May-4-017 (005.) ARM 017.4 Data Verification Page 1 of 10 Crop Code SEGIN SEGIN SEGIN SEGIN SEGIN SEGIN Common sesa> Common sesa> Common sesa> Common sesa> Common sesa> Common sesa> Part Rated PLANT C PLANT C PLANT C PLANT C PLANT C PLANT C Rating Date Jul-9-016 Jul-9-016 Aug-1-016 Aug-6-016 Dec-13-016 Dec-1-016 Rating Type PHYGEN PHYGEN PHYGEN PHYGEN PHYGEN MOICON Rating Unit % % % % % % Number of Subsamples 1 1 1 1 1 1 Assessed By J. Rose J. Rose J. Rose J. Rose J. Rose J. Rose Days After First/Last Applic. 13 13 13 13 7 7 41 41 150 150 158 158 Trt-Eval Interval 13 DA-A 13 DA-A 7 DA-A 41 DA-A 150 DA-A 158 DA-A Plot Sub 1 3 4 5 6 101 1 0 0 0 0 5.4 10 1 30 5 15 0 5.79 103 1 0 0 0 5.7 104 1 0 0 5 0 5.67 105 1 5 0 0 0 5.69 106 1 30 30 0 0 5.65 107 1. 108 1 5 5 0 0 5.6 109 1 5 85 75 60 5.4 110 1. 111 1 0 40 5 0 5.4 11 1. 10 1 5 5 5 0 5.56 09 1 0 0 0 0 5.54 08 1 30 0 5 0 5.56 07 1 0 5 0 0 5.58 06 1 0 15 5 0 5.7 05 1. 04 1 0 0 5 0 5.68 03 1 5 0 10 0 5.71 0 1 35 50 80 4.86
May-4-017 (005.) ARM 017.4 Data Verification Page of 10 Crop Code SEGIN SEGIN SEGIN SEGIN SEGIN SEGIN Common sesa> Common sesa> Common sesa> Common sesa> Common sesa> Common sesa> Part Rated PLANT C PLANT C PLANT C PLANT C PLANT C PLANT C Rating Date Jul-9-016 Jul-9-016 Aug-1-016 Aug-6-016 Dec-13-016 Dec-1-016 Rating Type PHYGEN PHYGEN PHYGEN PHYGEN PHYGEN MOICON Rating Unit % % % % % % Number of Subsamples 1 1 1 1 1 1 Assessed By J. Rose J. Rose J. Rose J. Rose J. Rose J. Rose Days After First/Last Applic. 13 13 13 13 7 7 41 41 150 150 158 158 Trt-Eval Interval 13 DA-A 13 DA-A 7 DA-A 41 DA-A 150 DA-A 158 DA-A Plot Sub 1 3 4 5 6 01 1 10 90 75 55 5.9 301 1 0 10 50 0 5.4 30 1. 303 1. 70 75 5.65 304 1. 95 85 75 5.3 305 1 5 10 0 0 5.68 306 1 5 30 0 0 5.67 307 1 0 5 5 0 5.7 308 1. 50 0 5. 309 1. 5 10 0 5.61 310 1 0 5 5 0 5.54 311 1. Sort Order: Assessment (Serpentine within blocks)
May-4-017 (005.) ARM 017.4 Data Verification Page 3 of 10 Crop Code Part Rated Rating Date Rating Type Rating Unit Number of Subsamples Assessed By Days After First/Last Applic. Trt-Eval Interval Plot Sub 101 1 10 1 103 1 104 1 105 1 106 1 107 1 108 1 109 1 110 1 111 1 11 1 10 1 09 1 08 1 07 1 06 1 05 1 04 1 03 1 0 1 SEGIN SEGIN Common sesa> Common sesa> PLANT C PLANT C Dec-1-016 Dec-1-016 WEIGHT YIELD LB lb/ac 1 1 J. Rose 158 158 158 158 158 DA-A 158 DA-A TY1 1 7 8 4.56 1110.6 3.34 810.1 5.06 18. 3.58 869.4 5.08 133.4.98 73.8 3.95 959.8 1.95 474.8 4.45 1083.8 4.05 984.7 5.33 196. 3.6 880.1 5.15 151.9 3 78.3 5 114.1 3.48 844.8 1.3 301.3
May-4-017 (005.) ARM 017.4 Data Verification Page 4 of 10 Crop Code Part Rated Rating Date Rating Type Rating Unit Number of Subsamples Assessed By Days After First/Last Applic. Trt-Eval Interval Plot Sub 01 1 301 1 30 1 303 1 304 1 305 1 306 1 307 1 308 1 309 1 310 1 311 1 SEGIN 1.6 390.1 1.78 433.4 1.96 476.1 1.37 334.3 4.83 117.8 3.59 871.8 4.78 1160.5 1.36 331.9 3.6 879.7 3.71 90. SEGIN Common sesa> Common sesa> PLANT C PLANT C Dec-1-016 Dec-1-016 WEIGHT YIELD LB lb/ac 1 1 J. Rose 158 158 158 158 158 DA-A 158 DA-A TY1 1 7 8
May-4-017 (005.) ARM 017.4 Site Description Page 5 of 10 Investigator: Jack Rose General Trial Information Conducted Under GLP: No Conducted Under GEP: No Investigator: Jack Rose Harvested Width, Unit: 6 FT Harvested Length, Unit: 30 FT % Standard Moisture: 6 Crop Description Site and Design Treated Plot Width: 6 FT Treated Plot Length: 5 FT Treated Plot Area: 150 FT Treatments: 11 Replications: 3 Study Design: RACOBL Randomized Complete Block (RCB) A Application Date: Jul-16-016 Appl. Start Time: 7:30 AM Appl. Stop Time: 8:30 AM Application Method: SPRAY Application Timing: PREPRE Application Placement: BROSOI Applied By: J. Rose Air Temperature, Unit: 76 f % Relative Humidity: 93 Wind Velocity, Unit: 1 MPH Wind Direction: S Dew Presence (Y/N): N no Soil Temperature, Unit: 80 F Soil Moisture: good % Cloud Cover: 100 Application Description No. Date By Deviations 1.Jul-16-016 J. Rose Treatments 7 and 10 not sprayed Reasons: Bottle failure Crop Code SEGIN SEGIN SEGIN SEGIN SEGIN Common sesame Common sesame Common sesame Common sesame Common sesame Part Rated PLANT C PLANT C PLANT C PLANT C PLANT C Rating Date Jul-9-016 Jul-9-016 Aug-1-016 Aug-6-016 Dec-13-016 Rating Type PHYGEN PHYGEN PHYGEN PHYGEN PHYGEN Rating Unit % % % % % Number of Subsamples 1 1 1 1 1 Assessed By J. Rose J. Rose J. Rose J. Rose J. Rose Days After First/Last Applic. 13 13 13 13 7 7 41 41 150 150 Trt-Eval Interval 13 DA-A 13 DA-A 7 DA-A 41 DA-A 150 DA-A AL AA Trt Treatment Rate No. Name Rate Unit 1 3 4 5 1 Untreated 0.0 d 4.3 cd 3.3 b 0.0 b AFFORIA.5 oz/a 1.5 a 1.1 bc 6.7 b 0.0 b 3 Starane Ultra 0.66 pt/a 0. d 8.6 bcd 0.0 b 0.0 b 4 Gramoxone Inteon 3 pt/a 0.0 d 1.1 d.5 b 0.0 b 5 Sharpen fl oz/a 0.4 cd 1.5 bcd.5 b 5.0 b
May-4-017 (005.) ARM 017.4 AOV Means Table Page 6 of 10 Crop Code SEGIN SEGIN SEGIN SEGIN SEGIN Common sesame Common sesame Common sesame Common sesame Common sesame Part Rated PLANT C PLANT C PLANT C PLANT C PLANT C Rating Date Jul-9-016 Jul-9-016 Aug-1-016 Aug-6-016 Dec-13-016 Rating Type PHYGEN PHYGEN PHYGEN PHYGEN PHYGEN Rating Unit % % % % % Number of Subsamples 1 1 1 1 1 Assessed By J. Rose J. Rose J. Rose J. Rose J. Rose Days After First/Last Applic. 13 13 13 13 7 7 41 41 150 150 Trt-Eval Interval 13 DA-A 13 DA-A 7 DA-A 41 DA-A 150 DA-A AL AA Trt Treatment Rate No. Name Rate Unit 1 3 4 5 6 Valor oz/a 1.4 a.1 bc.5 b 6.7 ab 7 Fierce 3 oz/a 8,4-D Amine pt/a 0.8 bc 14.8 bcd 1.7 b 0.0 b 9 Clarity pt/a 0.9 b 7.0 a 78.3 a 63.3 a 10 Affinity BroadSpec 1 oz/a 11 Facet 3 fl oz/a 0.0 d 8.1 b 5.0 b 0.0 b COC pt/a AMS 8.5 lb/100 gal LSD P=.05. 0.39 19.5 9.15 38.01 Standard Deviation. 0.1 11.06 5.03 1.96 CV. 36.66 54.0 44.15 171.87 Bartlett's X. 7.6 6.733.905 3.43 P(Bartlett's X). 0.14 0.457 0.81 0.18 Skewness. 0.168 1.3018*.1476* 1.8098* Kurtosis. -1.5368 1.0561 3.079* 1.584
May-4-017 (005.) ARM 017.4 AOV Means Table Page 7 of 10 Crop Code Part Rated Rating Date Rating Type Rating Unit Number of Subsamples Assessed By Days After First/Last Applic. Trt-Eval Interval Trt Treatment Rate No. Name Rate Unit 1 Untreated AFFORIA.5 oz/a 3 Starane Ultra 0.66 pt/a 4 Gramoxone Inteon 3 pt/a 5 Sharpen fl oz/a SEGIN SEGIN SEGIN Common sesame Common sesame Common sesame PLANT C PLANT C PLANT C Dec-1-016 Dec-1-016 Dec-1-016 MOICON WEIGHT YIELD % LB lb/ac 1 1 1 J. Rose J. Rose 158 158 158 158 158 158 158 DA-A 158 DA-A 158 DA-A ET6 TY1 1 6 7 8 5.593-4.780 a 1161.7 a 5.673-3.517 b 854.0 b 5.647-5.105 a 140.0 a 5.60-4.455 ab 108.8 ab 5.680-4.040 ab 980.9 ab
May-4-017 (005.) ARM 017.4 AOV Means Table Page 8 of 10 Crop Code Part Rated Rating Date Rating Type Rating Unit Number of Subsamples Assessed By Days After First/Last Applic. Trt-Eval Interval Trt Treatment Rate No. Name Rate Unit 6 Valor oz/a 7 Fierce 3 oz/a 8,4-D Amine pt/a 9 Clarity pt/a 10 Affinity BroadSpec 1 oz/a 11 Facet 3 fl oz/a COC pt/a AMS 8.5 lb/100 gal LSD P=.05 Standard Deviation CV Bartlett's X P(Bartlett's X) Skewness Kurtosis SEGIN SEGIN SEGIN Common sesame Common sesame Common sesame PLANT C PLANT C PLANT C Dec-1-016 Dec-1-016 Dec-1-016 MOICON WEIGHT YIELD % LB lb/ac 1 1 1 J. Rose J. Rose 158 158 158 158 158 158 158 DA-A 158 DA-A 158 DA-A ET6 TY1 1 6 7 8 5.350 3.345 b 813.0 b 5.60-4.77 ab 1039.1 ab 5.313-1.640 c 399.7 c 5.510-4.450 ab 1083.8 ab 0.5 1.389 301.14 0.151 0.6810 165.53.4 17.1 17.1 6.01 13.473 13.379 0.537 0.061 0.063-0.870-0.7649-0.761-0.191-0.1936-0.035
May-4-017 (005.) ARM 017.4 AOV Means Table Page 9 of 10 Randomized Complete Block (RCB) AOV For SEGIN Common sesame PLANT C Jul-9-016 PHYGEN % 1 J. Rose 13 13 13 DA-A AL (Data Column ) Total 19 8.80507 Replicate 0.067453 0.03376 0.755 0.4975 Treatment 8 8.33560 1.041950 3.39 0.0001 Error 9 0.40197 0.044664 Randomized Complete Block (RCB) AOV For SEGIN Common sesame PLANT C Aug-1-016 PHYGEN % 1 J. Rose 7 7 7 DA-A AA (Data Column 3) Total 3 145.313738 Replicate 76.044888 38.0444 0.311 0.7383 Treatment 8 10757.78407 1344.73009 10.984 0.0001 Error 13 1591.484778 1.41906 Randomized Complete Block (RCB) AOV For SEGIN Common sesame PLANT C Aug-6-016 PHYGEN % 1 J. Rose 41 41 41 DA-A (Data Column 4) Total 0 15466.666667 Replicate 1.388889 0.694444 0.07 0.9730 Treatment 8 151.500000 1901.56500 75.7 0.0001 Error 10 5.777778 5.77778 Randomized Complete Block (RCB) AOV For SEGIN Common sesame PLANT C Dec-13-016 PHYGEN % 1 J. Rose 150 150 150 DA-A (Data Column 5) Total 6 19866.666667 Replicate 516.666667 58.333333 0.536 0.5954 Treatment 8 11633.333333 1454.166667 3.015 0.087 Error 16 7716.666667 48.91667 Randomized Complete Block (RCB) AOV For SEGIN Common sesame PLANT C Dec-1-016 MOICON % 1 J. Rose 158 158 158 DA-A ET6 (Data Column 6) Total 1 0.49301 Replicate 0.001040 0.00050 0.033 0.9674 Treatment 7 0.30437 0.04346.778 0.0577 Error 1 0.187744 0.015645 Randomized Complete Block (RCB) AOV For SEGIN Common sesame PLANT C Dec-1-016 WEIGHT LB 1 J. Rose 158 158 158 DA-A (Data Column 7) Total 0 30.340741 Replicate 0.106469 0.05334 0.115 0.897 Treatment 8 5.596857 3.199607 6.900 0.003 Error 10 4.637415 0.463741 Randomized Complete Block (RCB) AOV For SEGIN Common sesame PLANT C Dec-1-016 YIELD lb/ac 1 158 158 158 DA-A TY1 1 (Data Column 8) Total 0 178895.697619 Replicate 669.7440 3134.8610 0.114 0.8930 Treatment 8 1508684.647065 188585.580883 6.883 0.003 Error 10 73998.36314 7399.83631 Crop Code SEGIN, BDIC, Sesamum indicum, Common sesame = US Part Rated PLANT = plant C = Crop is Part Rated Rating Type PHYGEN = phytotoxicity - general / injury MOICON = moisture content WEIGHT = weight YIELD = yield Rating Unit % = percent LB = pound lb/ac = pounds per acre Assessed By J. Rose = TDA 057530 AL = Automatic log transformation of X+1 AA = Automatic arcsine square root % transformation ET6 = Excluded treatment 6 TY1 = 4.0*[7]*(100-[6])/94
May-4-017 (005.) ARM 017.4 Trial Treatments Page 10 of 10 Trt Treatment Form Form Form Rate No. Type Name Conc Unit Type Rate Unit 1 CHK Untreated HERB AFFORIA 50.8 % WG.5 oz/a 3 HERB Starane Ultra.8 LBA/GAL EC 0.66 pt/a 4 HERB Gramoxone Inteon LB/GAL L 3 pt/a 5 HERB Sharpen.85 LBA/GAL SC fl oz/a 6 HERB Valor 51 %AW/W WG oz/a 7 HERB Fierce 76 %AW/W WG 3 oz/a 8 HERB,4-D Amine 4 LBA/GAL L pt/a 9 HERB Clarity 4 LBAE/GAL EC pt/a 10 HERB Affinity BroadSpec 50 % WG 1 oz/a 11 HERB Facet 1.5 LBAE/GAL L 3 fl oz/a -quinclorac 1.5 3 ADJ COC pt/a FERT AMS 8.5 lb/100 gal Replications: 3, Untreated treatments: 1, Design: Randomized Complete Block (RCB), Treatment units: US standard, Treated 'Plot' experimental unit size Width: 6 feet, Treated 'Plot' experimental unit size Length: 5 feet, Application volume: 0 GAL/AC, Mix size: liters, Format definitions: G-All7.def, G-All7.frm Product quantities required for listed treatments and applications of trials included in this table: Amount* Unit Treatment Name Form Conc Form Unit Form Type Lot Code 1.87 g AFFORIA 50.8 % WG 8.50 ml Starane Ultra.8 LBA/GAL EC 37.500 ml Gramoxone Inteon LB/GAL L 1.56 ml Sharpen.85 LBA/GAL SC 1.498 g Valor 51 %AW/W WG.47 g Fierce 76 %AW/W WG 5.000 ml,4-d Amine 4 LBA/GAL L 5.000 ml Clarity 4 LBAE/GAL EC 0.749 g Affinity BroadSpec 50 % WG 5.000 ml Facet 1.5 LBAE/GAL L * 'Per area' calculations based on spray volume= 0 GAL/AC, mix size= liters (mix size basis).