Technical Specifications for RICE- Brokens 5 % for Syria Commodity code: CERRIC011 Version: V14.1 Date of issue: 11 November 2014 Developed: Van Hoan NGUYEN, OSPFQ- WFP Reviewed: Van Hoan NGUYEN, OSPFQ- WFP Approved: Shane PRIGGE, OSPFQ- WFP 1. SCOPE This specification is applied for milled white Rice Brokens 5% that WFP purchases and distributes to beneficiaries in Syria. 2. DEFINITION Rice: is the whole kernels obtained from the species of rice (ORZYA, SATIVA) Paddy: means rice that is not yet dehusked. Husked rice: (Brown Rice or Cargo Rice): is rice from which the external husks have been removed through the process of husking, handling and boiling, which may result in partial loss of the bran, and is known as Cargo Rice. White rice (full husking): is husked rice from which the bran layers and germ have been removed through a process of threshing, and is classified according to its degree of whiteness into the following: - Partially white rice: is rice from which the external husk, some of the layers of the internal husk and most of the bran have been removed, and its kernels are tainted with a brown colour. - Fully white rice: is rice resulting after the removal of the external husk, layers of the internal husk and most of the bran. Extraneous matters: are the organic and in-organic components other than rice, and they include: - Extraneous Organic Matters: such as foreign (objectionable) seeds, husks, dietary fiber, fragments of straw and paddy rice etc. - In-organic Extraneous Matters: such as stones, sand, soil, metal and all other impurities. Part of rice kernels: means each part of the whole kernel that is divided lengthwise in to 10 equal parts. Damaged kernels: are whole kernels showing obvious deterioration due to moisture, temperature, insects, diseases or other factors such as rotten rice. 1 / 4
Yellow kernels (Heat damaged kernels): are whole kernels which have been affected by an increase of moisture and temperature, causing the colour to change from its natural state to yellow, and these kernels are considered among the damaged kernels percentage. Red kernels: are whole kernels whose natural colour is red provided that the red colour covers more than 1/4 of the surface of the kernel, or in which there are red streaks. Immature kernels: are safe whole kernels whose size is less than that of normal kernels (non-ripe) or whole kernels with a greenish colour. Chalky kernels: are safe whole kernels with half or more of its surface being an opaque white, and whose appearance is chalky with the exception of glutinous rice. Broken rice: is a part of the kernel the size of which is less than 3/4 of the normal safe kernel. Dead insect calculation: When calculating the ratio of dead insects, more than half of an insect or every two main parts of the insect (for example the head and chest), is considered to be one dead insect. Well milled is the removal of bran entirely to the extent that the rice kernel has a beautiful appearance. 3. REFERENCE Codex standard for rice CODEX STAN 198-1995 Syria standard for rice, S.N.S 319/1995 Thai Rice Standards, 1997 Vietnam White Rice Standards, TCVN 5644:2008 and TCVN 5643:1999 4. SPECIFICATION 4.1 General requirements Rice shall be fresh, free from abnormal flavours, odours and live insects. 4.2 Specific requirements Rice must also comply with other requirements specified in table 1. 4.3 Contaminants 4.3.1 Heavy metals The products covered by the provisions of this standard shall be free from heavy metals in amounts which may represent a hazard to human health. 4.3.2 Pesticide residues Rice shall comply with those maximum residue limits established by the Codex Alimentarius Commission for this commodity. 4.3.3 Mycotoxins Rice must not contain more than 5.0 ppb Ochratoxin A. 4.4 Hygiene 4.4.1 It is recommended that the product covered by the provisions of this standard be prepared and handled in accordance with the appropriate sections of the Recommended International Code of Practice General Principles of Food Hygiene 2 / 4
(CAC/RCP 1-1969), and other Codes of Practice recommended by the Codex Alimentarius Commission which are relevant to this product. 4.4.2 To the extent possible in good manufacturing practice, the product shall be free from objectionable matter. 4.4.3 When tested by appropriate methods of sampling and examination, the product: shall be free from micro-organisms in amounts which may represent a hazard to health; shall be free from parasites which may represent a hazard to health; and shall not contain any substance originating from micro-organisms, including fungi, in amounts which may represent a hazard to health. 5. PACKAGING AND MARKING The below requirements are only applied for purchases of Rice packed in bags. 5.1 Packaging Bags for Rice must comply with below requirements: - Bags is made of woven polypropylene (PP) are to be given special food grade ultraviolet treatment. - Bags have a heat cut mouth to prevent fibrillation and have sewn single folder bottom. - Bags must be closed by double stitching with suitable thread. - Bags must be clean, sound and free from insect, fungal infestation. - Bags must be new, uniform, strong, fit for export and multiple handing. - Construction of fabric must be solid to sustain harsh handling. - The bags of finished product must pass the drop test (after each drop, there shall be no rupture or loss of contents) following the principles of the drop test standard (EN 277, ISO 7965-2 or equivalent) with following sequence: + Butt dropping: Bag is dropped from a height of 1.20m on the bottom and the top of the bag. + Flat dropping: Bag is dropped from a height of 1.60m twice on one flat face and twice on the opposite flat face. Two percent marked bags (included in the price) must be sent with the lot. 5.2 Marking Below information must be printed on the bags: - Name of the product - Net weight - Name of supplier - Additional marking as per contractual agreement 6. ANALYTICAL REQUIREMENTS The principal tests in table 1 must be performed in order to check if the quality of the Rice meets above requirements. Additional analyses shall be defined in case of further quality assessment is required. 3 / 4
Table 1: List of compulsory tests and reference method No Tests Requirements Reference method (or equivalent) 1 Moisture Max. 14.0 % ISO 7301 2 Protein content Min 7.0 % ISO 7301 3 Ash content (total ash) Max. 0.5 % ISO 7301 4 Damaged and yellow kernels Max. 0.45 % ISO 7301 5 Rotten kernels Max. 0.5 % ISO 7301 6 Unripe and red kernels Max. 2.0 % ISO 7301 7 Chalky kernels Max. 3.0 % ISO 7301 8 Broken kernels Max. 5.0 % ISO 7301 9 Paddy kernels Max. 0.01 % ISO 7301 10 Extraneous matter Max. 0.15 % ISO 7301 11 Dead insect (in part or whole) Max. 30 per 100kg ISO 7301 12 Live insect Nil ISO 7301 13 Arsenic (inorganic) Max.0.2 ppm AOAC 986.15 14 Cadmium Max.0.4 ppm AOAC 999.10 15 Pesticide residues Showed at: http://www.codexalimentarius.n EU 15662 et/pestres/ data/commodities/details.html?i d=158 16 Phoxim 0.01 mg/kg 17 Methyl bromide 0.01 mg/kg 18 Ochratoxin A Max. 5.0 ppb AOAC 2000.3 19 Milling degree Well milled ISO 7301 20 Organoleptic quality Natural odour, colour, bright appearance Visual inspection 21 Average kernel length (only if required) As per contractual agreement 4 / 4
Technical Specifications for BULGUR WHEAT Specification reference: Bulgur Wheat grain Version: V13.0 Date of issue: 20 September 2013 Developed: Van Hoan NGUYEN, OSPFQ- WFP Reviewed: Shane PRIGGE, OSPFQ- WFP Approved: Shane PRIGGE, OSPFQ- WFP 1. SCOPE This specification applies to Bulgur wheat purchased by WFP. 2. DEFINITIONS Impurities: all other material than processed wheat kernels which includes but not only, wheat kernels, other plan seeds, dirt, others). Purity includes only bulgur wheat and excludes all other material. Ungelatinized kernels: Kernels with its cross section are semi-transparent and show spots of starchy appearance (inside section is in white color and not well cooked). Scorched Kernels: Kernels exposed to excessive processing conditions that lead to colour modification and loss in nutritional value. Kernels which are red and crimson colored (except brown bulgur wheat). Brown bulgur wheat: Bulgur obtained from red bread wheat. 3. REFERENCE Bulgur wheat shall comply, in terms of raw materials, composition or manufacture, except when specified otherwise in the contract, with the following the recommended International Code of Practice: General Principles of Food Hygiene CAC/RCP 1-1969 Rev 4-2003 including Annex Hazard Analysis and Critical Control Point (HACCP) System and Guidelines for its application. 4. RAW MATERIALS Bulgur wheat shall be manufactured from fresh wheat of good quality, free from foreign materials, substances hazardous to health, excessive moisture, insect damage and fungal contamination and shall comply with all relevant national food laws and standards. Wheat shall conform to Codex STAN 152-1985 and if required by the contract, be obtained from non-genetically modified varieties. 5. PROCESSING Bulgur wheat is obtained by cleaning, cooking, drying and cracked by removing the husk of wheat grains. 1 / 4
For compliance with Codex standards the processor must be able to demonstrate by principle and practice the adoption, implementation and recording of: Good Manufacturing Practice Hazard Analysis Critical Control Point program In this context an appointed WFP Inspector / Quality Surveyor is entitled to visit the factory without prior notice during any period when WFP product is being manufactured to check that the GMP and HACCP systems are in place. The Inspector / Quality Surveyor may request to see: Records (i.e. names of people in charge of the process and quality control, temperatures of the process, cleaning schedules, etc). Procedures (e.g. cleaning, personnel hygiene, HACCP, sampling and analysis). Instructions (e.g. process instructions, cleaning instructions). The quality manual for the process or factory. The manufacturer must be registered under national food law as a processor of foods for human consumption. 6. PRODUCT SPECIFICATION 6.1 General requirements Moisture: 13.0 % max. (by weight) Organoleptic: Natural smell, taste and color Kernel Size: - Over 2.5mm: 1.0% max. (by weight) - Between 1.5mm-2.5mm: 98.5% max. (by weight) - Under 1.5mm: 0.5% max. (by weight) Purity: 99.9% min. (by weight) Impurities: 0.1% max. (by weight) Scorched kernel (whole, or parts): 0.2% max. (by weight) Ungelatinized kernels: 1.0% max. (by weight) Total ash: 1.75% max. (by weight, on dry basis) Ash insoluble in acid: 0.3% max. (by weight, on dry basis) Protein: 9.3% min. (by weight, on dry basis) Crude fibres: 2.3% max. (by weight, on dry basis) 6.2 Microbiology Bulgur wheat shall not exceed the following levels of microbiological contamination: Table 1: Limit of microorganisms in Bulgur wheat Microorganisms Mesophyllic aerobic bacteria Coliforms Salmonella Escherichia Coli Staphylococcus aureus Bacillus cereus Yeasts and moulds Maximum levels 10,000 cfu per g 100 cfu per g 0 cfu per 25g <10 cfu per g <10 cfu per g 50 cfu per g 1,000 cfu per g 2 / 4
6.3 Contaminants Bulgur wheat shall be free from objectionable matter; not contain any substances originating from micro-organisms or any other poisonous or deleterious substances such as anti-nutritional factors, heavy metals or pesticide residues, in amounts which may represent a hazard to health. Permitted level of total aflatoxin: 20 ppb (B1, B2, G1, G2). Heavy metals: below levels specified in Codex Stan 193-1995, in particular Pb max 20 ppb and Cd max 100 ppb. 6.4 Fit for human consumption guarantee Suppliers shall have to check the quality of their products and guarantee that they are fit for human consumption. 7. PACKAGING AND MARKING As per contractual agreement. 8. STORING Bulgur wheat must be stored under dry, ventilated and hygienic conditions. 9. SAMPLING REQUIREMENTS Representative samples can be drawn according to international sampling method standards at the bagging section or in the warehouse. 10. ANALYTICAL REQUIREMENTS The principal tests in table 2 must be performed in order to check if the quality of the Bulgur wheat meets above requirements. Additional analyses shall be defined in case of further quality assessment. 3 / 4
Table 2: List of compulsory tests and reference methods No Analyses/tests Limit Reference method (or equivalent) 1 Moisture 13.0 % max. (by weight) ISO 712: 2009 Organoleptic Natural smell, taste and color Organoleptic examination 2 Kernel Size 3 - Over 2.5mm 1.0% max. (by weight) 4 - Between 1.5mm- 2.5mm 98.5% max. (by weight) 5 - Under 1.5mm 0.5% max. (by weight) 6 Purity 99.9% min. (by weight) Visual examination 7 Impurities 0.1% max. (by weight) Visual examination Scorched kernel (whole, or 0.2% max. (by weight) 8 parts) Visual examination 9 Ungelatinized kernels 1.0% max. (by weight) Visual examination 1.75% max. (by weight, on Total ash 10 dry basis) ISO 2171:2007 0.3% max. (by weight, on Ash insoluble in acid 11 dry basis) ISO 5985:2002 9.3% min. (by weight, on dry Protein basis) AOAC 981.10 12 ISO 20483:2006 2.3% max. (by weight, on Crude fibres 13 dry basis) AOAC 962.09 14 Mesophyllic aerobic bacteria 10,000 cfu per g max. ICC No 125 15 Coliforms 100 cfu per g max. AACC 42-11 16 Salmonella 0 cfu per 25g max. AOAC 2005.03 17 Escherichia Coli <10 cfu per g max. AACC 42-25B 18 19 Yeasts and moulds 1,000 cfu per g max. ICC No 146 AACC 42-50 GMO (only if required) Negative (< 0.9% of GMO material) 4 / 4
Technical Specifications for WHOLE LENTIL Specification reference: Whole Lentil Version: V13.0 Date of issue: 27 February, 2013 Developed: Van Hoan NGUYEN, OSPFQ-WFP Reviewed: Shane PRIGGE, OSPFQ-WFP; Approved: Shane PRIGGE, OSPFQ-WFP 1. SCOPE This specification applies to Whole Lentil purchased by WFP. 2. DEFINITION Damaged lentils may be peeled, split, broken, sprouted, distinctly green, frost damaged, distinctly deteriorated or discoloured by weather or disease, insect damaged, heat damaged or otherwise damaged in a way which materially affects quality. Peeled, split and broken includes lentils which are otherwise sound but which are less than three-quarters of whole seeds or where less than one-half of the seed coat is intact. Lentils with cracked or clipped seed coats are considered sound when the cotyledons are firmly held together. Insect damaged are any lentil grains which has been damaged by insects or pests. Heated lentils are usually dark tan to black in appearance. If the sample contains lentils with tan-coloured cotyledons and a distinct heated odour, then the grading factors is heated. Frost damaged is normally indicated by a combination of wrinkling and close adherence of the seed coat to the cotelydon. The seed coat may be translucent in appearance, and the cotyledons are brittle in texture. Frost damage is included in the tolerance for Damage. Sprouted: Lentils are considered sprouted when the seed coat splits and the primary root emerges from between the cotyledons. Foreign material includes anything that is not a lentil or part of a lentil. Total foreign material includes inorganic material and all other foreign materials. 3. REFERENCE Codex Standard for certain pulses grains (Codex Stan 171-1989, rev. 1-1995). Canada Grain Commission: Official grain grading guide- Lentil (http://www.grainscanada.gc.ca). Turkish Standard for Lentil (TS 143). 4. PRODUCT SPECIFICATION 4.1 General requirements Moisture: Peeled, split and broken: 14.0% max 3.5 % max 1 / 4
Insect damaged: 1.0% max Total damage: 3.5% max Inorganic material: 0.2% max Total foreign material: 0.5% max Minimum Size: 3mm diameter Organoleptic: Clean and bright appearance, Natural smell Live insect: Nil Color: As per contractual agreement Whole Lentil shall not contain contaminants and toxins in amounts which may represent a hazard to human health. Specific limit of some contaminants and toxins is presented in table 1. Table 1: Limit of contaminants and toxins No Contaminant and toxin Limit Heavy metal 1 Arsenic (As) 0.10 ppm max. 2 Copper (Cu) 2.0 ppm max. 3 Lead (Pb) 0.10 ppm max. 4 Cadmium (Cd) 0.02 ppm max. 5 Mercury (Hg) 0.01 ppm max. Pesticide residues 6 Carbamate < 10 ppb 7 Organochlorine < 10 ppb 8 Organophosphorus < 10 ppb 9 Pyrethroid < 10 ppb Toxic or noxious seeds 10 Crotolaria (Crotolaria spp.) Free 11 Corn cockle (Agrostemma githago L.) Free 12 Castor bean (Ricinus communis L.) Free 13 Jimson weed (Datura spp.) Free Radiation 14 Radiation 10 Bq/Kg max. Mycotoxins 15 Aflatoxin (total B1+B2+G1+G2) 20 ppb max. 16 Fumosin 5 ppb max. 17 Zearalenone 100 ppb max. 18 Ochratoxin A 5 ppb max. 5. PACKAGING AND MARKING As per contractual agreement. 6. STORING Whole Lentil must be stored under dry, ventilated and hygienic conditions. 2 / 4
7. SAMPLING REQUIREMENTS Representative samples can be drawn according to international sampling method standards at the bagging section or in the warehouse. For packed units, sampling frequency and reference method are showed in table 2. One laboratory samples of about 3 kg is required by lot or sub-lot of 500MT maximum. For the bulk (static and flowing), the sampling must follow the rules described in paragraphs 5.2 of ISO 24333-2009. Table 2: Sampling rules Lot or sublot size (MT) 100 101-200 201-300 301-400 401-500 Number of increment 3 % of bags and minimum 50 bags (e.g. 60 increments for a lot of 100 MT, packed in 50 kg bag) 3 % of bags (e.g. 120 increments for a lot of 200 MT, packed in 50 kg bag) 3 % of bags (e.g. 180 increments for a lot of 300 MT, packed in 50 kg bag) 3 % of bags (e.g. 240 increments for a lot of 400 MT, packed in 50 kg bag) 3 % of bags (e.g. 300 increments for a lot of 500 MT, packed in 50 kg bag) Place of sampling Warehouse or during production Reference GAFTA 124-2 7. ANALYTICAL REQUIREMENTS The principal tests in table 3 must be performed in order to check if the quality of the Whole Lentil meets above requirements. Additional analyses shall be defined in case of further quality assessment. Table 3: List of compulsory tests and reference methods No Parameters Recommended level Reference methods (or equivalent) 1 Moisture 14.0% max ISO 712-2009 2 Peeled, split and broken 3.5 % max ISO 605 3 Insect damaged 1.0% max Visual inspection 4 Total damage 3.5% max Visual inspection 5 Inorganic material 0.2% max Visual inspection 6 Total foreign material 0.5% max Visual inspection 7 Minimum Size 3mm diameter ISO 605 8 Organoleptic Clean and bright appearance, Natural smell ISO 605 9 Live insect Nil Visual inspection 10 Color As per contractual agreement Visual inspection A guide for grading is presented in annex 1. 3 / 4
Annex 1: Guide for grading of lentil grain The grading shall be performed as follow: - Draw and weight a test portion (about 200g) - Separate the test portion into component groups - Weigh materials of the component groups - Express the amount of material groups in percentage (see guide in table 4) Table 4: Record sheet for grading of lentil grain Mass of the test portion (grams)- M.. gr Component Mass of component (grams) Result calculation (expressed in % by mass of the test portion) Peeled, split and broken a = a x 100 / M Insect damaged b = b x 100 / M Heated lentils Frost damage Sprouted Other damaged Total damage c = (a + b + c) x 100 / M Inorganic material d = d x 100 / M Other foreign materials i Total foreign material = (d + i) x 100 / M 4 / 4
Technical Specifications for Specification reference: Iodized Salt Version: 13.1 Date of issue: 26 March 2013 IODIZED SALT Developed: Van Hoan NGUYEN, OSPFQ-WFP Reviewed: Shane PRIGGE, OSPFQ-WFP Approved: Shane PRIGGE, OSPFQ-WFP 1. SCOPE This specification applies to Iodized Salt distributed by WFP. 2. RAW MATERIALS 2.1 Salt Salt used for Iodized Salt conforms to Codex Standard for Salt (CODEX STAN 150-1985, Rev. 1-1997). 2.2 Iodine Source Potassium iodate (KIO 3 ) added in salt shall be of food grade quality and conform to all applicable Codex standards. Iodized Salt producers should purchase potassium iodate from WFP approved premixes suppliers: BASF (Stern Vitamin), DSM, Fortitech, Nicholas Piramal, Hexagon Nutrition or their authorized dealers and GAIN premix facility. Addresses of premix suppliers are on http://foodquality.wfp.org 3. PROCESSING The production of salt shall only be performed by reliable manufacturers having the knowledge and the equipment requisite for the adequate production of food grade salt. For compliance with Codex standards the manufacturers must be able to demonstrate by principle and practice the adoption, implementation and recording of: - Good Manufacturing Practice - Hazard Analysis Critical Control Point program The manufacturer must be registered under national food law as a manufacturer of foods for human consumption. 1/3
4. PRODUCT SPECIFICATION 4.1 General requirements Iodized Salt is dried, sieved, edible and iodized for human consumption. Sodium chloride as NaCl: min 97.0 % (on dry matter) Moisture content: max 3.0% (m/m) Water insoluble matter: max 0.2 % (m/m) Iodine: 30.0 50.0 mg/kg (means 50 84mg of potassium iodate per kg of salt) Colour: shall be white and 10 g of salt in 100 ml water shall give a colourless solution having a neutral reaction. 4.2 Particle size distribution Regular salt - min 85 % pass through 1.00 mm sieve - max 20 % pass through 0.212 mm sieve Otherwise: particle size will be specified in the purchase contract. 4.3 Food additives Food additives listed in Tables 1 and 2 of the Codex General Standard for Food Additives (CODEX STAN 192-1995) in Food Category 12.1.1 (Salt) may be used in foods subject to this standard. All additives used shall be of food grade quality. 4.4 Chemical contaminants Contaminants in the Iodized Salt shall not exceed the following levels: Table 1: Limit of chemical contamination in Iodized Salt Item Alkalinity (as Na 2 CO 3 ) Acid insoluble matter Sulphate (as SO 4 ) Arsenic Copper Lead Cadmium Mercury Calcium Tin (as Sn) 2/3 Maximum limit 0.1 % (m/m) 0.15 % (m/m) 0.5 % (m/m) 0.5 mg/kg 2.0 mg/kg 2.0 mg/kg 0.5 mg/kg 0.1 mg/kg 0.5 % (m/m) 100.0 mg/kg Iodized Salt shall not contain other contaminants and toxins in amounts which may represent a hazard to health. 5. PACKAGING Iodised salt shall be packed in air tight bags of either high density polyethylene (HDPE) or polypropylene (PP) (laminated or non-laminated) or LDPE-lined jute bags (Grade 1803 DW jute bags lined with 150 gauge polyethylene sheet). Marking: as per contractual agreement.
6. STORING Iodized Salt must be stored under dry, ventilated and hygienic conditions. 7. ANALYTICAL REQUIREMENTS The principal tests in table 2 must be performed in order to check if the quality of Iodized Salt meets above requirements. Additional analyses shall be defined in case of further quality assessment. Table 2: List of test/analysis No Parameter Limit Analytical method (or equivalent) 1 Organoleptic - Normal smell - Colour: white - 10g of salt in 100ml water shall give a colourless solution having a neutral reaction 2 Particle size - min 85 % pass through 1.00 mm sieve - max 20 % pass through 0.212 mm sieve Or: as per specified in the purchase contract. 3 Sodium chloride (NaCl) Min 97.0 % (m/m, on dry matter) ISO 2481 4 Moisture content Max 3.0 % (m/m) ISO 2483:1973 5 Water insoluble matter Max 0.2 % (m/m) ISO 2479 6 Iodine 30.0 50.0 mg/kg ESPA/CN 109/84 7 Alkalinity (as Na 2 CO 3 ) Max 0.1 % (m/m) ISO 3196 8 Acid insoluble matter Max 0.15 % (m/m) ISO 2479 9 Sulphate (as SO 4 ) Max 0.5 % (m/m) ISO 2480 10 Arsenic (As) Max 0.5 mg/kg ECSS/SC 312-1982 11 Copper (Cu) Max 2.0 mg/kg ECSS/SC 144-1977 12 Lead (Pb) Max 2.0 mg/kg ECSS/SC 313-1982 13 Cadmium (Cd) Max 0.5 mg/kg ECSS/SC 314-1982 14 Mercury (Hg) Max 0.1 mg/kg ECSS/SC 312-1982 3/3
Specification reference: Tomato paste Version: 1.0 Date of issue: 26 th May 2011 Technical specification for: TOMATO PASTE 1. INTRODUCTION 1.1 Product type Tomato Paste is prepared from sound, ripe red tomatoes (Lycopersicon/Lycopersicum esculentum P. Mill) and packed in tin cans. 1.2 Standards and recommendations Tomato Paste shall be manufactured in accordance with: Recommended International Code of Practice: General Principles of Food Hygiene, CAC/RCP 1-1969 Rev 3 1997 Amended (1999) including Annex Hazard Analysis and Critical Control Point (HACCP) System and Guidelines for its application and Codex Standard for processed Tomato concentrates (Codex Stan 57-1981). 2. PROCESSING Tomato Paste production must respect the national and international code practice for processing of this commodity. For compliance with Codex standards, the processor must be able to demonstrate by principle and practice the adoption, implementation and recording of: Good Manufacturing Practice Hazard Analysis Critical Control Point program In this context an appointed WFP Inspector / Quality Surveyor is entitled to visit the factory without prior notice during any period when WFP product is being manufactured to check that the GMP and HACCP systems are in place. The Inspector / Quality Surveyor may request to see: Records (i.e. names of people in charge of the process and quality control, temperatures of the process, mixing times / quantity, cleaning schedules, etc). Procedures (e.g. cleaning, personnel hygiene, HACCP, sampling and analysis). Instructions (e.g. process instructions, cleaning instructions). The quality manual for the process or factory. The producer must be registered under national food law as a processor of foods for human consumption. In addition, the producer must have a legal authorization to produce this commodity in the country where the factory is located. 1 /4
3. PRODUCT SPECIFICATIONS 3.1. Main requirements Tomato Paste is manufactured according to a process that should confer to the finished product the following specifications: Organoleptic Concentration (Brix) Consistency by Bostwick (at 12 Brix, at 30 0 C) Colour (at 12 Brix) ph Acidity Sugar (at dry matter) Salt Normal/typical taste and odor. Absence of burnt taste, fermented taste and smell. 28% minimum 4-11 cm/30s 2 minimum Gardner Color Scale 4.5 maximum 7% maximum 42% minimum 2% maximum If required by recipient country, Tomato Paste needs to be obtained from non-genetically modified varieties. 3.2. Microbiology Microbiological contamination in the Tomato Paste shall not exceed the following levels: Total Coliform 10 cfu/g maximum Escherichia Coli Absent Salmonella Absent Staphylococcus aureus Absent Lysteria monocytogenes Absent Bacillus cereus 50 cfu per g maximum Howard mould count 60% maximum 3.3 Chemical Contaminants and Toxins It shall be free from objectionable matter; free from radioactivity; not contain any substances originating from micro-organisms or any other poisonous or deleterious substances such as anti-nutritional factors, heavy metals or pesticide residues, in amounts which may represent a hazard to health. Heavy metal content must be below levels specified in Codex Stan 193-1995, in particular: Mercury (Hg) Cadmium (Cd) Lead (Pb) Arsenic (As) Tin (Sn) 0.5ppm maximum 0.05ppm maximum 1.0ppm maximum 1.0ppm maximum 100ppm maximum 3.4 Shelf life It shall retain above qualities for at least two year from date of manufacture when stored dry at ambient temperatures prevalent in the country of destination. 2 /4
4. PACKAGING Tomato paste can be packaged into tin can to constitute the primary packaging. The secondary packaging is cartons to facilitate transportation and storage. 4.1. Tins The metal containers (tins) must be coated internally and externally with lacquers appropriate for the product. Specifications and guarantees for the material, lacquers and other treatments used shall be available. Likewise, the facility must obtain the acceptable ranges and limits for the double seam dimensions and other characteristics of the filled can specific to the can type, size and supplier. Together with fill standards required for the product, these specifications will be used to ensure the finished product is hermetically sealed during the seaming operation. 4.2. Cartons Cartons should be new, strong cardboard cartons containing tins, manufactured from wellconstructed paper. Slip sheets or plywood should be placed inside each container to provide the required stacking strength. Pallets with appropriate stacking configuration could also be used 5. MARKING 5.1. On tins The following information should be available on tins: Name of the product Net weight Name of manufacturing facility (including country of origin) Batch number (should be traceable to retort and seamer used for manufacturing) Production date (and shift, if there is more than one shift) Best before date / Expiry date Additional marking as per contractual agreement 5.2. On cartons The following information should be available on each carton: Name of the product Number of tins per carton Net weight Name and address of the supplier (including country of origin) Production date Expiry date Additional marking as per contractual agreement 6. STORING Tomato paste must be stored under cool, dry and hygienic conditions. 3 /4
7. ANALYTICAL REQUIREMENTS Table 1: List of compulsory tests and reference methods N o Specifications Recommended value Reference method* 1 Organoleptic Normal/typical taste and odor. Absence of burnt taste, fermented taste and smell. 2 Concentration (Brix) 28% minimum 3 4 Consistency by Bostwick (at 12 Brix, at 300C) Colour (at 12 Brix) 4-11 cm/30s 2 minimum Gardner Color Scale 5 ph 4.5 maximum AOAC 981. 6 Acidity 7% maximum 7 Sugar (at dry matter) 42% minimum 8 Salt 2% maximum ISO 3634:1979 9 Total Coliform 10 cfu/g maximum 10 Escherichia Coli Absent 11 Salmonella Absent 12 Staphylococcus aureus Absent 13 Lysteria monocytogenes Absent 14 Bacillus cereus 50 cfu per g maximum 15 Howard mould count 60% maximum AOAC 965.41 * or equivalent 4 /4
Technical Specifications of RATION Commodity code: PPFRTN000 Version: 15.0 Date of issue: 25 May 2015 Developed: Van Hoan NGUYEN Reviewed: Van Hoan NGUYEN, Charles JELENSPERGER, Shane PRIGGE Approved: Isabelle MBALLA 1. SCOPE This specification applied for Ration that WFP purchase and distribute to beneficiaries. As per contractual agreement, the Ration may include some or all of the commodities listed at table 1. The proportion of each commodity in the ration will be specified in the contract. Table 1: List of commodities of Ration No Commodity No Commodity 1 White Rice 5% 15 Canned Chicken Luncheon meat 2 Bulgur Wheat 16 Canned Mackerel 3 Split Lentil 17 Canned Tuna 4 Whole Lentil 18 Canned Sardines 5 Chickpeas 19 Canned Fava Beans 6 Beans 20 Canned Chickpeas 7 Fortified Wheat Flour 21 Cheddar cheese 8 Pasta (Macaroni, Spaghetti, Vermicelli) 22 Cream cheese 9 White Sugar 150 23 Black tea 10 Iodized Salt 24 Dates 11 Sunflower Oil 25 Jam 12 Palm oil 26 Coffee 13 Tomato Paste 27 Tahini 14 Canned Beef 28 Halva 2. GENERAL REQUIREMENTS Unless otherwise specified in the contracts, all commodities in the Ration must comply with the following guidelines or standards of Codex Alimentarius: 1 / 24
Recommended International Code of Practice: General Principles of Food Hygiene CAC/RCP 1-1969 Rev 4-2003 including Annex Hazard Analysis and Critical Control Point (HACCP) System and Guidelines for its application, of the Codex Alimentarius. General principles for addition of essential nutrients to foods: CAC/GL 09-1987 (amended 1989, 1991), of the Codex Alimentarius. General standard for the labelling of prepacked foods: CODEX STAN 1-1985, of the Codex Alimentarius. 3. PRODUCT SPECIFICATIONS Quality of all commodities in the Ration must meet WFP specifications (for certain commodities at the following link: http://foodqualityandsafety.wfp.org/specifications;jsessionid=38613b2681405f4a3938b1f98 E66ADB8) and local, international standards for these commodities. Specific requirements for packaging, marking and analytical requirements are showed at following paragraphs. 4. SHELF LIFE Shelf life of commodities shall be specified in the contract. 5. PACKAGING REQUIREMENT Primary packaging The products covered by the provisions of this specification must be packed in appropriate packaging which safeguard the hygienic, nutritional, technological, and organoleptic qualities of the product. Unless otherwise specified in the contracts, primary packaging must comply with general requirements showed in table 2. Table 2: General requirements for primary packaging Commodities Rice, Bulgur Wheat, Split lentil, Whole lentil, Chickpeas, Beans, Wheat flour 1, Pasta, Sugar, Salt Rice, Bulgur Wheat, Split lentil, Whole lentil, Net weight/ volume < 1kg bags 1 to 5 kg bags >5 to 25 kg bags 2 Packaging requirements Laminate 60PE/LDPE+12PETor equivalent. Bags must be well sealed in order to prevent leakage during transport Laminate 80PE/LDPE+12PETor equivalent. Bags must be well sealed in order to prevent leakage during transport New uniform strong polypropylene (PP) bag fit for export and multiple handing. Density: Min. 80 grams per square meter. 1 Or Wheat flour can be packed in same packaging for >5-25kg bags 2 Do not include in the secondary packaging. Two percent of spare printed bags as per marking requirements must be shipped along with the cargo and included in the price. 2 / 24
Chickpeas, Beans, Wheat flour Oil Tomato paste Canned fish Canned beef Canned beans, chickpeas 1.0 or 1.5 litres bottle 3 to 5 litres jerry cans (plastic) 0.2 to 0.5 kg can 0.5 to 1.0 kg can Bags made of woven PP are to be given special food grade ultraviolet treatment. Construction of fabric must be solid to sustain harsh handling. Bags shall be double stitched. Made of Polyethylene Terephtalate (PET). They shall be hermetically closed thanks to a safety device. PET bottles shall be suitable for foodstuff, clean and free from any abnormal odor. High Density Polyethylene (HDPE), with heat-sealed membranes and screw-top lids. They shall be made by blow-molding and be seamless so that they can not leak (except at the closure) unless ruptured. The containers must be suitable for foodstuffs, have stoppers fitted with safety devices and must be hermetically sealed. The containers shall have two flat walls, a built-in handle and a screw top. Specifications: - Material: HDPE - Color: white/translucent - Net weight: 200gm minimum for 5 litres empty jerry cans. - Rated capacity: 3.0 or 5.0 litres - Screw cap with inner plug Typical wall thickness: 1.0 mm (middle of side panels) The metal containers (tins) must be coated internally and externally with lacquers appropriate for the product. Specifications and guarantees for the material, lacquers and other treatments used shall be available. Likewise, the facility must obtain the acceptable ranges and limits for the double seam dimensions and other characteristics of the filled can specific to the can type, size and supplier. Together with fill standards required for the product, these specifications will be used to ensure the finished product is hermetically sealed during the seaming operation. Secondary packaging Unless otherwise specified in the contracts, except >5kg bags of Rice, Bulgur Wheat, Split lentil, Whole lentil, Chickpeas, Beans, all commodities of the Ration shall be packed in one carton box of strong, uniform, fit for storage and multiple handling. General requirements for carton box is showed in table 3. All weak, torn, dirty, used or unserviceable cartons to be rejected outright and shall be replaced at supplier s cost. Two percent of spare printed carton as per marking requirements must be shipped along with the cargo and included in the price. Table 3: Requirements for Carton Net weight Max. 20kg Packaging requirements New, strong cardboard cartons, manufactured from well-constructed double walled corrugated board (5 ply) with a specific weight of approximately 750 grams per square meter. - Cartons should have burst strength of approximately 61 pounds per inch or equivalent. - Carton seams should be glued, stapled. 3 / 24
5. MARKING Cartons shall be fully filled and stacked well for maximum strength. Slip sheets or plywood should be placed inside each container to provide the required stacking strength. Pallets with appropriate stacking configuration could also be used. Requirements for bags, cans and cartons shall be specified in the contract. 6. ANALYTICAL REQUIREMENTS The principal tests in table 4-30 must be performed in order to check if the quality of commodities in the Ration meets WFP requirements. Additional tests may be defined in case of further quality assessment is required. List of tests of commodities in the Ration would be updated and showed at: http://foodqualityandsafety.wfp.org/specifications;jsessionid=38613b2681405f4a3938b1f98 E66ADB8 Table 4: List of compulsory tests and reference method for RICE 5% (Version 14.1_For Syria) No Tests Requirements Reference method (or equivalent) 1 Moisture Max. 14.0 % ISO 7301 2 Protein content Min 7.0 % ISO 7301 3 Ash content (total ash) Max. 0.5 % ISO 7301 4 Damaged and yellow kernels Max. 0.45 % ISO 7301 5 Rotten kernels Max. 0.5 % ISO 7301 6 Unripe and red kernels Max. 2.0 % ISO 7301 7 Chalky kernels Max. 3.0 % ISO 7301 8 Broken kernels Max. 5.0 % ISO 7301 9 Paddy kernels Max. 0.01 % ISO 7301 10 Extraneous matter Max. 0.15 % ISO 7301 11 Dead insect (in part or Max. 30 per 100kg ISO 7301 whole) 12 Live insect Nil ISO 7301 13 Arsenic (inorganic) Max.0.2 ppm AOAC 986.15 14 Cadmium Max.0.4 ppm AOAC 999.10 15 Pesticide residues Showed at: http://www.codexalimentarius. EU 15662 net/pestres/ data/commodities/details.html?id=158 16 Phoxim 0.01 mg/kg 17 Methyl bromide 0.01 mg/kg 18 Ochratoxin A Max. 5.0 ppb AOAC 2000.3 19 Milling degree Well milled ISO 7301 20 Organoleptic quality Natural odour, colour, bright appearance Visual inspection 4 / 24
21 Average kernel length (only As per contractual if required) agreement Table 5: List of compulsory tests and reference method for BULGUR WHEAT (WFP spec reference: V13.0, 20 September 2013) No Tests Requirements Reference method (or equivalent) 1 Moisture 13.0 % max. (by weight) ISO 712: 2009 Natural smell, taste and Organoleptic Organoleptic 2 color examination Kernel Size 3 - Over 2.5mm 1.0% max. (by weight) 4 - Between 1.5mm- 2.5mm 98.5% max. (by weight) 5 - Under 1.5mm 0.5% max. (by weight) 6 Purity 99.9% min. (by weight) Visual examination 7 Impurities 0.1% max. (by weight) Visual examination Scorched kernel (whole, or 0.2% max. (by weight) 8 parts) Visual examination 9 Ungelatinized kernels 1.0% max. (by weight) Visual examination 1.75% max. (by weight, Total ash 10 on dry basis) ISO 2171:2007 0.3% max. (by weight, on Ash insoluble in acid 11 dry basis) ISO 5985:2002 12 Protein 9.3% min. (by weight, on dry basis) AOAC 981.10 ISO 20483:2006 2.3% max. (by weight, on Crude fibres 13 dry basis) AOAC 962.09 14 Mesophyllic aerobic bacteria 10,000 cfu per g max. ICC No 125 15 Coliforms 100 cfu per g max. AACC 42-11 16 Salmonella 0 cfu per 25g max. AOAC 2005.03 17 Escherichia Coli <10 cfu per g max. AACC 42-25B 18 19 Yeasts and moulds 1,000 cfu per g max. ICC No 146 AACC 42-50 GMO (only if required) Negative (< 0.9% of GMO material) 5 / 24
Table 6: List of compulsory tests and reference method for SPLIT LENTIL (WFP spec reference: V1.0, 27 March 2011) No Tests Requirements Reference method (or equivalent) 1 Moisture 12% max ICC No 110 ISO 712-2009 2 Total damage 2% max 3 Total foreign material 1% max 4 Unhusked grains 1% max 5 Broken 2% max 6 Discoloured 1% max 7 Cooking time 15 minutes (no soaking) 8 Organoleptic Clean and bright appearance, Natural smell 9 Live insect Nil Visual 10 Aflatoxin 20 ppb max ISO 16050 11 GMO (only if required) Negative Table 7: List of compulsory tests and reference methods for WHOLE LENTIL (WFP spec reference: V13.0, 27, February, 2013) No Parameters Recommended level Reference methods (or equivalent) 1 Moisture 14.0% max ISO 712-2009 2 Peeled, split and broken 3.5 % max ISO 605 3 Insect damaged 1.0% max Visual inspection 4 Total damage 3.5% max Visual inspection 5 Inorganic material 0.2% max Visual inspection 6 Total foreign material 0.5% max Visual inspection 7 Minimum Size 3mm diameter ISO 605 8 Organoleptic Clean and bright appearance, Natural smell ISO 605 9 Live insect Nil Visual inspection 10 Color As per contractual agreement Visual inspection 6 / 24
Table 8: List of compulsory tests and reference methods for CHICKPEAS No Parameters Recommended level 1 Moisture: 12 % max Reference methods (Or equivalent) ICC No 110 ISO 712-2009 2 Foreign matter 1 % max by weight ISO 2591-1 3 Size 8-9 mm, 90% min by weight ISO 2591-1 4 Undersize 3 % max by weight ISO 3310-2 5 Spoilt kernels 3 % max by weight ISO 3310-2 6 Broken 3 % max by weight ISO 3310-2 7 Mixing ratio 10% max by weight ISO 3310-2 8 Goat and unmatured 5% max by weight ISO 3310-2 9 Cooking time 60-90 minutes after 24 h soaking 10 Organoleptic Natural taste, smell and color 11 Live insect Nil Visual 12 Aflatoxin 20 ppb ISO 16050 13 GMO (Only if required) Table 9: List of compulsory tests and reference methods for BEANS No Requirements Maximum limits Reference method (or equivalent) 1 Foreign matter, % m/m 0.75 2 Inorganic matter, % m/m 0.2 3 Other edible grains, % m/m 0.2 4 Pest damaged grains, % m/m 2.0 5 Heat damaged grains, % m/m 0.2 6 Contrasting varieties, % m/m 1 ISO 605 7 Broken/split, % m/m 2.0 8 Discoloured, % m/m 1.0 9 Total defectives grains, % m/m 3.5 10 Filth, % m/m 0.1 11 Moisture, % m/m 14.0 ISO 24557 Total aflatoxin 12 (AFB1+AFB2+AFG1 +AFG2), ppb 10.0 ISO 16050 13 Live insect Nil 14 Cooking test 90 minutes for 12hrs soaking 15 Organoleptic quality 16 Colour and/or varieties Clean and bright appearance, Natural odour As per contractual agreement 7 / 24
Table 10: List of compulsory tests and reference method for FORTIFIED WHEAT FLOUR (WFP spec reference: V4.0, 23 May 2011) No Tests Requirements Reference method (or equivalent) 1 Organoleptic Pleasant smell; Typical taste and color 2 Moisture content 14 % maximum ICC No 110 ISO 711-2009 3 Ash 0.65% maximum of dry matter ICC No. 104 4 Protein 11 % minimum of dry matter ICC No. 105 5 Zeleny index 30 ml minimum ICC No 116 & 118 ISO 5529 6 Delayed Zeleny value + 5 ml minimum sedimentation 7 Hagberg Falling Number (HFN) 230 min. (incl. 60 sec preparation) ICC No 107 ISO 3093 8 Wet gluten 28 % minimum AACC 38-12A ICC No 155 ISO 21415-1 9 Gluten index 85 % minimum ICC 155 AACC 3812 Chopin Alveograph 10 W 215 minimum AACC 54-30A ISO 27971 11 P 80 minimum 12 L 80 minimum 13 Fatty acid maximum 120 mg KOH per 100 gram dry matter ISO 7305 AOAC 14022 14 Vitamin A 1.0 mg/kg AOAC 992.04 AACC 86-03 15 Iron 15.0 mg/kg AOAC 944.02 AACC 40-41B 8 / 24
Table 11: List of compulsory tests and reference method for PASTA (WFP spec reference: V14.0, 21 July 2014) (applicable for Macaroni, Spaghetti, Vermicelli) N o Tests Requirements Reference method (or equivalent) 1 It should be homogenous in colour and shape, free of spots. Free of off smell, moulds, foreign material and insects. Comply 2 Length As per contractual agreement 3 Diameter As per contractual agreement 4 Thickness As per contractual agreement 5 Cooking test The product holds its shape and texture after boiling it for 10 minutes. Organic, visual examination Measurement Measurement Measurement Cooking 6 Broken 3.0% max. by weight Visual examination 7 Moisture 13.0% max. by weight ISO 712 8 Protein 10.5-12.0% by weight AOAC 981.10 ISO 20483 9 Ash 0.9% max. by weight in ISO 2171 dry matter 10 Cellulose 0.5% max. by weight 11 Ash insoluble in acid of dry 0.15% max. by weight AOCS Ba 5b-68 matter 12 Soluble solids 8.0% max. by weight 13 Sodium and potassium salts 1.0% max. by weight 14 Acidity (mg KOH per 100g dry 4.0 max. ISO 7305 matter) 15 Arsenic (As) 1.0 mg/kg max. AOAC 986.15 16 Lead (Pb) 2.0 mg/kg max. AOAC 999.11 17 Mercury (Hg) 1.0 mg/kg max. AOAC 971.21 18 Total plate count 10,000 cfu/g max. ICC No 125 AACC 42-11 19 Salmonella (per 25g) 0 cfu/25g AACC 42-25B 20 Escherichia Coli 0 cfu/g AOAC 991.14 21 Staphylococcus aureus 0 cfu/g AACC 42-30B 22 Yeast & Moulds 200 cfu/g max. ICC No 146 AACC 42-50 23 GMO (only if required) Negative (< 0.9% of GMO material) 9 / 24
Table 12: List of compulsory tests and reference method for WHITE SUGAR 150 (WFP spec reference: V14.0, 20 February 2014) No Tests Requirements Reference method (or equivalent) 1 Taste Natural Sensorial examination 2 Smell Natural Sensorial examination 3 Colour of the solution 150 ICUMSA units max ICUMSA Method GS 2/3-10 (2011) 4 Moisture content 0.10% m/m max ICUMSA Method GS 2/1/3/9-15 (2007) 5 Conductivity ash 0.10% m/m max ICUMSA Method GS 2/3/9-17 (2011) 6 Polarization 99.5 Z min ICUMSA Method GS 1/2/3/9-1 (2011) 7 Invert sugar content 0.10% m/m max ICUMSA Method GS 2/3/9-5 (2011) 8 Coliforms 10 cfu/10g max ISO 4832 9 Salmonella Absent in 25 g ISO 6759 10 Yeast and Mould 20 cfu/10g max ICUMSA Method GS 2/3-47 (1998) 11 Sulphur dioxide (SO2) 70 mg/kg max ICUMSA Method GS 2/1/7/9-33 (2011) 12 Arsenic (As) 0.5 mg/kg max ICUMSA Method GS 2/3/9-25 (2007) 13 Lead (Pb) 0.5 mg/kg max ICUMSA Method GS 2/3-24 (1998) 14 Copper (Cu) 1.0 mg/kg max ICUMSA Method GS 9-9 (2013) 10 / 24
Table 13: List of compulsory tests and reference method for IODIZED SALT (WFP spec reference: V13.1, 26 March 2013) No Tests Requirements Reference method (or equivalent) 1 Organoleptic - Normal smell - Colour: white - 10g of salt in 100ml water shall give a colourless solution having a neutral reaction 2 Particle size - min 85 % pass through 1.00 mm sieve - max 20 % pass through 0.212 mm sieve Or: as per specified in the purchase contract. 3 Sodium chloride (NaCl) Min 97.0 % (m/m, on dry matter) ISO 2481 4 Moisture content Max 3.0 % (m/m) ISO 2483:1973 5 Water insoluble matter Max 0.2 % (m/m) ISO 2479 6 Iodine 30.0 50.0 mg/kg ESPA/CN 109/84 7 Alkalinity (as Na2CO3) Max 0.1 % (m/m) ISO 3196 8 Acid insoluble matter Max 0.15 % (m/m) ISO 2479 9 Sulphate (as SO4) Max 0.5 % (m/m) ISO 2480 10 Arsenic (As) Max 0.5 mg/kg ECSS/SC 312-1982 11 Copper (Cu) Max 2.0 mg/kg ECSS/SC 144-1977 12 Lead (Pb) Max 2.0 mg/kg ECSS/SC 313-1982 13 Cadmium (Cd) Max 0.5 mg/kg ECSS/SC 314-1982 14 Mercury (Hg) Max 0.1 mg/kg ECSS/SC 312-1982 11 / 24
Table 14: List of compulsory tests and reference method for SUNFLOWER OIL (WFP spec reference: V2.0, 20 May 2011) No Tests Requirements Reference method (or equivalent) 1 Organoleptic Neutral/bland taste; absence of foreign odours and flavours 2 Moisture and volatile matter 0.2% maximum ISO 662:1998 AOCS Ca 2d-25 IUPAC 2.601 3 Insoluble impurities 0.05% maximum ISO 663:2007 AOCS Ca 3a-46 IUPAC 2.604 4 Free fatty acid 0.15% maximum expressed as oleic acid ISO 18395:2005 AOCS Ca 5a-40 AOAC 940.28 5 Acid value 0.6 mg maximum of ISO 660:2009 KOH/g oil AOCS Cd 3d-63 6 Color 5-1/4 inch Lovibond cell Red: 1.5 maximum BS 684-1.14:1998 AOCS Cc 13b-45 Yellow: 15 maximum 7 Soap content 0.005% maximum AOCS Cc 15-60 BS 684 Section 2.5 8 Peroxide number 2 milliequivalents ISO 3960:2007 maximum of active oxygen BS 684-2.14:2001 per kg oil AOCS Cd 8-53 AOAC 965.33 IUPAC 2.501 9 Saponification value 188-194 mg KOH/g oil ISO 3657:2002 AOCS Cd 3-25 10 Iodine value 118 141 g / 100g oil ISO 3961:2009 AOAC 993.20 IUPAC 2.205 11 Unsaponifiable matter 1.5% maximum ISO 18609:2000 ISO 3596:2000 AOCS Ca 6a 40 IUPAC 2.401 12 Refractive index (ND 40 o C) 1.461 1.468 ISO 6320:2000 AOCS Cc 7-25 AOAC 921.08 IUPAC 2.102 13 Relative density (20 o C /water at 20 C) 0.918 0.923 AOCS 10c-95 IUPAC 2.101 14 Vitamin A 24000 36000 UI per kg oil AOAC 2001.13 15 Vitamin D 2400 3600 UI per kg oil AOAC 2002.05 12 / 24
Table 15: List of compulsory tests and reference method for PALM OLEIN OIL (WFP spec reference: V2.0, 20 May 2011) No Tests Requirements Reference method (or equivalent) 1 Organoleptic Neutral/bland taste; absence of foreign odours and flavours 2 Moisture and volatile matter 0.2% maximum ISO 662:1998 AOCS Ca 2d-25 IUPAC 2.601 3 Insoluble impurities 0.05% maximum ISO 663:2007 AOCS Ca 3a-46 IUPAC 2.604 4 Free fatty acid 0.1% maximum expressed as palmitic acid ISO 18395:2005 AOCS Ca 5a-40 AOAC 940.28 5 Acid value 0.6 mg maximum of KOH/g ISO 660:2009 6 Color 5-1/4 inch Lovibond cell Red: 3 maximum Yellow: 30 maximum AOCS Cd 3d-63 AOCS Cc 13b-45 BS 684-1.14:1998 7 Soap content 0.005% maximum AOCS Cc 15-60 BS 684 Section 2.5 8 Peroxide value 2 milliequivalents maximum of active oxygen per kg of oil ISO 3960:2007 BS 684-2.14:2001 AOCS Cd 8-53 AOAC 965.33 IUPAC 2.501 9 Melting point 24 C maximum AOAC 920.156 ISO 6321:2002 10 Saponification 194-202 mg KOH per g oil ISO 3657:2002 AOCS Cd 3-25 11 Iodine value 55-60 g per 100g oil ISO 3961:2009 AOAC 993.20 IUPAC 2.205 12 Unsaponifiable matter 1.3% maximum ISO 18609:2000 ISO 3596:2000 AOCS Ca 6a 40 IUPAC 2.401 13 Refractive index (ND 40 o C) 1.458 1.460 ISO 6320:2000 AOCS Cc 7-25 AOAC 921.08, IUPAC 2.102 14 Relative density (40 o C /water at 20 C) 0.889 0.920 AOCS 10c-95 IUPAC 2.101 15 Vitamin A 24000 36000 UI per kg oil AOAC 2001.13 16 Vitamin D 2400 3600 UI per kg oil AOAC 2002.05 13 / 24
Table 16: List of compulsory tests and reference method for TOMATO PASTE (WFP spec reference: V1.0, 26 May 2011) No Tests Requirements Reference method (or equivalent) 1 Organoleptic Normal/typical taste and odor. Absence of burnt taste, fermented taste and smell. 2 Concentration (Brix) 28% minimum Consistency by Bostwick (at 12 Brix, at 300C) 4-11 cm/30s 3 Colour (at 12 Brix) 2 minimum Gardner 4 Color Scale 5 ph 4.5 maximum AOAC 981. 6 Acidity 7% maximum ISO 7305 7 Sugar (at dry matter) 42% minimum ISO 3634 8 Salt 2% maximum ISO 3634:1979 9 Total Coliform 10 cfu/g maximum AOAC 2005.03 10 Escherichia Coli Absent AOAC 991.14 11 Salmonella Absent ISO 6579 12 Staphylococcus aureus Absent AOAC 975.55 13 Lysteria monocytogenes Absent AOAC 993.09 14 Bacillus cereus 50 cfu per g maximum AOAC 980.31 15 Howard mould count 60% maximum AOAC 965.41 14 / 24
Table 17: List of compulsory tests and reference method for CANNED BEEF (WFP spec reference: V1.0, 30 March, 2010) N o Tests Requirements Reference method (or equivalent) Nutrition value 1 Moisture 65% max AOAC 950.46 2 Protein 13.0% min AOAC 992.15 3 Fat 18% max AOAC 960.39 4 Ash 2.5% max AOAC 920.153 5 Organoleptic (texture, color, smell, taste) Food additives Max 6 Salt 3% AOAC 935.47 7 Sodium nitrite 100 mg/kg ISO/DSI 2918 Carbonhydrates 8 8% By difference: % CHO= 100%- (%moisture+ % protein+% fat+% ash) 9 Ascorbic acid 300 mg/kg AOAC 967.22 10 Starch 6 % AOAC 996.11 Can Net weight 700/800g CODEX STAN 119-1981, REV. 1 1995 11 12 Incubation test Seam check (vacuum, seam thickness, seam length, countersink depth, cover hook, body hook, actual overlap, % overlap, body hook butting, free space, 13 tightness) Microbiology Max (CFU/g) 14 Total of yeast and moulds 0 AOAC 997.02 15 Total coliforms 0 ISO 4831 : 1993 16 Escherichia Coli 0 AOAC 986.33 17 Salmonella 0 ISO 6888 : 1993 18 Staphylococcus aureus 0 AOAC 2003.07 19 Clostridium botulinum 0 AOAC 977.26 20 Clostridium perfringens 0 ISO 7937: 1985 Chemical contaminants and toxins Max (mg/kg) 21 Cadmium (Cd) 0.05 AOAC 945.58 22 Lead (Pb) 0.5 AOAC 934.07 23 Tin (Sn) 250 AOAC 985.16 24 Sudan red dyes (I, II, II and IV) 0 HPLC or LC-MS/MS Veterinary drugs residues Max (mg/kg) 25 Tetracyline 0.1 AOAC 995.09 26 Chloramphenicol Not detected ISO 13493: 1998 Hormone residues Max (mg/kg) 27 Dietylstylbestrol 0 AOAC 956.10 15 / 24