Overview of Production and Nutrient Content of DDGS. Dr. Jerry Shurson Department of Animal Science University of Minnesota

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Overview of Production and Nutrient Content of DDGS Dr. Jerry Shurson Department of Animal Science University of Minnesota

What is DDGS? o o o Distiller s dried grains with solubles (DDGS) n By-product of the dry-milling ethanol industry Nutrient composition is different between dry-mill, wet-mill and beverage alcohol by-products n n n n n DDGS fuel ethanol DDGS - whiskey distilleries Corn gluten feed wet mill Corn gluten meal wet mill Brewer s dried grains beer manufacturing Nutrient content depends on the grain source used o Corn DDGS - Midwestern US o Wheat DDGS - Canada o Sorghum (milo) DDGS - Great Plains US o Barley DDGS

Comparison of Nutrient Composition (100% Dry Matter Basis) of Golden DDGS to Corn Gluten Feed, Corn Gluten Meal, Corn Germ Meal, and Brewer s Dried Grains Golden DDGS (UM) Corn Gluten Feed (NRC) Corn Gluten Meal (NRC) Corn Germ Meal (Feedstuffs) Brewer s Dried Grains (NRC) Protein, % 30.6 23.9 66.9 22.2 28.8 Fat, % 10.7 3.3 3.2 1.1 7.9 NDF, % 43.6 37.0 9.7 No data 52.9 DE, kcal/kg 4011 3322 4694 No data 2283 ME, kcal/kg 3827 2894 4256 3222 2130 Lys, % 0.83 0.70 1.13 1.00 1.17 Met, % 0.55 0.39 1.59 0.67 0.49 Thr, % 1.13 0.82 2.31 1.22 1.03 Trp, % 0.24 0.08 0.34 0.22 0.28 Ca, % 0.06 0.24 0.06 0.33 0.35 Available P, % 0.80 0.54 0.08 0.17 0.21

Types of Distiller s By- Products from Dry-Grind Ethanol Plants o o o o o o Wet distiller s grains n Primarily beef, some dairy Dry distiller s grains n Beef and dairy Wet distiller s grains with solubles n Beef and dairy Dried distiller s grains with solubles n Dairy, swine, poultry, some beef Modified wet cake (blend of wet and dry distiller s grains) n Primarily beef, some dairy Condensed distiller s solubles n n Beef and dairy Ontario, Canada - swine liquid feeding systems

Proportion of Distiller s Grains Marketed Wet vs Dry 60% 40% Wet Dry

Samples of High Quality, Golden Corn DDGS VeraSun - Aurora, SD CVEC - Benson, MN Al-Corn - Claremont, MN MGP Lakota, IA CMEC - Little Falls, MN Agri-Energy - Luverne, MN LSCP - Marcus, IA DENCO Morris, MN

Dry-Milling Average Ethanol Yield Per Bushel (25.4 kg) of Corn o Ethanol o DDGS o CO2 10.2 liters 8.2 kg 8.2 kg Slide courtesy of Ms. Kelly Davis, CVEC, Benson, MN

U.S. DDGS Production 7000000 7,000,000 Metric Tons 6000000 5000000 4000000 3000000 2000000 1000000 0 3,500,000 3,000,000 1,800,000 900,000 320,000 1980 1985 1990 1995 2000 Est 2005 Source: Steve Markham Commodity Specialists Company

U.S. DDGS Consumption Estimate 2001 Estimate 2002 4% 15 % 36% 60% Dairy Beef Poultry/Swine 5% 45% Dairy Beef Poultry Swine 35% Estimate 2003 Estimate 2004 39% 4% 11% 46% Dairy Beef Poultry Swine 3% 37% 16 % 44% Dairy Beef Poultry Swine CSC 2005

Estimated DDGS Usage in U.S. Swine Feeds 2001-2004 (Metric Tonnes) 1,200,000 1,000,000 800,000 600,000 400,000 2001 2002 2003 2004 200,000 0

U.S. DDGS Exports Are Increasing 900000 800000 700000 600000 500000 400000 300000 200000 100000 0 1996 1998 2000 2002 Source: Commodity Specialists Company Metric Tons

Major U.S. DDGS Importing Countries (84% of Total Exports) 8.3% 9.2% 9.3% 11.0% 22.6% 24.0% Ireland UK Canada Spain Mexico Portugal

Asian Countries Importing U.S. DDGS (4.5% of Total Exports) Malaysia Indonesia Taiwan Vietnam S. Korea Philippines China Thailand Japan

Comparison of Proximate Analysis of High Quality U.S. Golden Corn DDGS with Chinese DDGS (100% Dry Matter Basis) 35 30 25 % 20 15 10 5 US Avg China-Taiwan China-Korea 0 Moist. Protein Fat Fiber Ash U.S. Avg. = average of values obtained from samples from 10 New Generation dry-mill ethanol plants (Spiehs et al., 2002) China-Taiwan = actual analyzed values of a Chinese DDGS sample collected in Taiwan in 2003 China-Korea = actual analyzed values of a sample of Chinese DDGS obtained from S. Korea in 2005

Comparison of Calculated Digestible Energy, Metabolizable Energy for Swine of U.S. New Generation DDGS to Chinese DDGS (100% Dry Matter Basis) 4500 4000 3500 3000 2500 2000 1500 1000 500 0 DE, Mcal/kg ME, Mcal/kg U.S. Avg. China-Taiwan China-Korea U.S. Avg. = average of calculated values obtained from DDGS samples from 10 New Generation ethanol plants (Spiehs et al., 2002) China-Taiwan = calculated values from actual proximate analysis of a sample of Chinese DDGS obtained from Taiwan in 2003 China-Korea = calculated values from actual proximate analysis of a sample of Chinese DDGS obtained from S. Korea in 2005

Comparison of Amino Acid Analysis of U.S. New Generation DDGS with Chinese DDGS (100% Dry Matter Basis) 1.4 1.2 1 % 0.8 0.6 0.4 0.2 US Avg China-Taiwan China-Korea 0 Lys Met Cys Thr Trp U.S. Avg. = average of values obtained from samples from 10 New Generation dry-mill ethanol plants (Spiehs et al., 2002) China-Taiwan = actual analyzed values of a Chinese DDGS sample collected in Taiwan in 2003 China-Korea = actual analyzed values of a sample of Chinese DDGS obtained from S. Korea in 2005

Comparison of Macro-mineral Analysis of U.S. New Generation DDGS with Chinese DDGS (100% Dry Matter Basis) 1 0.9 0.8 0.7 0.6 0.5 0.4 0.3 0.2 0.1 0 Ca, % P, % K, % Mg, % Na, % US Avg. China-Taiwan China-Korea U.S. Avg. = average of values obtained from samples from 10 New Generation dry-mill ethanol plants (Spiehs et al., 2002) China-Taiwan = actual analyzed values of a Chinese DDGS sample collected in Taiwan in 2003 China-Korea = actual analyzed values of a sample of Chinese DDGS obtained from S. Korea in 2005

Comparison of Trace Mineral Analysis of U.S. New Generation DDGS with Chinese DDGS (100% Dry Matter Basis) 700 600 500 400 300 200 US Avg. China-Taiwan China-Korea 100 0 Zn, ppm Mn, ppm Cu, ppm Fe, ppm U.S. Avg. = average of values obtained from samples from 10 New Generation dry-mill ethanol plants (Spiehs et al., 2002) China-Taiwan = actual analyzed values of a Chinese DDGS sample collected in Taiwan in 2003 China-Korea = actual analyzed values of a sample of Chinese DDGS obtained from S. Korea in 2005

Ethanol Plants are Developing New Distiller s By-Products n n n n n n DDG Winnebago High protein DDGS Dakota Commodities De-germed or partial de-germed DDGS Quick fiber Removing P Others

Comparison of Nutrient Content of Dakota Gold DDGS with High Protein Dakota Gold (100% DM Basis) 40 35 30 25 20 15 10 5 0 Protein, % Fat, % NDF, % Ash, % DDGS HP DDGS

Comparison of Amino Acid Content of Dakota Gold DDGS with High Protein Dakota Gold (100% DM Basis) 1.2 1 0.8 0.6 0.4 DDGS HP DDGS 0.2 0 Lys, % Met, % Cys, % Thr, % Trp, %

Comparison of Mineral Content of Dakota Gold DDGS with High Protein Dakota Gold (100% DM Basis) 0.9 0.8 0.7 0.6 0.5 0.4 0.3 0.2 0.1 0 Ca, % P, % Na, % S, % DDGS HP DDGS

Proximate Analysis and Calculated Swine Energy Values Among 27 U.S. DDGS Sources (100% Dry Matter Basis) Nutrient Average Range Dry matter, % 89.3 87.3 92.4 Crude protein, % 31.0 28.7 32.9 Fat, % 10.6 8.8 12.4 Fiber, % 7.2 5.4 10.4 Ash, % 6.1 3.0 9.8 ADF, % 13.6 8.0 18.1 Swine DE, kcal/kg 4053 3737 4319 Swine ME, kcal/kg 3790 3504 4048

Amino Acid Analysis Averages and Ranges Among 27 U.S. DDGS Sources (100% Dry Matter Basis) Nutrient Average Range Arg, % 1.31 1.01 1.48 His, % 0.84 0.71 0.98 Ile, % 1.17 1.01 1.31 Leu, % 3.58 2.91 3.96 Lys, % 0.89 0.61 1.06 Met, % 0.65 0.54 0.76 Cys, % 0.68 0.61 0.76 Phe, % 1.51 1.36 1.72 Thr, % 1.15 1.01 1.28 Trp, % 0.25 0.18 0.28 Val, % 1.58 1.31 1.80

Mineral Analysis Averages and Ranges Among 27 U.S. DDGS Sources (100% Dry Matter Basis) Nutrient Average Range Ca, % 0.08 0.02 0.12 P, % 0.75 0.42 0.99 K, % 0.96 0.45 1.27 Mg, % 0.29 0.14 0.38 S, % 0.62 0.34 1.05 Na, % 0.15 0.04 0.52 Zn, ppm 62 38 105 Mn, ppm 19 9 27 Cu, ppm 6 3 10 Fe, ppm 133 77 239

Nutrient Composition of High Quality U.S. Corn DDGS for Ruminants Nutrient % of Dry Matter Crude protein 30.1 Ruminally undegradable protein (% of CP) 55.0 NE maintenance (Mcal/kg) 2.07 NE gain (Mcal/kg) 1.41 NE lactation (Mcal/kg) 2.26 NDF 41.5 ADF 16.1 Ether extract 10.7

Comparison of Energy Values of DDGS for Swine (88% DM Basis) Golden DDGS Calculated U of M Golden DDGS Trial avg. U of M Traditional DDGS Calculated U of M DDGS NRC (1998) DE, kcal/kg 3488 Range 3418-3537 ME, kcal/kg 3162 Range 3087-3215 3528 Range 2975-4086 3367 Range 2820-3916 3409 3449 3098 2672 Corn (NRC, 1998): DE (kcal/kg) = 3484 ME (kcal/kg) = 3382

Comparison of DE and ME Estimates of DDGS for Swine (88% DM) DE, Mcal/kg ME, Mcal/kg NE, Mcal/kg U of M Golden DDGS (1999) 3.49 3.37 No data U of M Traditional (1999) 1 3.41 3.10 No data KSU New Generation (2004) 2 3.87 3.49 3.70 2.61 KSU Old Generation (2004) 3 3.73 3.13 3.59 2.45 Hanor-Hubbard-Ajinomoto (2004) 4 No data 3.25 2.42 NRC (1998) 3.45 2.67 No data 1 Calculated values 2 Determined by growth and metabolism trials (source Dakota Gold) 3 Not DDGS but corn gluten from a NE ethanol plant 4 Determined by growth trials (source Dakota Gold)

Comparison of Energy Values of Golden Corn DDGS for Poultry (88% DM Basis) AME, kcal/kg 2260 Range 2090-2418 Golden DDGS NRC (1994) 2480 TME, kcal/kg 2850 Range 2650-3082 3097 Source: Noll and Parsons. 2003. Unpublished data.

Comparison of Amino Acid Composition of DDGS (88% dry matter basis) Golden DDGS Traditional DDGS DDGS (NRC, 1998) Lysine, % 0.75 (17.3) 0.47 (26.5) 0.59 Methionine, % 0.63 (13.6) 0.44 (4.5) 0.48 Threonine, % 0.99 (6.4) 0.86 (7.3) 0.89 Tryptophan, % 0.22 (6.7) 0.17 (19.8) 0.24 Valine, % 1.32 (7.2) 1.22 (2.3) 1.23 Arginine, % 1.06 (9.1) 0.81 (18.7) 1.07 Histidine, % 0.67 (7.8) 0.54 (15.2) 0.65 Leucine, % 3.12 (6.4) 2.61 (12.4) 2.43 Isoleucine, % 0.99 (8.7) 0.88 (9.1) 0.98 Phenylalanine, % 1.29 (6.6) 1.12 (8.1) 1.27 Values in ( ) are CV s among plants

Standardized Ileal True Digestible Amino Acid Levels and Coefficients of Corn DDGS for Swine (10 Sources of Golden DDGS) Amino acid True Dig. Amino Acid, % Digestibility Coefficient, % Average Lysine 0.30 0.54 44 61 57 Methionine 0.48 0.60 74 85 79 Threonine 0.61 0.76 62 71 67 Tryptophan 0.13 0.14 74 80 77 Source: Stein et al., 2005. Unpublished data.

True Digestible Amino Acid Levels of Golden Corn DDGS for Poultry (5 Sources) Amino acid True Dig. Amino Acid, % Average Digestibility Coefficient, % Average Methionine 0.35 0.53 0.43 86-90 88 Cystine 0.28 0.57 0.40 66-85 76 Lysine 0.37 0.74 0.53 59-83 71 Arginine 0.73 1.18 0.93 80-90 86 Tryptophan 0.14 0.21 0.18 76-87 82 Threonine 0.61 0.92 0.74 67-81 75 Source: Noll and Parsons. 2003. Unpublished data.

Fig. 1. Regression of digestible lys (%) and color (L*, b*) 60 55 50 R 2 = 0.71 L*, b* score 45 40 35 R 2 = 0.74 L* b* Linear (L*) Linear (b*) 30 25 20 0.20 0.30 0.40 0.50 0.60 0.70 0.80 Lys (%) Source: Dr. Sally Noll (2003)

Fig. 2. Regression of digestible cys (%) and color (L*, b*) 60 55 50 R 2 = 0.66 L*, b* score 45 40 35 R 2 = 0.67 L* b* Linear (L*) Linear (b*) 30 25 20 0.20 0.30 0.40 0.50 0.60 0.70 0.80 Cys (%)

Fig. 3. Regression of digestible thr (%) and color (L*, b*) 60 55 R 2 = 0.37 50 L*, b* score 45 40 35 R 2 = 0.40 L* b* Linear (L*) Linear (b*) 30 25 20 0.20 0.30 0.40 0.50 0.60 0.70 0.80 0.90 1.00 Thr (%)

Comparison of Phosphorus Level and Relative Availability of DDGS for Swine (88% dry matter basis) Golden DDGS Traditional DDGS DDGS NRC (1998) Corn NRC (1998) Total P, % 0.78 Range 0.62-0.87 P Availability, % 90 Range 88-92 0.79 0.73 0.25 No data 77 14 Available P, % 0.70 No data 0.56 0.03

Comparison of Phosphorus Level and Relative Availability of DDGS for Poultry (88% dry matter basis) Golden DDGS NRC (1994) Total P, % 0.74 0.72 P Availability, % 61 Range 54-68 54 Available P, % 0.45 0.39 Source: 2003 Lumpkins, Dale, and Batal, University of Georgia. Abstract.

Relative Value of DDGS Differs Depending on Species Feed Dollars/ ton Assumptions: Corn $2.00 / bu SBM $175.00 / ton Urea $360.00 / ton Non-ruminant diets corn/sbm Ruminant diets typical diets with competing by-products. Dairy Lactation $114.24 Poultry Finisher $100.09 Layer Diet $104.66 Swine G-F Diet $96.34 Beef Feedlot $108.00 Source: Tilstra, Land O Lakes

U of M DDGS Web Site www.ddgs.umn.edu We have developed a DDGS web site featuring: * nutrient profiles and photos of DDGS samples * research summaries - swine, poultry, dairy, & beef - DDGS quality * presentations given * links to other DDGS related web sites * international audiences