks of DENTSPLY International Inc. CEMENTATION Calibra Operatory Kit 7
8 CELTRA DUO ONE BLOCK TWO TECHNIQUE OPTIONS 1 Minimal effort Grinding Polishing Luting Clinical outcomes Significantly higher fracture strength than traditional glass ceramics can be achieved in the same time without any additional equipment. Molar crown, block size C14, standard grinding program CELTRA DUO MIN 14:30 MIN glass ceramics MIN 13:00 min CELTRA DUO MPA 210 MPa glass ceramics MPA 120 MPa Grinding 8 SIGNIFICANTLY STRONGER THAN GLASS CERAMICS IN THE SAME TIME.
9 2 Maximum strength Grinding Glazing Luting The clinical outcome Glaze-firing CELTRA DUO can raise its fracture strength to 370 MPA in a total production time of only 27 minutes and 30 seconds. It takes 50 minutes and 50 seconds to achieve a comparable stength with Lithium Disilicate Molar crown, block size C14, standard grinding program CELTRA DUO lithium disilicate CELTRA DUO MPA MIN MIN 14:30 13:00 27:30 MIN 13:30 24:20 13:00 50:50 MIN 370 MPa lithium disilicate MPA 360 MPa Grinding Crystallisation Stain & Glaze firing SAME STRENGTH AS LITHIUM DISILICATE IN LESS TIME*. 9 * Stains and Glaze are applied onto a tooth-colored restoration
10 Finish strong CELTRA DUO can be cemented using DENTSPLY Prime & Bond XP and Calibra. These products offer proven compatibility and a successful clinical history. Other cementation systems may also be applicable. 1 Easy clean up 2 Shade Stable Chemistry Translucent Light Medium Dark Opaque Displayed colors may not perfectly represent the actual product Light cure excess cement up to 10 seconds to initiate a gel phase that makes clean up fast and simple. Five shades provide a full spectrum of aesthetic shading. The Shade Stable TM Chemistry ensures that the shades will not shift over time. Marginal Integrity of ceramic inlays after thermal cycling Without separate light curing of the adhesive layer Dentin Enamel MARGINAL INTEGRITY [%] 50 * * * Significantly lower than XP BOND + Self Cure Activator + Calibra 0 XP Bond + SCA + Calibra ED Primer 2 + Panavia F Multilink Primer 2 + Multilink 2 Syntac Classic 2 + Variolink II 2 10 Prime & Bond XP is formally known as XP Bond 1 Frankenberger et al (2008). Luting of ceramic inlays in vitro:marginal quality of self etch and etch-and-rinse adhesives versus self-etch cement. Dent Mater, Feb;24(2): Not a registered trademark of DENTSPLY International Inc.
11 FORGIVING 3 Technique Robustness XP Bond has shown promise, as it is relatively insensitive to the amount of residual dentin moisture. This characteristic can effectively widen the window of opportunity for bonding to demineralised dentin, and can generate a system with excellent dentin adhesion under a wide range of clinical conditions. (M. Latta) 1 Classic Etch&Rinse Adhesives require an optimum level of dentin moisture to reach their full potential. However, this is difficult to achieve and can lead to insufficient bond strength and post-operative sensitivities. Prime & Bond XP is forgiving! It offers extra Performance even under different levels of dentin moisture. Less worries for better results! Shear Bond Strength on over wet and over dried dentin 2 SHEAR BOND STRENGTH [MPa] Optimum Over wet Over dried 0 XP Bond Excite 3 Optibond Solo Plus 3 ScotchBond 1 TX 3 Syntac 3 Prime & Bond XP is formally known as XP Bond 1 Latta MA, Clinical Perspectives on Current Dental Adhesives, 2008 The Academy of Dental therapeutics and Stomatology ADTS CE course 2 Source: Latta et al.: Effect of Residual Dentin Moisture on Shear Bond Strength. J DentRes 2010; 89 (Spec Iss B): 4 3 Not a registered trademark of DENTSPLY International Inc. 11
12 ORDERING INFORMATION Product Name Product Code CELTRA Starter Kit CELTRA CAD Blocks (packs of 4) CELTRA DUO for Cerec and inlab CELTRA LT A1, C CELTRA LT A2, C CELTRA LT A3, C CELTRA LT A3.5, C CELTRA LT B2, C CELTRA HT A1, C CELTRA HT A2, C CELTRA HT A3, C Etching gel and neutraliser D CELTRA DUO Blocks Starter Kit Calibra Operatory Kit 12 1 CELTRA DUO > > One block two applications > > Exceptional aesthetics > > Outstanding strength 2 Calibra Operatory Kit > > Quick and easy application > > Everything from one source
13 Product Name Calibra Operatory Kit Product Code X Prime & Bond XP Prime & Bond XP Refill, 1 5 ml Self Cure Activator Self Cure Activator, ml K 3 Calibra Bonding System > > Non technique sensitive > > High adhesion performance > > Complete dark curing in conjunction with Calibra and Self-Cure Activator 13
14 ORDERING INFORMATION Product Name Product Code CELTRA Universal Glaze Universal Glaze 5 g D CELTRA Universal Liquids Universal Stain & Glaze Liquid 15 ml D Universal Stain & Glaze Liquid 50 ml D CELTRA Universal Stains Universal Stain, shade 0 5 g D Universal Stain, shade 1 5 g D Universal Stain, shade 2 5 g D Universal Stain, shade 3 5 g D Universal Stain, shade 4 5 g D Universal Stain, shade i1 5 g D Universal Stain, shade i2 5 g D Universal Stain, White 5 g D Universal Stain, Cream 5 g D Universal Stain, Sunset 5 g D Universal Stain, Copper 5 g D Universal Stain, Khaki 5 g D Universal Stain, Olive 5 g D Universal Stain, Mahogany 5 g D Universal Stain, Violet 5 g D Shade Guide - Universal Stains CELTRA Stains Starter kit Content: 1x Universal Stain & Glaze liquid / 15x Universal Stain / 1x Brush / 1x Firing Cotton / 1x Pin for firing / 1x Universal glaze D D CELTRA may be processed with CAD CAM systems capable of accepting Sirona material holders. For Information about the different CAD/CAM systems and their use, please contact your respective CAM supplier. For more information please contact your local DENTSPLY Territory Manager. 14
15 Product Name Product Code Dentsply All-Ceramic Die Material F Dentsply All-Ceramic Die Material F Dentsply All-Ceramic Die Material F Dentsply All-Ceramic Die Material F Dentsply All-Ceramic Die Material F Dentsply All-Ceramic Die Material F Dentsply All-Ceramic Die Material F Dentsply All-Ceramic Die Material F Dentsply All-Ceramic Die Material F Dentsply All-Ceramic Die Material F Dentsply All-Ceramic Die Material F Dentsply All-Ceramic Die Material F Auxiliary firing paste SuperPeg II CELTRA firing pin set 6 pcs CELTRA firing pads 3 pcs Die Material Shade Guide
16 K Last Revision: 01/ DENTSPLY (Australia) Pty Ltd. ABN Gilby Rd Mount Waverley VIC 3149 Phone: Fax: Data on file DENTSPLY (New Zealand) Tel: 0800 DENTSPLY ( ) Fax: 0800 DENTFAX ( )
the new dna of high strength glass ceramics
the new dna of high strength glass ceramics 1 the new dna of high strength glass ceramics Together with the Fraunhofer Institute and VITA, we have developed a new class of materials for high-strength glassceramics
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