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1 CD/K/4:2013 ICS FDEAS 820:2013 FINAL DRAFT EAST AFRICAN STANDARD Dextrose Monohydrate (Glucose powder) Specification EAST AFRICAN COMMUNITY EAS 2013 First Edition 2013
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3 CD/K/4:2013 Copyright notice This EAC document is copyright-protected by EAC. While the reproduction of this document by participants in the EAC standards development process is permitted without prior permission from EAC, neither this document nor any extract from it may be reproduced, stored or transmitted in any form for any other purpose without prior written permission from EAC. Requests for permission to reproduce this document for the purpose of selling it should be addressed as shown below or to EAC s member body in the country of the requester: East African Community 2013 All rights reserved East African Community P.O.Box 1096 Arusha Tanzania Tel: /8 Fax: / eac@eachq.org Web: Reproduction for sales purposes may be subject to royalty payments or a licensing agreement. Violators may be persecuted ii EAC 2013 All rights reserved
4 CD/K/4:2013 Contents Page Foreword... iv 1 Scope Definition Requirements Environment... Error! Bookmark not defined. 6 Hygiene Packaging Labelling Sampling... 6 Annex A (normative) Determination of ph in dextrose monohydrate (glucose powder)... 8 Annex B (normative) Determination of total acidity in dextrose monohydrate (glucose powder)... 9 Annex C (informative) Bibliography EAC 2013 All rights reserved iii
5 CD/K/4:2013 Foreword Development of the East African Standards has been necessitated by the need for harmonizing requirements governing quality of products and services in the East African Community. It is envisaged that through harmonized standardization, trade barriers that are encountered when goods and services are exchanged within the Community will be removed. In order to achieve this objective, the Community established an East African Standards Committee mandated to develop and issue East African Standards. The Committee is composed of representatives of the National Standards Bodies in Partner States, together with the representatives from the private sectors and consumer organizations. Draft East African Standards are circulated to stakeholders through the National Standards Bodies in the Partner States. The comments received are discussed and incorporated before finalization of standards, in accordance with the procedures of the Community. East African Standards are subject to review, to keep pace with technological advances. Users of the East African Standards are therefore expected to ensure that they always have the latest versions of the standards they are implementing. CD/K/4 was prepared by Technical Committee EASC/ TC/019, Sugar and Sugar products. iv EAC 2013 All rights reserved
6 CD/K/4:2013 Introduction EAC 2013 All rights reserved v
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8 DRAFT EAST AFRICAN STANDARD CD/K/4:2013 Dextrose Monohydrate (Glucose powder) Specification 1 Scope. This draft East African Standard specifies the requirements and methods of test and sampling for dextrose monohydrate (glucose powder) intended for human consumption as food and industrial applications. This standard does not apply to dextrose monohydrate for intravenous applications 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EAS 39, Code of practice for food and drink manufacturing industry EAS 38, Labelling of pre-packaged foods ISO 1741 Dextrose -- Determination of loss in mass on drying -- Vacuum oven method ISO 1743 Glucose syrup -- Determination of dry matter content -- Refractive index method ISO 4832 Microbiology of food and animal feeding stuffs -- Horizontal method for the enumeration of coliforms -- Colony-count technique ISO 4833 Microbiology of food and animal feeding stuffs -- Horizontal method for the enumeration of microorganisms -- Colony-count technique at 30 degrees C EAC 2013 All rights reserved 1
9 ISO 5377 Starch hydrolysis products -- Determination of reducing power and dextrose equivalent -- Lane and Eynon constant titre method ISO 5379: Starches and derived products -- Determination of sulfur dioxide content -- Acidimetric method and nephelometric method ISO 5809 Starches and derived products -- Determination of sulphated ash ISO 6579 Microbiology of food and animal feeding stuffs -- Horizontal method for the detection of Salmonella spp ISO Microbiology of food and animal feeding stuffs -- Horizontal method for the enumeration of coagulase-positive staphylococci (Staphylococcus aureus and other species) -- Part 1: Technique using Baird- Parker agar medium ISO Starch and derived products -- Heavy metals content -- Part 1: Determination of arsenic content by atomic absorption spectrometry ISO Starch and derived products -- Heavy metals content -- Part 1: Determination of lead content by atomic absorption spectrometry ISO 16654:2001 Microbiology of food and animal feeding stuffs -- Horizontal method for the detection of Escherichia coli O157 ISO Microbiology of food and animal feeding stuffs -- Horizontal method for the enumeration of yeasts and moulds -- Part 1: Colony count technique in products with water activity greater than 0,95 3 Terms and Definition For the purposes of this standard the following definition shall apply: Dextrose monohydrate purified and crystallized D-glucose containing one molecule of water of crystallization Extraneous matter Organic matter originating from sugar cane plants and/or their products other than molasses Foreign matter 2 EAC 2013 All rights reserved
10 Organic and inorganic materials ( such as sand, soil, glass) and other extraneous matter in molasses 4 Requirements 4.1 General Requirements Glucose powder shall be : a) in the form of fine white crystals or a white powder b) Free from off-flavours. c) free from foreign matter, d) free from other sugars, soluble starch and dextrin. e) readily soluble in water and give a sweet solution 4.2 Specific requirements Dextrose monohydrate shall comply with the compositional requirements/limits specified in Table 1. Table 1 Compositional requirements/limits for Dextrose monohydrate (glucose powder) Sl No Characteristics Requirements/li mits Test methods i) Moisture content, %, max. 10 ISO 1741 ii) Dextrose equivalent (dry matter basis) min. iii) D-glucose content (dry matter basis).m/m, %, min. iv) v) vi) Sulphated ash, dry matter basis, m/m, %, max. Sulphur dioxide (SO 2 ) ppm, % max. Total solids content m/m, %, min ISO ISO ISO ISO ISO 1743 vii) ph Annex A viii) Total acidity as HCl/g, max Annex B EAC 2013 All rights reserved 3
11 5. food additives Only the food additives permitted in CODEX STAN 192 standards for food additives may be used 6. Contaminants 6.1 Pesticide residues Dextrose Monohydrate ( glucose powder) shall comply with those maximum pesticide residues established by the codex alimentarius commission for this commodity 6.2 Heavy metal Dextrose Monohydrate ( glucose powder) shall be free from heavy metals in amounts which may represent a hazard to human health. 7 Hygiene Dextrose monohydrate shall be manufactured and handled in premises conforming to the EAS 39 Hygiene for food and drink manufacturing industry Code of practice Microbiological limits Dextrose monohydrate shall comply with the microbiological limits stipulated in Table 3. Table 3 Microbiological limits 4 EAC 2013 All rights reserved
12 SL No. Parameter Limits Test method ii) Yeasts and Moulds cfu per g, max. 20 ISO iii) iv) Coliforms cfu per g, max 10 ISO 4832 v) E. Coli cfu per 30 g, max Absent ISO vi) Salmonella cfu per 30 g, max. Absent ISO 6579 vii) Staphylococcus aureus cfu per 30 g, max. Absent ISO Packaging 8.1 The product shall be packed in food grade materials that ensure product safety and integrity 8.2The package fill shall conform to the Weights and Measures acts of the East African Partner States 9. Labelling Labelling shall be done in accordance with EAS 38, in addition the following shall be legibly and indelibly marked on each package: i) name of the product as dextrose Monohydrate or Glucose powder ii) name, address and the physical location of the manufacturer/importer/packer; iii) brand/trade name; EAC 2013 All rights reserved 5
13 iv) batch or code number; v) net weight in metric units ; vi) storage conditions; vii) date of manufacture; viii) expiry date; ix) instructions for use; x) country of origin; xii) instructions on disposal of used packaged; xiii) declaration of status if raw material is genetically modified. 10. Sampling In drawing, preparing, storing and handling of samples, the following precautions and directions shall be observed. Samples shall be taken in a protected place not exposed to damp air, dust or soot. The sampling instruments shall be clean and dry before use. When sampling for microbiological purposes,the sampling instruments and containers for samples shall be sterilized preferably by dry heat at 170 C for one hour before use. Precautions shall be taken to protect the samples, the material being sampled, the sampling instruments and the containers for samples from adventitious contamination. The samples shall be placed in clean, dry, and moisture-proof containers. 6 EAC 2013 All rights reserved
14 The sample containers shall be sealed air tight after filling, and marked with full details of sampling: the date of sampling, batch number, name and place of factory, name of the person sampling and other important particulars of the consignments. Samples shall be protected from light as far as practicable and shall be stored in a cool and dry place. EAC 2013 All rights reserved 7
15 Annex A (normative) Determination of ph in dextrose monohydrate (glucose powder) Weigh 10 g of glucose powder and dissolve it in 100 ml of carbon dioxide-free water. Take the reading of the solution (ph) using a ph meter. 8 EAC 2013 All rights reserved
16 Annex B (normative) Determination of total acidity in dextrose monohydrate (glucose powder) Dissolve 5.0 g of glucose powder in 50 ml of carbon dioxide-free water. Add a few drops of phenolphthalein indicator and titrate with N sodium hydroxide to a distinct pink colour. Not more than 0.30 ml is required for neutralization. Calculate the total acidity as HCl/g. Total acidity = Titre used x Normality Weight of the sample (g) EAC 2013 All rights reserved 9
17 Annex C (informative) Bibliography Sri Lanka Standard 617 Specification for glucose. Codex Alimentarius Commission Codex Stan, Dextrose monohydrate. 10 EAC 2013 All rights reserved
18 DEAS 304:2013 EAC 2013 All rights reserved
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