Compound ID:.7.6 8.64 8.55 8.37 7.57 8.35 7.33 7.3 6.87 GSK83875A-DMSO DMSO 4.3MHz 6.8 4. 4.8 4.6 3.78 3.33 3..8.8.5.5.6. Acquisition Parameters Date: 4-3-6T9:34: Pulse Sequence: zg3 Temperature: 96.7 C Number of Scans: 6 Frequency: 4.3 MHz Spectral Width: 8.8 Hz Nucleus: H Data Points: 3768 Relaxation Delay: s Pulse Width: 4.5 us F - Processing Parameters Data Points: 65536 DC:.5 LB:.3 Hz First Point:.5 FT: Hyper Quadrature Phase: Global 6 5 4 3.8.9.9.8.3 9 8.6.7 3.8 7. 6 f (ppm) 5..95 4 4.5 3.3 3 6. - - -3
4-3-4 4:5: / GSK83875A HPLC analysis ==== GSK83875A HPLC Report ==== Name : GSK83875A ID :GSK83875A Tray# : e : ul InjectionVail# Volum Information : 48 Data Filename : GSK83875A_7.lcd Method Filename : AB---MIN-45C.lcm Date Acquired : 4-3-4 4:35:4 Description : METHOD: - COLUMN: XBRIDGE 3.5UM.*5MM MOBILE: HO(.5%TFA)-ACN(.5%TFA) 7-8 MIN ACN FROM % TO % OVEN: 45C TOTAL FLOW RATE:.8ML/MIN -7 MIN ACN FROM % TO % <Chromatogram> GSK83875A.664 C:\acdata\43\4\LC-3\GSK83875A_7.lcd mv 5 Det.A Ch 5..5 5. 7.5 Det.A Ch / 4nm <Result> Area 699374 699374 Height 4867 4867 MedKoo Cat#: 4475 Name: GSK83875A CAS#: 635-97- Lot#BBC436 Chemical Formula: C7H9FN8O3 Exact Mass: 53.3467 Molecular Weight: 53.57 Area %.. PeakTable Detector A Ch 4nm Peak# Ret. Time.664 Total C:\acdata\43\4\LC-3\GSK83875A_7.lcd
GSK83875A HPLC analysis 4-3-4 4:5: / ==== GSK83875A HPLC Report ==== Information Name : GSK83875A ID : GSK83875ATray# : Injection Volume : ul : 48 Vail# Data Filename : GSK83875AA_7.lcd Method Filename : AB---MIN-45C.lcm Date Acquired : 4-3-4 4:35:4 Description : METHOD: - COLUMN: XBRIDGE 3.5UM.*5MM MOBILE: HO(.5%TFA)-ACN(.5%TFA) 7-8 MIN ACN FROM % TO % OVEN: 45C TOTAL FLOW RATE:.8ML/MIN -7 MIN ACN FROM % TO % <Chromatogram> B37-93A C:\acdata\43\4\LC-3\GSK83875A_7.lcd.664 Det.A Ch 5..5 5. mv 7.5 Det.A Ch / 54nm <Result> PeakTable Area 574954 574954 Height 95 95 MedKoo Cat#: 4475 Name: GSK83875A CAS#: 635-97- Lot#BBC436 Chemical Formula: C7H9FN8O3 Exact Mass: 53.3467 Molecular Weight: 53.57 Area %.. Detector A Ch 54nm Peak# Ret. Time.664 Total C:\acdata\43\4\LC-3\GSK83875A_7.lcd
: C:\QC\GSK83875A.D : B-8A GSK83875A LCMS analysis : IMM-FTE : AGILENT LCMS E : P-B-5 : 4/3/4 :6:34 : :.8 µl : D:\CHEM3_\METHOD\P-.M : 4/3/4 :5:59 : IMM-FTE ( ) : C:\Chem3\\METHODS\DEF_LC.M : 6// 6:4:44 : Easy-Access Method: 'P-'. DAD A, Sig=54,6 Ref=off (C:\QC\GSK83875A.D) mau 4 8 6 4.5.5..5 DAD C, Sig=4,6 Ref=off (C:\QC\GSK83875A.D) mau 5 5 75 5 5 ES-API, Pos, Scan, Frag: 7.5.5 MSD TIC, MS File (C:\QC\GSK83875A.D) 4 8 6 4 ES-API, Pos, Scan, Frag: 7.5.5 4 35 3 5 5 5 4/3/4 :33:9.5 MedKoo Cat#: 4475 Name: GSK83875A CAS#: 635-97- Lot#BBC436 Chemical Formula: C7H9FN8O3.43.5 MSD 533, EIC=53.7:533.7 (C:\QC\GSK83875A.D) /
: C:\QC\GSK83875A.D : B-8A : :. :. : DAD A, Sig=54,6 Ref=off # [] [] [mau*s] [mau] %. VV.43 4768.734 546.3936. : 4768.734 546.3936 : DAD C, Sig=4,6 Ref=off # [] [] [mau*s] [mau] %. VV.593 76.843 764.6995. : 76.843 764.6995 3: MSD TIC, MS File # [] [] %.5 VV.8.5377e7.3353e6. :.5377e7.3353e6 4: MSD 533, EIC=53.7:533.7 # [] [] %.43 BV.65.8687e6 4.8648e5. :.8687e6 4.8648e5 *** *** 4/3/4 :33:9 /
79: MS Spectrum MS Spectrum 8 6 4 *MSD SPC, time=.4 of C:\QC\GSK83875A.D ES-API, Pos, Scan, Frag: 7 Max: 747584 67. 4 6 8 4/3/4 :33:58 / 534. 533. m/z