Stabilisers INGREDIENTS. Acidified milk drinks. Premigum XLB Premigum XLB-8034 Premigum XLB Premigum XLB Premigum XLB-12054

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INGREDIENTS Acidified milk drinks Stabilisers To stabilise acidified milk drinks, different ingredients such as pectin, soy fibre polysaccharides (soy soluble fibre) and some types of carboxy methyl cellulose can be used. Premium Ingredients works continuously evaluating different types of hydrocolloids in order to find the ones that bring optimal functionality, fulfilling customer requirements and offering, apart from stability, a broad range of textures adapted to each market. Premigum XLB-15032 Premigum XLB-8034 Premigum XLB-15016 Premigum XLB-15027 Premigum XLB-12054

Basic principle for acidified milk drinks stabilisation Stabilisers are used in acidified milk drinks to protect milk casein micelles in an acid environment like juice. Stabilisers avoid casein micelles aggregation, preserving small particle size and keeping them in suspension. Therefore, it prevents protein precipitation, occurrence of undesirable sediment with sandy texture at the bottom of the container and clarification of the rest of the beverage. Stabilisers help to maintain original organoleptic characteristics of the acidified milk drink. Traditionally, high methoxyl pectin has been used for this purpose. ph 6.7-5.8 ph 5.8-5.2 ph 5.2-3.8 No Stabilizer K-Casein Casein micelle Precipitation HM - Pectin HM - Pectin Suspension Model of non-homogenised casein micelles, subject to different ph, with and without stabiliser-pectin.

Product range and recommendations Body Freshness Stability Optimal Dose* Cost ph range Premigum XLB-15032 * *** **** 3.80-4.10 0.2-0.3 *** Premigum XLB-8034 ** *** *** 3.80-4.10 0.3-0.5 ** Premigum XLB-15016 *** *** *** 3.80-4.10 0.3-0.5 ** Premigum XLB-15027 **** ** ** 3.90-4.10 0.5-0.6 * Premigum XLB-12054 ***** * * 3.90-4.10 0.6-0.7 * *Recommended dose to stabilise 0,3% protein. Acidified milk drinks Premigum XLB-15032 Based on soluble soy fibre (without E number) and pectin. It provides a very fluid drink with high stability. Premigum XLB-8034 Based on pectin. Traditionally the most extended. It provides a lot of freshness to the drink. Premigum XLB-15016 Based on pectin and guar gum. It provides slightly more viscous texture than the previous ones. Premigum XLB-15027 Based on carboxy methyl cellulose and phosphate. It gives a creamier texture. Premigum XLB-12054 Based on carboxy methyl cellulose and guar gum. Used in Danao type drinks and also recommended for higher milk content drinks.

Stability analysis Comparative chart of the acidified milk drinks clarification rates, stabilized with the following products and the indicated doses, by applying a centrifugal force of 4000 rpm. The lower the clarification rate, the higher drink stability it is provided by the stabiliser. 30 25 24.71 28.99 % / h 20 15 15.89 19.09 19.22 10 5 0 Measurement of the acidified milk drink clarification rate through STEP technology (Space + Time resolved Extinction Profiles) using equipment Lumin Sizer 611. Spontaneously occurred clarification it is forced in each sample by centrifugation and it is quantified by transmitting light at every point and every moment.

General formula (by phases) INGREDIENTS Phase A Phase B Phase C % Juice 25.00 Citric acid To desired ph (optimal for final drink) Stabiliser It depends on the stabiliser Sugar 1.50 Water to 41.80 Skimmed milk powder 1.00 Sugar 7.00 Water 25.20

Acidified milk drinks General process 1 Phase A preparation: Add the juice to the mixing tank. If the juice is from fruit juice concentrate, add the concentrate and the water needed. Add the necessary citric acid for a ph of 3.8-4.1 in the final drink (add most of the citric acid in this phase and adjust the ph in the final drink. ph has to be below 4.5 before final correction). 2 Phase B preparation: Disperse the stabiliser in the sugar. In a different tank with agitation or recirculation, add the stabiliser with sugar to the water and heat up to 80ºC. Mix at high speed until complete solution. Cool fast to 20-25ºC. 3 Add Phase B on Phase A. 4 Phase C preparation: Disperse the skimmed milk powder in the sugar. In a different tank with agitation, dissolve the skimmed milk powder and the sugar in the water (recommended 45-50ºC). Mix during 10 minutes and cool to 20-25ºC. 5 Acidified milk drink preparation: Add slowly Phase C on Phases A+B, under agitation. Adjust slight variations to desired Brix and ph. UHT treatment: preheat to 65-70ºC, homogenise at 180 bar, pasteurise at 120ºC, cool to 4-6ºC. Fill. Notes: If the recipe contains flavours, preservatives and / or colours, add at the end, before UHT treatment. The recipe is an approximation, it can be different depending on the final drink characteristics. BR-DA-003-(ENG)R0