TV 2 DANMARK A/S Rugaardsvej 25 DK-5100 Odense C Eurofins Product Testing Smedeskovvej 38 DK-8464 Galten Denmark Tel. +45 70 22 42 76 Fax +45 70 22 42 75 ProductTesting-GA @eurofins.dk www.eurofins.dk Analytical report Sample material Sample identification 1 Receipt of samples September 5, 2017 Analytical period September 5 September 28, 2017 Date September 28 th, 2017 Your ref. 1 Our ref. 392-2017-00303801/BJ1 Task The sample was tested for typical textile parameters. Furthermore the samples was microbiological tested for total aerobic microbial count as well as coliform bacteria Picture of sample Results Please see enclosure with detailed test results. Conclusion The sample passed all the tests conducted. The sample did not have high microbiological values and coliform bacteria were not detected. Eurofins Product Testing A/S Brian Jensen MSc. Chemistry The test results relate only to the items tested. The report shall not be reproduced except in full without the written approval of the testing laboratory. \\DK02FIVA\SAGER\2017\392\00303801\06-REPORTS\FORSIDE.DOC Page 1 of 1
Page : 1 of 10 TEST REPORT APPLICANT ADDRESS : EUROFINS PRODUCT TESTING A/S : C/ Smedeskovvej 38 8464 -Galten CUSTOMER REFERENCE : SAMPLE 00303801 SAMPLE DESCRIPTION : Jeans SAMPLE RECEIVE DATE : 08/09/2017 TEST START DATE : 11/09/2017 TEST ENDING DATE : 28/09/2017 The following test item(s) was/were performed on selected sample(s) and/or component(s) appointed by applicant. TEST REQUESTED TEST METHOD / REGULATION RESULT Determination of Organotin compounds (TBT/TPhT, DBT/DOT) Determination of certain aromatic amines derived from azo colorants ISO/TS 16179 :2012 EN 14362-1:2012 See results See results Determination of formaldehyde ISO 14184-1:2012 See results Nickel release EN 1811- EN 12472 See results Determination of Toxylated Alkylphenols ISO 18254-1:2016 See results Determination of Pentaclorophenol UNE 59510:2007 See results ************ FOR FURTHER DETAILS, PLEASE REFER TO THE FOLLOWING PAGE(S) ************* Signed for and on behalf of Eurofins Textile Testing Spain Enrique Rivas Graciá General Manager
Page : 2 of 10 Results obtained refer only to samples, products or material received in Laboratory, as described in point related to sample description, and tested in conditions shown in present report. ensures that this job has been performed according to our Quality System and complying contract and legal conditions. Test uncertainties not reported are at customer disposal. If you happen to have any comments, please do it by sending email to textile_spain@eurofins.com and referring to this report number. Reproduction of this document is only valid if it is done completely and under the written permission of. SAMPLE PICTURES ***TO BE CONTINUED***
Page : 3 of 10 COMPONENT LIST Component No. Description Related Sample(s) 1 Main fabric 00303801 2 Metallic Button 00303801 3 Zipper fabric 00303801 ***TO BE CONTINUED***
Page : 4 of 10 TEST RESULTS Organotin compounds Content ISO/TS 16179:2012 Testing Date : 13/09/2017 Procedure used : Standard Test temperature : 25 ºC Component nº1 REACH requirement RESULT DBT (mg/kg) (0.1 %) DOT (mg/kg) (0.1 %) TPhT (mg/kg) (0.1 %) TBT (mg/kg) Note Not detected < MDL Method detection Limit = 10 mg/kg
Page : 5 of 10 Determination of certain aromatic amines derived from azo colorants EN 14362-1:2012 Remark: This standard is cancelled and suppressed. Testing Date : 11/09/2017 Detection and quantification method : GC/MS Component nº1 4-aminobiphenyl (mg/kg) Benzidine (mg/kg) 4-chlorotoluidine (mg/kg) 2-naphthylamine (mg/kg) o-aminoazotoluene (mg/kg) 2-amino-4-nitrotoluene (mg/kg) p-chloroaniline (mg/kg) 2,4-diaminoanisole (mg/kg) 4,4-diaminodiphenylmethane (mg/kg) 3,3-dichlorobenzidine (mg/kg) 3,3-dimethoxybenzidine (mg/kg) 3,3-dimethylbenzidine (mg/kg) 4,4-diamino-3,3-dimethyl diphenylmethane (mg/kg) p-cresidine (mg/kg) 4,4-methylene-bis-2-chloroaniline (mg/kg) 4-aminophenylether (mg/kg) 4,4-thioaniline (mg/kg) o-toluidine (mg/kg) 2,4-diaminotoluidine (mg/kg) 2,4,5-trimethylaniline (mg/kg) o-anisidine (mg/kg) Aniline (mg/kg) 1,4-phenylenediamine (mg/kg) 4-aminoazobenzene (mg/kg) RESULT Note = Not detected < MDL MDL Method detection Limit = 5 mg/kg REACH requirement : 30 mg/kg
Page : 6 of 10 Determination of certain aromatic amines derived from azo colorants EN 14362-1:2012 Remark: This standard is cancelled and suppressed. Testing Date : 11/09/2017 Detection and quantification method : GC/MS Component nº3 4-aminobiphenyl (mg/kg) Benzidine (mg/kg) 4-chlorotoluidine (mg/kg) 2-naphthylamine (mg/kg) o-aminoazotoluene (mg/kg) 2-amino-4-nitrotoluene (mg/kg) p-chloroaniline (mg/kg) 2,4-diaminoanisole (mg/kg) 4,4-diaminodiphenylmethane (mg/kg) 3,3-dichlorobenzidine (mg/kg) 3,3-dimethoxybenzidine (mg/kg) 3,3-dimethylbenzidine (mg/kg) 4,4-diamino-3,3-dimethyl diphenylmethane (mg/kg) p-cresidine (mg/kg) 4,4-methylene-bis-2-chloroaniline (mg/kg) 4-aminophenylether (mg/kg) 4,4-thioaniline (mg/kg) o-toluidine (mg/kg) 2,4-diaminotoluidine (mg/kg) 2,4,5-trimethylaniline (mg/kg) o-anisidine (mg/kg) Aniline (mg/kg) 1,4-phenylenediamine (mg/kg) 4-aminoazobenzene (mg/kg) RESULT Note = Not detected < MDL MDL Method detection Limit = 5 mg/kg REACH requirement : 30 mg/kg
Page : 7 of 10 Formaldehyde Content ISO 14184-1:2011 Testing Date : 11/09/2017 Sample weight : Sample 1 = 0.9926 g Sample 2 = 1.0071 g. Application range of calibration plot : 16-600 mg/kg Component nº1 RESULT Formaldehyde (mg/kg) Sample 1 Formaldehyde (mg/kg) Sample 2 Average Note Not detected < MDL Method detection Limit = 16 mg/kg
Page : 8 of 10 Ethoxylated Alkylphenols Content ISO 18254-1:2016 Testing Date : 11/09/2017 Determination and quantification method : LC-MS/MS Component nº1 RESULT NP (mg/kg) Sum NPEOn (mg/kg) Note Not detected < MDL Method detection Limit NP = 10 mg/kg Method detection Limit NPEOn: 10 mg/kg REACH requirement NP: 1000 mg/kg NPEOn: 100 mg/kg
Page : 9 of 10 Pentaclorophenols Content UNE 59510:2007 Testing Date : 13/09/2017 Component nº1 PCP (mg/kg) Note Not detected < MDL Method detection Limit = 0.02 mg/kg REACH requirement : 5 mg/kg RESULT
Page : 10 of 10 Nickel Content UNE-EN 1811:2011 Testing Date: 13/09/2017 Procedure used : ICP-MS Digestion method : Microwave digestion Component nº2 Nickel (ug/cm2/week) RESULT Limit PASS No clear decision FAIL 0,5 ug/cm2/week < 0,28 > 0,28 and <0,88 > 0,88 Test Notes: Report Unit: ug/cm2/week n.d= not detected (<MDL) MDL (Method Detection Limit)= 0.05 μg/cm2/week ** END OF TEST REPORT **
CERTIFICATE OF ANALYSIS TEST Reg.nr.222 Eurofins Product Testing A/S Smedeskovvej 38 8464 Galten Att: Product Testing Resultater Received on 08-09-2017 Report code AR-17-DH-189247-01 Analysis start 08-09-2017 EOL batch Analysis completed 12-09-2017 Batch code EUDKHL-00840963 Date Printed 12-09-2017 Sample code 588-2017-00321481 Sample description 392-2017-003038011 Sample marking 392-2017-00303801 Test Parameter Result Unit U(%) Est. value UM8VU UMH19 AOAC 991.14. / E-Cultural technique (media film) Coliforms < 1 cfu/g Escherichia coli < 1 cfu/g NMKL 86 / E-Cultural technique (non-chromogenic media) Aerobic Plate Count 30 C 580 cfu/g <L.Q. / <LOQ <L.D. / <LOD :Below limit of quantification :Below limit of detection ND / N.D. x.dupl :Not detected :x determination < :Less than/below > :Greater than/above Analytical Service Manager Jytte Warming Eurofins Steins Laboratorium A/S T +45 70 22 42 86 Ladelundvej 85 DK-6600 Vejen DENMARK Any query regarding this certificate of analysis shall be adressed to Eurofins Steins Customer Service + 45 7022 4286 or e-mail food@eurofins.dk. Results relate only to the item tested. Results are stated content in the sample, unless otherwise indicated. U(%): Expanded uncertainty of measurement (coverage factor k=2) Results shall not be reproduced except in full without written permission from Eurofins Steins. For all tests Eurofins Steins General Terms and Conditions of Sale applies; full text on www.eurofins.dk AR1 V: 3.6 F +45 70 22 42 95 www.eurofins.dk food@eurofins.dk Vat nr: DK87373010 AR-17-DH-189247-01 1 / 1