Evaluation of bond to Enigma High Impact Denture Base

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page 13 Evaluation of bond to Enigma High Impact Denture Base 1 Assignment Evaluation of the bonding strength between each layer of artificial tooth material and denture base resin at the site of fracture after a tensile strength test. The following materials were evaluated: Evaluation Denture Base Material Teeth-Material 1. Enigma High-Base enigmalife Neck PMMA 2. Enigma High-Base enigmalife Dentine Composite 3. Enigma High-Base enigmalife Enamel Composite 2 Materials 2.1 Denture Base Material As Denture base Material was Enigma High-Base used. The Instruction for use was observed, particularly: Thick dentures Boil sufficient water to cover clamped flask, remove heat and place the flask into the water. Add 200ml cold water for every 2 liters of water used and leave for 60 minutes. Apply low heat to maintain temperature of water at about 70ºC for 30 minutes bring to the boil in not less than 10 minutes and boil for a further 20 minutes. Residual monomer content <1.6%. After all curing cycles bench cool the flask for 30 minutes prior to immersing in cold water before deflasking.

page 14 2.2 enigmalife Anterior sets were manufactured from Neck- Dentine and Enamel Material For the given Evaluation we prepared three sets of enigmalife Anterior teeth respectively completely from Neck, Dentine and Enamel Material. enigmalife Enamel Material (Composite) enigmalife Dentine Material (Composite) enigmalife Neck Material (PMMA) 3 Specimens All specimens were prepared according to the following photos.

page 15 4 Tensile strength test Bonding strength to denture resin was done in accord with ISO22112:2006-Point 5.3.1 5 Results 5.1 enigmalife Composite Enamel We obtained optimal results regarding the bonding strength of artificial tooth enamel material to Enigma High-Base. 5.2 enigmalife Composite Dentine We obtained optimal results regarding the bonding strength of artificial tooth dentine material to Enigma High-Base. 5.3 enigmalife Neck PMMA We obtained optimal results regarding the bonding strength of artificial tooth neck material to Enigma High-Base.

page 16 6 Comparison between enigmalife Neck, Dentine and Enamel Materials From the bonding properties point of view there was no visible difference between any of the tooth materials. 7 Conclusion All materials show a very good bond to the base material.

page 17 Evaluation of bond to Enigma High Impact Denture Base together with "Schottlander Composite Bonder" 1 Assignment Evaluation of the bonding strength between each layer of artificial tooth material and denture base resin at the site of fracture after a tensile strength test. Schottlander Composite Bonder was only applied to enigmalife Dentine and enigmalife Enamel The following materials were evaluated: Evaluation Denture Base Material Teeth-Material Bonder 1. Enigma High- Base enigmalife Neck PMMA --- 2. Enigma High- Base enigmalife Dentine Composite Schottlander Composite Bond 3. Enigma High- Base enigmalife Enamel Composite Schottlander Composite Bond 2 Materials 2.1 Denture Base Material As Denture base Material was Enigma High-Base used. The Instruction for use was observed, particularly: Thick dentures Boil sufficient water to cover clamped flask, remove heat and place the flask into the water. Add 200ml cold water for every 2 liters of water used and leave for 60 minutes. Apply low heat to maintain temperature of water at about 70ºC for 30 minutes bring to the boil in not less than 10 minutes and boil for a further 20 minutes. Residual monomer content <1.6%. After all curing cycles bench cool the flask for 30 minutes prior to immersing in cold water before deflasking.

page 18 2.2 Bonder Only on Dentine and Enamel -material was Schottlander Composite Bond applied. The Instruction for use was observed, particularly: Preparation of the contact surface between teeth material and base material. Sandblast the area to be connected with aluminum oxide with a particle size of 50 micron and at 2 bars pressure. Clean with oil-free compressed air. Application of Schottlander Composite Bond With a brush generously apply Schottlander Composite Bond and allow the solvents to evaporate for approximately one minute. Apply a second layer. Polymerize each layer in accordance with the light curing unit employed (9 min in Labolight). Polymerisation Device Bonding Opaque Gingival Paste & High Chroma Intermediate Polymerisation Final Polymerisation Surface Treatment Labolight LV-II/III 1 min. 0,5 min. 9 min. 9 min.

page 19 2.3enigmalife Anterior sets were manufactured from Neck, Dentine and Enamel Material For the given Evaluation we prepared three sets of enigmalife Anterior teeth respectively completely from Neck, Dentine and Enamel Material. enigmalife Enamel Material (Composite) enigmalife Dentine Material (Composite) enigmalife Neck Material (PMMA) 3 Specimens All specimens were prepared according to the photos.

page 20 4 Tensile strength test Bonding strength to denture resin was done in accord with ISO22112:2006-Point 5.3.1 5 Results 5.1 enigmalife Composite Enamel We obtained optimal results regarding the bonding strength of artificial tooth enamel material to Enigma High-Base. 5.2 enigmalife Composite Dentine We obtained optimal results regarding the bonding strength of artificial tooth dentine material to Enigma High-Base. 5.3 enigmalife Neck PMMA We obtained optimal results regarding the bonding strength of artificial tooth neck material to Enigma High-Base.

page 21 5.4 Comparison between enigmalife Neck-, Dentine and Enamel Material From the bonding properties point of view there was no visible difference between any of the tooth materials. 6 Conclusion All materials show a very good bond to the base material.

page 22 Evaluation of bond to "Pegasus" Pourable Cold Cure Denture Base 1 Assignment Evaluation of bonding strength between each artificial teeth material and Pegasus pourable cold cure denture resin at the site of fracture after a tensile strength test. Following material mix was evaluated: Evaluation Denture Base Material Teeth-Material 1. 2. 3. Pegasus Pourable Cold Cure Pegasus Pourable Cold Cure Pegasus Pourable Cold Cure enigmalife Neck PMMA enigmalife Dentine Composite enigmalife Enamel Composite 2 Materials 2.1 Denture Base Material Denture Base Material was Pegasus Pourable Cold Cure used. Directions are as shown.

page 23 2.2 enigmalife Anterior sets from full Neck Dentine and Enamel Material For the given Evaluation we prepared three sets of enigmalife Anterior teeth respectively from full Neck, Dentine and Enamel Material. enigmalife Enamel Material (Composite) enigmalife Dentine Material (Composite) enigmalife Neck Material (PMMA) 3 Specimens All specimens were prepared according to the following photos.

page 24 4 Tensile strength test Bonding strength to denture resin was done in accord with ISO22112:2006 Point 5.3.1 5 Results 5.1 enigmalife Enamel We obtained optimal results regarding the bonding strength of artificial tooth enamel material to Pegasus Pourable Cold Cure. 5.2 enigmalife Dentine We obtained optimal results regarding the bonding strength of artificial tooth dentine material to Pegasus Pourable Cold Cure 5.3 enigmalife Neck We obtained optimal results regarding the bonding strength of artificial tooth neck material to Pegasus Pourable Cold Cure

page 25 6 Comparison between enigmalife Neck, Dentine and Enamel Material From the bonding properties point of view there was no difference between any of the tooth materials. 7 Conclusion All materials show a very good bond to the Pegasus Pourable Cold Cure base material. 13.04.2015