Instruction Number: 5681 Component Description > COMPONENT SHEET > K 1690 COMBINATION BOILER/COOLING SYSTEM Alkalinity P/T (HCl) 1 x 5229 Instruction *1 x 9198 Sample Tube, Graduated, 25 ml, plastic w/cap 1 x R 0638 Phenolphthalein Indicator, DB 1 x R 0645 Total Alkalinity Indicator, DB 1 x R 0724 Hydrochloric Acid.12 N, DB Chloride 1 x 5212 Instruction *1 x 9198 Sample Tube, Graduated, 25 ml, plastic w/cap 1 x R 0630 Chromate Indicator, DB 1 x R 0638 Phenolphthalein Indicator, DB 1 x R 0686 Sulfuric Acid N, DB 1 x R 0706 Silver Nitrate Reagent, DB Hardness total 1 x 5202 Instruction *1 x 9198 Sample Tube, Graduated, 25 ml, plastic w/cap 1 x R 0619 Hardness Buffer, DB 1 x R 0620 Hardness Indicator Powder 1 x R 0683 Hardness Reagent, DB Molybdenum 1 x 4029 Pipet, Calibrated 0.5 & 1.0 ml, plastic 2 x 4030 Pipets, Calibrated 0.5 & 1.0 ml, plastic w/cap 1 x 4078 Pipet, Graduated, 3 ml (0.5 ml div.), plastic 1 x 5359 Instruction *3 x 9198 Sample Tubes, Graduated, 25 ml, plastic w/cap 1 x R 0890 Molybdenum Buffer Solution 1 x R 0892 Molybdenum Titrating Solution, DB 1 x R 0900 Molybdenum Indicator Powder 1 x R 0901 Molybdenum Indicator Solvent Nitrite, Sodium 1 x 4035 Sample Tube, Calibrated 5 ml, plastic 1 x 5011 Instruction 1 x R 0819 Ferroin Indicator, DB 1 x R 0820 CAN Solution, DB Phosphonate 1 x 5051 Instruction *1 x 9198 Sample Tube, Graduated, 25 ml, plastic w/cap 1 x 9315 Test Paper, ph, 1.8 3.8 1 x R 0686 Sulfuric Acid N, DB 1 x R 0697 Thiosulfate N/10, DB 1 x R 0802P XO Indicator Powder 1 x R 0803 Phosphonate Titrating Solution, DB 1 x R 0805 Fluoride Masking Agent, DB Silica 1 x 3267 Cap, Test Cell, 5 ml, rectangular, plastic 1 x 4005 Cylinder, Graduated, 50 ml (1.0 ml div.), glass 1 x 4025 Test Cell, Calibrated 5 ml, plastic 1 x 4026 Dipper, plastic, large 3 x 4030 Pipets, Calibrated 0.5 & 1.0 ml, plastic w/cap 1 x 5321 Instruction 1 x 6002 Brush, Cell Cleaner *1 x 9198 Sample Tube, Graduated, 25 ml, plastic w/cap 1 x 9257 Comparator, Midget, Silica, 5 50 ppm 1 x R 1305Q Silica Reagent #4
1 x R 1305U Silica Reagent #3 1 x R 1306T Silica Reagent #1 1 x R 1306U Silica Reagent #2 Sulfite, Sodium 1 x 5203 Instruction *1 x 9198 Sample Tube, Graduated, 25 ml, plastic w/cap 1 x R 0638 Phenolphthalein Indicator, DB 1 x R 0699 Iodide Iodate Reagent, DB 1 x R 0725 Acid Starch Indicator Powder Misc. 1 x 5681 Component Sheet *Kit includes four. TO ORDER REPLACEMENT PARTS AND REAGENTS CALL TOLL FREE 800 TEST KIT (800 837 8548). 5/08 2016 Taylor Technologies, Inc. All Rights Reserved View Privacy Policy
1 x 5011 Instruction 1 x 9198R Sample Tube, Graduated (25 ml) w/ cap & red dot, plastic 1 x R-0819-C Ferroin Indicator, 2 oz, DB 2 x R-0820-C CAN Solution, 2 oz, DB SODIUM NITRITE (1 drop = 40 ppm) Instr. #5011 Sodium Nitrite Test 1. Rinse and fill 25 ml sample tube (#9198R) to 5 ml mark with cooled (room temperature) water to be tested (). 2. Add 4 drops R-0819 Ferroin Indicator. Swirl to mix. Sample should turn reddish orange (). 3. Add R-0820 CAN Solution dropwise, swirling and counting after each drop, until color changes from reddish orange to blue (). 4. Multiply drops of R-0820 CAN Solution by 40. Record as parts per million (ppm) sodium nitrite. NOTE: For results as nitrite, multiply sodium nitrite concentration by 0.67. 800-TEST KIT (837-8548) 410-472-4340 8/16
PHOSPHONATE EQUIVALENCE (PPM) ATMP (1.0); Na 5 ATMP (1.3); HEDP (0.9); K 6 HDTMP (1.2); DTPMP (1.45), Na 5 DTPMP (1.7) Instr. #5051 1 x 5051 Instruction 1 x 9198P Sample Tube, Graduated (25 ml) w/ cap & purple dot, plastic 1 x 9315 Test Paper, ph, 1.8-3.8, 200 strips 1 x R-0686P-C Sulfuric Acid N, 2 oz w/ purple cap, DB 1 x R-0697-C Thiosulfate N/10, 2 oz, DB 1 x R-0802P-I Xylenol Orange Indicator Powder, 10 g 1 x R-0803-C Phosphonate Titrating Solution, 2 oz, DB 1 x R-0805-C Fluoride Masking Agent, 2 oz, DB NOTE: Iron can cause negative interference at a level greater than 5 ppm. Orthophosphate and polyphosphate can cause positive interference at all levels. NOTE: Run a blank using tap water. Normal blank requires about 2 drops of R-0803 Phosphonate Titrating Solution to reach endpoint. 1. Rinse and fill 25 ml sample tube (#9198P) to 25 ml mark with water to be tested (). 2. Add: 1 drop R-0697 Thiosulfate N/10 10 drops R-0805 Fluoride Masking Agent 1 level dipper R-0802P Xylenol Orange Indicator Powder Swirl to mix. 3. Adjust ph between 2.6 and 3.0: Add 1 drop R-0686P Sulfuric Acid N. Swirl to mix. Dip test paper (#9315) into sample, in direction of arrow, for 3 seconds, with all color zones immersed. Match indicator zone (unnumbered square between 2.7 and 3.0 color standards) with color scale. Read printed ph value. If necessary, continue adding R-0686P Sulfuric Acid N dropwise, swirling and checking ph with a new test paper after each drop, until a ph between 2.6 and 3.0 is obtained. Sample should be yellow (). 4. Add R-0803 Phosphonate Titrating Solution dropwise, swirling and counting after each drop, until color changes from yellow to purplish pink (). 5. Subtract drops of R-0803 Phosphonate Titrating Solution in blank from drops in sample (Step 4). Multiply by appropriate conversion factor (see CONVERSION FACTORS). Record as parts per million (ppm) phosphonate. CONVERSION FACTORS: To express phosphonate as: Multiply drops by: Aminotri(methylenephosphonic acid) (ATMP)... 1.0 Aminotri(methylenephosphonic acid), pentasodium salt (Na 5 ATMP)... 1.3 1-Hydroxyethylidene-1,1-diphosphonic acid (HEDP)... 0.9 Hexamethylenediaminetetra (methylenephosphonic acid), hexapotassium salt (K 6 HDTMP)... 1.2 Diethylenetriaminepenta (methylenephosphonic acid) (DTPMP)... 1.45 Diethylenetriaminepenta (methylenephosphonic acid), pentasodium salt (Na 5 DTPMP)... 1.7 800-TEST KIT (837-8548) 410-472-4340 7/16
1 x 5202 Instruction 1 x 9198B Sample Tube, Graduated (25 ml) w/ cap & blue dot, plastic 1 x R-0619B-C Hardness Buffer, 2 oz w/ blue cap, DB 1 x R-0620B-I Hardness Indicator Powder, 10 g w/ blue dot 1 x R-0683-C Hardness Reagent, 2 oz, DB TOTAL HARDNESS (1 drop = 10 ppm) 5. Multiply drops of R-0683 Hardness Reagent by 10. Record as parts per million (ppm) total hardness as calcium carbonate. NOTE: For 14.6 ml sample, record drops as grains per gallon (gpg) total hardness as calcium carbonate. Instr. #5202 Total Hardness Test 1. Rinse and fill 25 ml sample tube (#9198B) to 25 ml mark with water to be tested (). NOTE: For results in grains per gallon (gpg), fill to 14.6 ml mark. 2. Add 5 drops R-0619B Hardness Buffer. Swirl to mix. 3. Add 1 dipper R-0620B Hardness Indicator Powder. Swirl until dissolved. Sample will turn red () if hardness is present. 4. Add R-0683 Hardness Reagent dropwise, swirling and counting after each drop, until color changes from red to blue (). 800-TEST KIT (837-8548) 410-472-4340 7/16
1 x 5203 Instruction 1 x 9198W Sample Tube, Graduated (25 ml) w/ cap & white dot, plastic 1 x R-0638W-C Phenolphthalein Indicator, 2 oz w/ white cap, DB 1 x R-0699-C Iodide Iodate Reagent, 2 oz, DB 1 x R-0725-I Acid Starch Indicator Powder, 10 g Sodium Sulfite Test NOTE: Sample must be cooled to less than 100ºF (38ºC) to prevent high test results. Sample must be protected from air contact while cooling to prevent low test results. 1. Collect water to be tested in a clean, preferably large-mouthed, bottle to overflowing. Immediately cap and cool to room temperature. SODIUM SULFITE (1 drop = 10 ppm) 3. Add 1 drop R-0638W Phenolphthalein Indicator. Swirl to mix. Sample will turn pink (). 4. Add R-0725 Acid Starch Indicator Powder a dipper at a time, swirling after each dipper, until color changes from pink to colorless. Add 2 more dippers. Swirl until dissolved. 5. Add R-0699 Iodide Iodate Reagent dropwise, swirling and counting after each drop, until sample changes from colorless to a faint but permanent blue (). 6. Multiply drops of R-0699 Iodide Iodate Reagent by 10. Record as parts per million (ppm) sodium sulfite. NOTE: For 14.6 ml sample, record drops as grains per gallon (gpg) sodium sulfite. NOTE: For results as sulfite, multiply sodium sulfite concentration by 0.64. Instr. #5203 2. Rinse and fill 25 ml sample tube (#9198W) to 25 ml mark with cooled (room temperature) water to be tested (). NOTE: For results in grains per gallon (gpg), fill to 14.6 ml mark. 800-TEST KIT (837-8548) 410-472-4340 9/16
1 x 5212C Instruction 1 x 9198O Sample Tube, Graduated (25 ml) w/ cap & orange dot, plastic 1 x R-0630-C Chromate Indicator, 2 oz, DB 1 x R-0638O-A Phenolphthalein Indicator,.75 oz w/ orange cap, DB 1 x R-0706-C Silver Nitrate Reagent, 2 oz, DB 1 x R-0736O-C Sulfuric Acid.6N, 2 oz w/ orange cap, DB Chloride Test NOTE: When sulfite content of sample water to be tested exceeds 10 ppm, the sulfite should be oxidized to prevent interference in test. A 25 ml sample is first adjusted to the appropriate ph, then 1 ml (or 25 drops) of R-0649 Hydrogen Peroxide Solution (sold separately) is added and thoroughly mixed. Continue with the rest of the procedure. CHLORIDE (1 drop = 10 ppm) 3. Add 5 drops R-0630 Chromate Indicator. Swirl to mix. Sample will turn yellow (). 4. Add R-0706 Silver Nitrate Reagent dropwise, swirling and counting after each drop, until color changes from yellow to a milky salmon (brick) red (). NOTE: Do not add enough R-0706 Silver Nitrate Reagent to give a brown color. First change from yellow to a milky salmon (brick) red is the endpoint. 5. Multiply drops of R-0706 Silver Nitrate Reagent by 10. Record as parts per million (ppm) chloride. Instr. #5212C 1. Rinse and fill 25 ml sample tube (#9198O) to 25 ml mark with water to be tested. 2. Add 2 drops R-0638O Phenolphthalein Indicator. If sample turns pink (), add R-0736O Sulfuric Acid.6N dropwise, swirling after each drop, until color changes from pink to colorless. If sample is colorless, proceed to Step 3. 800-TEST KIT (837-8548) 410-472-4340 9/16
1 x 5229C Instruction 1 x 9198G Sample Tube, Graduated (25 ml) w/ cap and green dot, plastic 1 x R-0638G-C Phenolphthalein Indicator, 2 oz w/ green cap, DB 1 x R-0645-C Total Alkalinity Indicator, 2 oz, DB 1 x R-0724-C Hydrochloric Acid.12N, 2 oz, DB P/T Alkalinity (HCI) Test 1. Rinse and fill 25 ml sample tube (#9198G) to 25 ml mark with water to be tested. P/T ALKALINITY (HCl) (1 drop = 10 ppm) 4. Add 5 drops R-0645 Total Alkalinity Indicator. Swirl to mix. Sample will turn green (). 5. Add R-0724 Hydrochloric Acid.12N dropwise, swirling and counting after each drop, until color changes from green to red (). Record total drops (Steps 3 & 5) as T reading. 6. Multiply P reading by 10. Record as parts per million (ppm) P alkalinity as calcium carbonate. Multiply T reading by 10. Record as ppm T alkalinity as calcium carbonate. NOTE: For 14.6 ml sample, record P reading as grains per gallon (gpg) P alkalinity as calcium carbonate. Record T reading as gpg T alkalinity as calcium carbonate. Instr. #5229C NOTE: For results in grains per gallon (gpg), fill to 14.6 ml mark. 2. Add 3 drops R-0638G Phenolphthalein Indicator. Swirl to mix. Sample will turn pink () if P alkalinity is present proceed to Step 3. If sample is colorless, proceed to Step 4. 3. Add R-0724 Hydrochloric Acid.12N dropwise, swirling and counting after each drop, until color just changes from pink to colorless. Record drops as P reading. 800-TEST KIT (837-8548) 410-472-4340 8/16
COLOR COMPARISON TEST SILICIA (5-50, 25-250, or 50-500 ppm) Instr. #5321 1 x 3267 Cap, Test Cell (5 ml), plastic 1 x 4005 Cylinder, Graduated (50 ml w/ 1.0 ml div), glass 1 x 4025 Test Cell, Calibrated (5 ml), plastic 1 x 4026 Dipper Spoon, 2 g, plastic, white 3 x 4030 Pipet, Calibrated (0.5 & 1.0 ml) w/ cap, plastic 1 x 5321 Instruction 1 x 6002 Brush, Test Cell 1 x 9198 Sample Tube, Graduated (25 ml) w/ cap, plastic 1 x 9257 Midget Comparator, Silica, Heterotrophy Blue, 5-50 ppm 1 x R-1305Q-II Silica Reagent #4, 50 g 1 x R-1305U-C Silica Reagent #3*, 2 oz 1 x R-1306T-C Silica Reagent #1**, 2 oz 1 x R-1306U-C Silica Reagent #2, 2 oz Silica Test For 5-50 ppm Silica 1. Rinse and fill 25 ml sample tube (#9198) to 25 ml mark with water to be tested. 2. Using a 1.0 ml pipet (#4030), add 1.0 ml R-1306T Silica Reagent #1. Swirl to mix. 3. Using a separate 1.0 ml pipet, add 1.0 ml R-1306U Silica Reagent #2. Swirl to mix. WAIT 5 MINUTES. 4. Using a separate 1.0 ml pipet, add 1.0 ml R-1305U Silica Reagent #3. Swirl to mix. 5. Using dipper spoon (#4026), add 1 level dipper R-1305Q Silica Reagent #4. Swirl until dissolved. WAIT 1 MINUTE. Transfer to 5 ml test cell (#4025) to 5 ml mark. 6. Wipe dry and place in comparator WITH FROSTED SIDE FACING OPERATOR. 7. Match color in test cell with a color standard. Record as parts per million (ppm) silica. For 5-250 ppm Silica 1. Rinse and fill 50 ml graduated cylinder (#4005) to 10 ml mark with water to be tested. 2. Dilute to 50 ml mark with distilled, deionized, or silica-free water. Pour back and forth into 25 ml sample tube (#9198) to mix. Transfer to 25 ml sample tube to 25 ml mark. 3. Using a 1.0 ml pipet (#4030), add 1.0 ml R-1306T Silica Reagent #1. Swirl to mix. 4. Using a separate 1.0 ml pipet, add 1.0 ml R-1306U Silica Reagent #2. Swirl to mix. WAIT 5 MINUTES. 5. Using a separate 1.0 ml pipet, add 1.0 ml R-1305U Silica Reagent #3. Swirl to mix. 6. Using dipper spoon (#4026), add 1 level dipper R-1305Q Silica Reagent #4. Swirl until dissolved. WAIT 1 MINUTE. Transfer to 5 ml test cell (#4025) to 5 ml mark. (OVER)
7. Wipe dry and place in comparator WITH FROSTED SIDE FACING OPERATOR. 8. Match color in test cell with a color standard. Multiply reading by 5. Record as parts per million (ppm) silica. COLOR COMPARISON TEST SILICIA (5-50, 25-250, or 50-500 ppm) Instr. #5321 *WARNING: Silica Reagent #3 (R-1305U) contains 5 15% (w/w) oxalic acid, a poison. **WARNING: Silica Reagent #1 (R-1306T) contains 10 20% (w/w) hydrochloric acid, a corrosive acid. For 5-500 ppm Silica 1. Rinse and fill 50 ml graduated cylinder (#4005) to 5 ml mark with water to be tested. 2. Dilute to 50 ml mark with distilled, deionized, or silica-free water. Pour back and forth into 25 ml sample tube (#9198) to mix. Transfer to 25 ml sample tube to 25 ml mark. 3. Using a 1.0 ml pipet (#4030), add 1.0 ml R-1306T Silica Reagent #1. Swirl to mix. 4. Using a separate 1.0 ml pipet, add 1.0 ml R-1306U Silica Reagent #2. Swirl to mix. WAIT 5 MINUTES. 5. Using a separate 1.0 ml pipet, add 1.0 ml R-1305U Silica Reagent #3. Swirl to mix. 6. Using dipper spoon (#4026), add 1 level dipper R-1305Q Silica Reagent #4. Swirl until dissolved. WAIT 1 MINUTE. Transfer to 5 ml test cell (#4025) to 5 ml mark. 7. Wipe dry and place in comparator WITH FROSTED SIDE FACING OPERATOR. 8. Match color in test cell with a color standard. Multiply reading by 10. Record as parts per million (ppm) silica. 800-TEST KIT (837-8548) 410-472-4340 10/16
1 x 4029 Pipet, Calibrated (0.5 & 1.0 ml), plastic 2 x 4030 Pipet, Calibrated (0.5 & 1.0 ml) w/ cap, plastic 1 x 4078 Pipet, Graduated (3 ml w/ 0.5 ml div), plastic 1 x 5359 Instruction 3 x 9198 Sample Tube, Graduated (25 ml) w/ cap, plastic 1 x R-0890-C Molybdenum Buffer Solution, 2 oz 1 x R-0892-C Molybdenum Titrating Solution, 2 oz, DB 1 x R-0900-I Molybdenum Indicator Powder, 10 g 1 x R-0901-C Molybdenum Indicator Solvent, 2 oz Molybdenum Test Molybdenum Indicator Solution Preparation: For 1 drop = 2, 20, or 50 ppm Molybdenum Using a 1.0 ml pipet (#4030), add 2.5 ml R-0901 Molydenum Indicator Solvent to a clean 25 ml sample tube (#9198). Add 5 level dippers R-0900 Molybdenum Indicator Powder. Swirl until solution turns a clear, reddish-orange color. Undissolved crystals will remain in the solvent-powder mixture (). MOLYBDENUM (1 drop = 2, 5, 20 or 50 ppm) For 1 drop = 5 ppm Molybdenum Using a 1.0 ml pipet (#4030), add 1.5 ml R-0901 Molydenum Indicator Solvent to a clean 25 ml sample tube (#9198). Add 3 level dippers R-0900 Molybdenum Indicator Powder. Swirl until solution turns a clear, reddish-orange color. Undissovled crystals will remain in the solvent-powder mixture (). For 1 drop = 2 ppm Molybdenum 1. Rinse and fill a clean 25 ml sample tube (#9198) to 25 ml mark with distilled, deionized, or molybdenum-free tap water. This will be the blank. 2. Rinse and fill a second clean 25 ml sample tube to 25 ml mark with water to be tested (). 3. Using a 1.0 ml pipet (#4030), add 1.0 ml R-0890 Molybdenum Buffer Solution to each 25 ml sample tube. Swirl to mix. 4. Using a separate 1.0 ml pipet (#4029), add 1.0 ml Molybdenum Indicator Solution (prepared above) to each sample tube, transferring as few undissolved crystals as possible. However, a few crystals that may be transferred will not affect results. Swirl to mix. The blank will turn peach () and the sample will turn reddish orange to red (Fig. 4) if molybdenum is present. 5. Add R-0892 Molybdenum Titrating Solution, dropwise, swirling and counting after each drop, to sample tube containing water sample, until sample color matches blank color, or until no further change in color occurs. 6. Multiply drops of R-0892 Molybdenum Titrating Solution by 2. Record as parts per million (ppm) molybdenum. NOTE: To convert molybdenum (Mo) readings to molybdate (MoO 4 ), multiply Mo readings by 1.7; to convert to sodium molybdate dihydrate (Na 2 MoO 4 2H 2 O), multiply by 2.52. Instr. #5359 (OVER)
MOLYBDENUM (1 drop = 2, 5, 20 or 50 ppm) Instr. #5359 For 1 drop = 5 ppm Mo 1. Rinse and fill a clean 25 ml sample tube (#9198) to 10 ml mark with distilled, deionized, or molybdenum-free tap water. This will be the blank. 2. Rinse and fill a second clean 25 ml sample tube to 10 ml mark with water to be tested (). 3. Using a 1.0 ml pipet (#4030), add 0.5 ml R-0890 Molybdenum Buffer Solution to each 25 ml sample tube. Swirl to mix. 4. Using a separate 1.0 ml pipet (#4029), add 0.5 ml Molybdenum Indicator Solution (prepared above) to each sample tube, transferring as few undissolved crystals as possible. However, a few crystals that may be transferred will not affect results. Swirl to mix. The blank will turn peach () and the sample will turn reddish orange to red (Fig. 4) if molybdenum is present. 5. Add R-0892 Molybdenum Titrating Solution, dropwise, swirling and counting after each drop, to sample tube containing water sample until sample color matches blank color or until no further change in color occurs. 6. Multiply drops of R-0892 Molybdenum Titrating Solution by 5. Record as parts per million (ppm) molybdenum. NOTE: To convert molybdenum (Mo) readings to molybdate (MoO 4 ), multiply Mo readings by 1.7; to convert to sodium molybdate dihydrate (Na 2 MoO 4 2H 2 O), multiply by 2.52. For 1 drop = 20 or 50 ppm Mo 1. Rinse and fill a clean 25 ml sample tube (#9198) to 25 ml mark with distilled, deionized, or molybdenum-free tap water. This will be the blank. 2. Using a 3 ml pipet (#4078), place water to be tested in a second clean 25 ml sample tube. NOTE: For 1 drop = 20 ppm, fill pipet to 2.5 ml mark. For 1 drop = 50 ppm, fill pipet to 1.0 ml mark. 3. Dilute to 25 ml mark with distilled, deionized, or molybdenum-free tap water (). 4. Using a 1.0 ml pipet (#4030), add 1.0 ml R-0890 Molybdenum Buffer Solution to each 25 ml sample tube. Swirl to mix. 5. Using a separate 1.0 ml pipet (#4029), add 1.0 ml Molybdenum Indicator Solution (prepared above) to each sample tube, transferring as few undissolved crystals as possible. However, a few crystals that may be transferred will not affect results. Swirl to mix. The blank will turn peach () and the sample will turn reddish orange to red (Fig. 4) if molybdenum is present. 6. Add R-0892 Molybdenum Titrating Solution dropwise, swirling and counting after each drop, to sample tube containing water sample until sample color matches blank color or until no further change in color occurs. 7. For 2.5 ml sample, multiply drops of R-0892 Molybdenum Titrating Solution by 20. Record as parts per million (ppm) molybdenum. For 1.0 ml sample, multiply drops of R-0892 Molybdenum Titrating Solution by 50. Record as ppm molybdenum. NOTE: To convert molybdenum (Mo) readings to molybdate (MoO 4 ), multiply Mo readings by 1.7; to convert to sodium molybdate dihydrate (Na 2 MoO 4 2H 2 O), multiply by 2.52. Fig. 4 800-TEST KIT (837-8548) 410-472-4340 8/16