AAFCO Proficiency Testing Program: 206 Participation
Lamb Feed, Medicated Swine Feed, Medicated 20632 2063 Poultry/Game Bird Feed Dairy Beef Feed Cattle Mineral Molasses Product, Dehydrated Cat Food, Dry Llama Feed Swine Feed, Medicated Goat Feed 20630 20629 20698 20628 2062 20626 20625 20624 Poultry Feed, Medicated 20623 Lamb Feed, Medicated 20622 Cattle Feed Supplement 2062 240 200 60 20 80 40 0 Animal Feed Scheme # Labs
Proximates AFS Analyte Participation: Median Labs Per Sample 0 20 40 60 80 00 20 40 60 80 200 Urea (%) Loss on Drying (%) Protein (%) Crude Fat (%) Crude Fiber (%) Ash (%) Total sugars (%) Urease (%) Fiber, Acid Detergent (%) Fiber, Neutral Detergent (%) Moisture (%) Loss on Drying, High Temp. (%) Starch (%) Fat, Acid hydrolysis (%) Fiber, total dietary TDF (%) Water activity (Units) Non Protein N (NPN) (%) Peroxide value (meq/kg) 6 26 32 45 49 59 2 34 44 9
Minerals AFS Analyte Participation: Median Labs Per Sample 0 20 40 60 80 00 20 40 Aluminum (mg / kg (ppm)) Boron (mg / kg (ppm)) Calcium (%) Cobalt (mg / kg (ppm)) Copper (mg / kg (ppm)) Fluorine (mg / kg (ppm)) Iodine (mg / kg (ppm)) Iron (mg / kg (ppm)) Magnesium (%) Manganese (mg / kg (ppm)) Phosphorus (%) Potassium (%) Salt as chloride (%) Selenium (mg / kg (ppm)) Sodium (%) Sulfur (%) Zinc (mg / kg (ppm)) Molybdenum (mg / kg (ppm)) Barium (mg / kg (ppm)) Vanadium (mg / kg (ppm)) Chloride (%) Arsenic, total (mg / kg (ppm)) Cadmium (mg / kg (ppm)) Chromium (mg / kg (ppm)) Lead (mg / kg (ppm)) Mercury (µg / kg (ppb)) Nickel (mg / kg (ppm)) 2 22 20 6 4 3 4 9 0 9 9 6 39 6 88 83 96 89 99 9 94 34 39
Vet Drugs Sub Scheme Amprolium (mg / kg (ppm)) Carbadox (mg / kg (ppm)) Chlortetracycline (mg / kg (ppm)) Decoquinate (mg / kg (ppm)) Ethoxyquin (mg / kg (ppm)) Hygromycin B (Units / kg) Lasalocid Sodium (mg / kg (ppm)) Melengestrol Acetate (mg / kg (ppm)) Monensin (mg / kg (ppm)) Nicarbazin (mg / kg (ppm)) Oxytetracycline (mg / kg (ppm)) Pyrantel Tartrate (mg / kg (ppm)) Salinomycin (mg / kg (ppm)) Tiamulin (mg / kg (ppm)) Tylosin (mg / kg (ppm)) Narasin (mg / kg (ppm)) Fenbendazole (mg / kg (ppm)) Ractopamine Hydrochloride (mg / kg (ppm)) Methoprene (mg /kg (ppm)) Carbadox, residual (µg / kg) Chlortetracycline, residual (µg / kg) Decoquinate, residual (µg / kg) Lasalocid sodium, residual (µg / kg) Melengestrol Acetate, residual (µg / kg) Monensin, residual (µg / kg) Oxytetracycline, residual (µg / kg) Pyrantel Tartrate, residual (µg / kg) Fenbendazole, residual (µg / kg) Ractopamine Hydrochloride, residual (µg / kg) AFS Analyte Participation: Median Labs Per Sample 0 5 0 5 20 25 0 0 0 2 2 2 2 3 4 4 5 5 6 6 4 6 22 0 Values Submitted
AFS Analyte Participation: Median Labs Per Sample Vitamins Choline Chloride (mg / kg (ppm)) Niacin (mg / kg (ppm)) Pantothenic Acid (mg / kg (ppm)) Riboflavin (mg / kg (ppm)) Thiamine (mg / kg (ppm)) Vitamin A (KU / kg) Vitamin B2 (µg / kg (ppb)) Vitamin D3 (KU / kg) Vitamin E (IU/kg) Vitamin C, phosphorylated (mg / kg (ppm)) Pyridoxine (µg / g) Folic Acid (mg / kg (ppm)) Biotin (mg / kg (ppm)) 0 5 0 5 20 25 3 2 2 5 4 22 20 2
Amino Acids AFS Analyte Participation: Median Labs Per Sample 0 2 4 6 8 0 2 4 6 8 20 22 24 Alanine (%) Arginine (%) Aspartic (%) Cysteine/Cystine (%) Glutamic (%) Glycine (%) Histidine (%) Isoleucine (%) Leucine (%) L-Lysine (%) Methionine (%) Phenylalanine (%) Proline (%) Serine (%) Threonine (%) Tryptophan (%) Tyrosine (%) Valine (%) Taurine (%) 2 3 6 9 20 20 20 20 20 20 2 2 2 2 2 2 2 22 23
Sugars AFS Analyte Participation: Median Labs Per Sample 0 2 3 4 5 Fructose (%) Galactose (%) Glucose (%) Lactose (%) Maltose (%) Sucrose (%) Raffinose (%) Stachyose (%)
Sample # Animal Feed Scheme 206 Z-Cut Homogeneity Screen Sample Name Pass Z-Cut %RSD % Protein # in Z-Cut 2062 Cattle Feed Supplement 0.00% 39.8 3 20622 Lamb Feed, Medicated 0.00% 2. 83 20623 Poultry Feed, Medicated 0.5% 9. 84 20624 Goat Feed 0.00% 9.4 84 20625 Swine Feed, Medicated 0.00% 20. 85 20626 Llama Feed.6%.5 8 2062 Cat Food, Dry 0.52% 33.6 88 20628 Molasses Product, Dehydrated 3.4% 9.3 80 20698 Cattle Mineral.5%.3 20 20629 Dairy Beef Feed 0.38% 30.6 9 20630 Poultry/Game Bird Feed 0.00% 2.9 92 2063 Swine Feed, Medicated 0.00% 20.8 82 20632 Lamb Feed, Medicated - - -
# Labs Pet Food Scheme Participation
Proximates PFS Analyte Participation: Median Labs Per Sample 0 0 20 30 40 50 60 Loss on Drying (%) 5 Protein (%) 55 Crude Fat (%) Crude Fiber (%) 29 30 Ash (%) 42 Total sugars (%) 4 Fiber, Acid Detergent (%) 8 Fiber, Neutral Detergent (%) Moisture (%) 9 Loss on Drying, High Temp. (%) 25 Starch (%) 6 Fat, Acid hydrolysis (%) Fiber, total dietary TDF (%) Water activity (Units) Total Saturated Fatty Acids (% (w/w)) 4 30 The Unknown Scheme
Minerals Aluminum (mg / kg (ppm)) Boron (mg / kg (ppm)) Calcium (%) Cobalt (mg / kg (ppm)) Copper (mg / kg (ppm)) Iodine (mg / kg (ppm)) Iron (mg / kg (ppm)) Magnesium (%) Manganese (mg / kg (ppm)) Phosphorus (%) Potassium (%) Salt as chloride (%) Selenium (mg / kg (ppm)) Sodium (%) Sulfur (%) Zinc (mg / kg (ppm)) Molybdenum (mg / kg (ppm)) Barium (mg / kg (ppm)) Vanadium (mg / kg (ppm)) Chloride (%) Arsenic, total (mg / kg (ppm)) Cadmium (mg / kg (ppm)) Chromium (mg / kg (ppm)) Lead (mg / kg (ppm)) Mercury (µg / kg (ppb)) Nickel (mg / kg (ppm)) 0 5 0 5 20 25 30 35 40 0 2 2 PFS Analyte Participation: Median Labs Per Sample 3 3 3 3 3 3 3 3 6 9 3 24 24 25 26 Samples 30 3 20544 Barley 32 34 35 Sample Name 2064 Tomato Pomace 20642 Lamb Meal 20643 Cheese Powder
NO VET DRUGS! But they are available in the DRW!!!
Vitamins PFS Analyte Participation: Median Labs Per Sample 0 2 3 Choline Chloride (mg / kg (ppm)) Niacin (mg / kg (ppm)) Pantothenic Acid (mg / kg (ppm)) Riboflavin (mg / kg (ppm)) Thiamine (mg / kg (ppm)) Vitamin A (KU / kg) Vitamin B2 (µg / kg (ppb)) Vitamin D3 (KU / kg) Vitamin E (IU/kg) Pyridoxine (µg / g) Folic Acid (mg / kg (ppm)) Biotin (mg / kg (ppm))
Amino Acids PFS Analyte Participation: Median Labs Per Sample 0 2 3 4 5 6 8 Alanine (%) Arginine (%) Aspartic (%) Cysteine/Cystine (%) Glutamic (%) Glycine (%) Histidine (%) Isoleucine (%) Leucine (%) L-Lysine (%) Methionine (%) Phenylalanine (%) Proline (%) Serine (%) Threonine (%) Tryptophan (%) Tyrosine (%) Valine (%) Taurine (%) 3 6 6 6 6 6 6 6 8
Sugars PFS Analyte Participation: Median Labs Per Sample 0 2 Fructose (%) Galactose (%) Glucose (%) Lactose (%) Maltose (%) Sucrose (%)
Pet Food Scheme 205-6 Z-Cut Homogeneity Screen Sample # Sample Name Pass Z-Cut %RSD % Protein # in Z-Cut 20544 Barley 3.4% 0.6 32 2064 Tomato Pomace 0.5% 20. 26 20642 Lamb Meal 0.00% 55.3 24 20643 Cheese Powder.38% 5.0 24 20644 Oat Flour - - -
Z-Score Indications in Animal Feed Scheme and Pet Food Scheme 206 to Date: 34,246 Tests -4-3 -2-0 2 3 4 Compliance 2 > Z > -2 Warning Actionable 3 < Z < -3 90.2% 4.6% 5.2%
Trilogy sources the base feeds. Mycotoxin Scheme Sample Engineering Materials thoroughly processed with regard to particle size and blending. 0,000 lb Masters Collection Carefully sourced feeds naturally contaminated with Mycotoxins. Incubated to raise concentration. Homogenous Samples for distribution. Certificate of Analysis and homogeneity data.
# Labs Mycotoxins Scheme Participation
Mycotoxin Analyte Participation All Labs Participating
Minerals Scheme Sample Engineering Base feed sourced from prior Check Samples. Minerals sourced separately. Able Laboratory Inc. Bob Kieffer Existing Minerals in base feed established during prior testing round. Added Minerals solubilized and sprayed over existing pre-ground base feed prior to blending and sample portioning. Spike concentrations calculated. Homogenous Samples for distribution.
# Labs Minerals Scheme Participation
Minerals Scheme Analyte Participation All Labs Participating
Method Codes Fatty Acids The Unknown Scheme Code Fatty Acid Groupings 54 Total Omega-3 Polyunsaturated Fatty Acids 56 Total Omega-6 Polyunsaturated Fatty Acids 58 Total Saturated Fatty Acids 62 Total Monounsaturated Fatty Acids 64 Total cis Monounsaturated Fatty Acids 66 Total Polyunsaturated Fatty Acids 68 Total cis Polyunsaturated Fatty Acids 0 Total Fat (equivalent to NLEA) 2 Total Fatty Acids Methods ##.0 Direct Methylation by Alkali Hydrolysis & GC ##.02 Direct Methylation by Acid-Alkali Hydrolysis & GC ##.99 Miscellaneous Code Individual Fatty Acids 0 Propionic Acid (3:0) 02 Butyric Acid (4:0) 03 Valeric Acid (5:0) 04 Caproic Acid (6:0) 06 Caprylic acid (8:0) 08 Capric acid (0:0) 0 Lauric Acid (2:0) 4 Myristic Acid (4:0 ) 6 Palmitic Acid (6:0) 8 Palmitoleic Acid (9c-6:) 20 Margaric acid (:0) 22 Stearic Acid (8:0) 24 Oleic Acid (9c-8:) 26 Linoleic Acid n-6 (8:2, all cis) 28 alpha-linolenic Acid n-3 (8:3, all cis) 30 Arachidic Acid (20:0) 32 Gondoic Acid (c-20:) 36 Arachidonic Acid n-6 (20:4, all cis) 38 Mead Acid n-9 (20:3, all cis) 40 Eicosapentaenoic Acid n-3 EPA (all cis) 42 Behenic Acid (22:0) 44 Erucic Acid (3c-22:) 46 Docosapentaenoic Acid n-3 DPA (all cis) 48 Lignoceric Acid (24:0) 50 Docosahexaenoic Acid n-3 DHA (all cis) 52 Nervonic Acid (24:) isomers
AAFCO Proficiency Testing Program Scheme Participation Animal Feed Scheme Proximates 3 % Minerals 44 % Vet Drugs % Vitamins 3 % Amino Acids 4 % Sugars % Pet Food Scheme Proximates 34 % Minerals 45 % Vitamins 4 % Amino Acids 5 % Sugars 2 % Mycotoxin Scheme Engineered Concentrations Minerals Scheme Engineered Concentrations
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