RHOPLEX SF-3122 Binder for Solvent-Free Exterior Flat and Satin Paints

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1 SF-3122 Binder for Solvent-Free Exterior Flat and Satin Paints Description SF-3122 emulsion represents Rohm and Haas Company's progress in the design of a binder for low VOC and solvent-free exterior flat and satin paints. By solvent free, we mean that there are no organic solvents used as ingredients in the formulation and no formulation ingredients that themselves are formulated with organic solvents. The product design involves a relatively soft all-acrylic polymer backbone for good film formation without coalescent solvent. Proprietary technology is utilized to provide dirt resistance. SF-3122 emulsion has performed well in laboratory tests for low temperature (45 F) film formation, adhesion, dirt resistance and grain crack resistance in solvent-free formulations. Early prototype exposures dating from the mid-1980s indicate excellent resistance to cracking and flaking. Dirt resistance and adhesion to gloss alkyd and chalking surfaces have been equivalent to that of AC-264 emulsion. Some sacrifice in tint retention has been noted in more recent exposures and ongoing studies are underway, including exposures with formulations containing ROPAQUE OP-62LO opaque polymer. SF-3122 is now on exposure involving many formulation and exposure variables, including PVC (flat to semigloss) and volume solids, tints, opaque polymer, zinc oxide level, mildewcide, substrate and exposure orientation. Rohm and Haas continues to evaluate techniques for solvent-free mildew protection. A zinc oxide formulation that passes stability tests has been prepared. SKANE M-8 mildewcide is suitable for this formulation if the low level of VOC introduced is acceptable: propylene glycol that contributes 3-4 g/l of VOC. SF-3122 emulsion has rheology characteristics similar to those of AC-264. Thus, paints may be thickened with HEC for good flow and leveling but with limited film build. Nonionic rheology modifiers respond well with SF-3122 with respect to flow, film build and efficiency. SF-3122 exhibits the excellent alkyd and chalk adhesion associated with AC-264 emulsion. Typical Physical Properties These properties are typical but do not constitute specifications. Appearance Brookfield Viscosity, 25 C White milky liquid 500 cp Solids Content 60.5% ph 9.5 Weight per U.S. gallon, lbs Specific Gravity 1.06 Bulking Value of Dry Solids, U.S. gal./lb..108 Minimum Film Formation Temperature 0 C Formulating Tips and Guidelines The following ingredient recommendations are based on starting point formulation GRS 1361M (low VOC quality white flat paint). These ingredients were determined in studies to be the most stable in formulations containing zinc oxide. These studies evaluated the effects of the level and type of zinc oxide, dispersants, surfactants, VOC level, and binder type on the adhesion and stability of exterior flat acrylic paints. Recommendations include only ingredients that have minimal or no contribution to VOC in the formulation. Other ingredients that contain organic volatiles may perform just as well or better in obtaining specific properties. Thickeners A combination of HEC and ACRYSOL RM-2020NPR is recommended for optimum application properties (flow and film build). HEC can be used alone, but flow will not be as good and film build will be noticeably reduced.

2 Dispersants The choice and level of dispersant is critical in achieving 30-day heat-age and roller stability in solvent-free paints based on SF-3122 that contain zinc oxide. TAMOL 731 dispersant is recommended. Paints formulated with TAMOL 850 and KTPP, a dispersant combination often used in exterior flat paints containing zinc oxide, did not pass 30-day heat-age stability at 140 F. Flat paints containing TAMOL 165 dispersant were deficient in mudcrack resistance. Note: A paint containing TAMOL 731 and Triethanolamine (TEA) had the best stability properties. Surfactant Several surfactants were evaluated. Triton CF-10 surfactant offered the most efficient pigment wetting when used in the grind. In-Can Preservation KATHON LX 1.5% microbicide is the recommended preservative. It should be added to the grind, before the binder, to prevent formation of grit in the paint. Defoamer Colloid 643 is the recommended defoamer. It is widely used and provides consistent results. Mildewcides A combination of 25 lbs. of zinc oxide and 2 lbs. of mildewcide is the recommended mildewcide package. This combination contributes approximately 3-4 g of VOC/l to the paint formulation and provides a high level of mildew resistance. For solvent-free formulating, American process zinc oxide at 50 lbs. per 100 gal. or Polyphase P-100 at a level of 3 lbs. per 100 gal. can be considered. TiO 2 Ti-Pure R-902 is the recommended pigment. It has good stability in formulations containing zinc oxide. Zinc Oxide Eagle Zinc 417W, an American processed grade of zinc oxide, is recommended. It contributed better stability than other grades evaluated. In solvent-free formulations containing zinc oxide, the American process grade provided better adhesion to chalky latex than the French process grade AZ066LP. Extenders A standard extender package was used for the white formulations Minex 4, Icecap K, and Attagel 50. This package was used for the zinc oxide formulation studies. Note: Although coalescent contributes to VOC, it improves film formation properties when application conditions are marginal (low temperature and wind). If coalescent is used, 3% Texanol based on polymer solids is recommended. A 5% coalescent level should not be exceeded. The addition of coalescent, such as Texanol, can reduce freeze-thaw stability. Freeze-thaw and heat-age stability of a formulation should be checked carefully. To preserve thermal stability, 20 lbs. of propylene glycol must be added with 3% Texanol.

3 EXTERIOR LOW VOC FLAT HOUSE PAINT BASED ON SF-3122 FORMULATION GRS 1361M Pounds Gallons Natrosol 250 MHR (2.5%) Water TAMOL 731 (25.0%) Triton CF Colloid KATHON LX Ti-Pure R Eagle Zinc 417W Minex Icecap K Attagel SF-3122 (60.5%) Colloid Natrosol 250 MHR (2.5%) Water Totals PVC: 45.8 Volume Solids: 36.5 Lbs/Gal: 11.7 Weight Solids: 54.7

4 FORMULATION DATA EXTERIOR FLAT HOUSE PAINT FORMULATION BASED ON SF-3122 FORMULATION GRS1361M Formulation GRS1361m was developed to provide stability with zinc oxide and appearance and resistance properties equivalent to those provided by proven, quality exterior acrylic formulations. As with formulating any latex binder with zinc oxide, dispersant/zinc oxide/titanium dioxide grade and level are key. The combination of Ti-Pure R-902 and TAMOL 731 gave good heat age and roller stability with the grade of zinc oxide specified. However, freeze-thaw stability has not yet been achieved. The formulation was compared with quality exterior flat conventionally formulated paints based on AC-264 and on MULTILOBE 200 emulsions. Results are given below. Formulation GRS1361M GRS1361G GRS1361H MULTILOBE 200/ VOC 25# ZnO, TAMOL 850/KTPP SF-3122/ AC-264/ Description LoVo 25# ZnO, TAMOL 731 VOC 25# ZnO, TAMOL 850/KTPP Initial Viscosity KU ICI ph Equilibrated Viscosity KU, unsheared/sheared 96/85 91/83 102/96 ICI ph Heat 140 F for 10 days KU Viscosity, unsheared ICI Viscosity ph Heat F for 30 days KU Viscosity, unsheared ICI Viscosity ph Freeze Thaw (5 cycles) fail (1) pass pass Roller Stability, 10 day/30 day pass/pass pass/pass pass/pass

5 Binder Formulation SF-3122 GRS1361M AC-264 GRS1361G MULTILOBE 200 GRS1361H (Gloss Alkyd) 7 day dry 30 mins fog box >1750 >1750 > hrs fog box >1750 (Chalky Latex) 7 day dry 30 mins fog box > >1750 (Chalky Oil) 7 day dry 30 mins fog box Wet Adhesion 7 day dry Gloss Alkyd: Blister none none none Knife Peel Chalky Latex: Blister 6D 4MD 6D Knife Peel Chalky Oil: Blister 8D 6M none Knife Peel FILM FORMATION Mud Cracking (30 mils, wet) pass pass pass LTFF, 10 mils pass pass pass Safe Handling Information Rohm and Haas Material Safety Data Sheets (MSDS) contain pertinent information that you may need to protect your employees and customers against any known health or safety hazards associated with our products. Under the OSHA Hazard Communication Standard, workers must have access to and understand MSDS on all hazardous substances to which they are exposed. Thus, it is important that you provide appropriate training and information to your employees and make sure they have available to them MSDS on any hazardous products in their workplace. Rohm and Haas Company sends MSDS for all its products, whether or not they are considered OSHA-hazardous, to the bill-to and/or ship-to locations of all its customers upon initial shipment (including samples). If you do not have access to one of these MSDS, please contact your local Rohm and Haas representative for an additional copy. Updated MSDS are sent upon revision to all customers of record. In addition, MSDS are sent annually to all customers receiving products deemed hazardous under the Superfund Amendments and Reauthorization Act. MSDS should be obtained from your suppliers of other materials recommended in this bulletin. Rohm and Haas Company is a member of the American Chemistry Council (ACC) and is committed to ACC s Responsible Care Program. ACRYSOL, KATHON, MULTILOBE,, ROPAQUE, SKANE and TAMOL are trademarks of Rohm and Haas Company, or of its subsidiaries or affiliates. These suggestions and data are based on information we believe to be reliable. They are offered in good faith, but without guarantee, as conditions and methods of use of our products are beyond our control. We recommend that the prospective user determine the suitability of our materials and suggestions before adopting them on a commercial scale. Suggestions for uses of our products or the inclusion of descriptive material from patents and the citation of specific patents in this publication should not be understood as recommending the use of our products in violation of any patent or as permission or license to use any patents of the Rohm and Haas Company. Rohm and Haas, 2008 All rights reserved. September A319

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