ALPHA ANALYTICAL LABORATORIES. Eight Walkup Drive Westborough, Massachusetts (508)
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1 Eight Walkup Drive Westborough, Massachusetts (508) Client: ERM-New England Laboratory Job Number: L Address: 399 Boylston Street 6th Floor Boston, MA Date Received: 28-SEP-2005 Attn: Jeremy Picard Date Reported: 05-OCT-2005 Project Number: Delivery Method: Alpha Site: RAYTHEON WAYLAND The following questions pertain only to MCP Analytical Methods An affirmative response to questions A,B,C & D is required for "Presumptive Certainty" status A. Were all samples received by the laboratory in a condition consistent with those YES described on their Chain-of-Custody documentation for the data set? B. Were all QA/QC procedures required for the specified analytical method(s) included YES in this report followed, including the requirement to note and discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? C. Does the analytical data included in this report meet all the requirements for YES "Presumptive Certainty", as described in section 2.0 of the MADEP document CAM VII A, "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D. VPH and EPH methods only: Was the VPH or EPH method run without significant NA modifications, as specified in Section 11.3? A response to questions E and F is required for "Presumptive Certainty" status E. Were all QC performance standards and recommendations for the specified method(s) YES achieved? F. Were results for all analyte-list compounds/elements for the specified method(s) NO reported? Any answers of NO to the above questions are addressed in the case narrative. I, the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized by: Technical Director :39 Page 1 of 20
2 Laboratory Job Number: L Date Reported: 05-OCT-2005 ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION L MW-555S WAYLAND, MA L MW-555MA WAYLAND, MA L MW-555MB WAYLAND, MA L MW-555D WAYLAND, MA L MW-554D WAYLAND, MA L MW-554MB WAYLAND, MA L MW-554S WAYLAND, MA L MW-554MA WAYLAND, MA L MW-556D WAYLAND, MA L MW-556S WAYLAND, MA L MW-556M WAYLAND, MA L DUP WAYLAND, MA :39 Page 2 of 20
3 Laboratory Job Number: L NARRATIVE REPORT Report Submission In reference to question F: At the client's request, all submitted samples were not analyzed for the full MCP list of compounds specified for the Method :39 Page 3 of 20
4 Laboratory Sample Number: L Date Collected: 26-SEP :40 MW-555S Number & Type of Containers: 1-Plastic Arsenic, Dissolved mg/l : :25 MG :39 Page 4 of 20
5 Laboratory Sample Number: L Date Collected: 26-SEP :40 MW-555MA Number & Type of Containers: 3-Plastic Arsenic, Dissolved ND mg/l : :33 MG :39 Page 5 of 20
6 Laboratory Sample Number: L Date Collected: 26-SEP :30 MW-555MB Number & Type of Containers: 1-Plastic Arsenic, Dissolved ND mg/l : :45 MG :39 Page 6 of 20
7 Laboratory Sample Number: L Date Collected: 26-SEP :30 MW-555D Number & Type of Containers: 1-Plastic Arsenic, Dissolved mg/l : :49 MG :39 Page 7 of 20
8 Laboratory Sample Number: L Date Collected: 27-SEP :50 MW-554D Number & Type of Containers: 1-Plastic Arsenic, Dissolved ND mg/l : :05 MG :39 Page 8 of 20
9 Laboratory Sample Number: L Date Collected: 27-SEP :00 MW-554MB Number & Type of Containers: 1-Plastic Arsenic, Dissolved ND mg/l : :10 MG :39 Page 9 of 20
10 Laboratory Sample Number: L Date Collected: 27-SEP :18 MW-554S Number & Type of Containers: 1-Plastic Arsenic, Dissolved mg/l : :14 MG :39 Page 10 of 20
11 Laboratory Sample Number: L Date Collected: 27-SEP :05 MW-554MA Number & Type of Containers: 1-Plastic Arsenic, Dissolved ND mg/l : :18 MG :39 Page 11 of 20
12 Laboratory Sample Number: L Date Collected: 27-SEP :35 MW-556D Number & Type of Containers: 1-Plastic Arsenic, Dissolved ND mg/l : :22 MG :39 Page 12 of 20
13 Laboratory Sample Number: L Date Collected: 27-SEP :35 MW-556S Number & Type of Containers: 1-Plastic Arsenic, Dissolved mg/l : :26 MG :39 Page 13 of 20
14 Laboratory Sample Number: L Date Collected: 27-SEP :45 MW-556M Number & Type of Containers: 1-Plastic Arsenic, Dissolved mg/l : :10 MG :39 Page 14 of 20
15 Laboratory Sample Number: L Date Collected: 27-SEP :00 DUP Number & Type of Containers: 1-Plastic Arsenic, Dissolved ND mg/l : :34 MG :39 Page 15 of 20
16 Laboratory Job Number: L QUALITY ASSURANCE BATCH LCS/LCSD ANALYSIS Parameter LCS % LCSD % RPD RPD Limit QC Limits for sample(s) (WG , WG ) Arsenic, Dissolved :39 Page 16 of 20
17 Laboratory Job Number: L QUALITY ASSURANCE BATCH MS/MSD ANALYSIS Parameter MS % MSD % RPD RPD Limit MS/MSD Limits for sample(s) (L , WG ) Arsenic, Dissolved :39 Page 17 of 20
18 Laboratory Job Number: L QUALITY ASSURANCE BATCH BLANK ANALYSIS Blank Analysis for sample(s) (WG ) Arsenic, Dissolved ND mg/l : :12 MG :39 Page 18 of 20
19 ADDENDUM I REFERENCES 60. Quality Assurance and Quality Control Requirements and Performance Standards for SW-846 Methods. MADEP BWSC. WSC-CAM-IIA (Revision 4), WSC-CAM-V C (Revision 2), WSC-CAM-IIIA (Revision 5). May GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found. METHOD Method number by which analysis was performed. ID Initials of the analyst. ND Not detected in comparison to the reported detection limit. NI Not Ignitable. ug/cart Micrograms per Cartridge. LIMITATION OF LIABILITIES Alpha Analytical, Inc. performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical, Inc., shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical, Inc. be held liable for any incidental consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical, Inc. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding times and splitting of samples in the field :39 Page 19 of 20
20 Laboratory Job Number: L LOGIN SPECIFIC INFORMATION Were project specific reporting limits specified? YES Cooler Information Cooler Custody Seal A Absent Container Information Container ID Container Type Cooler ph Temp Pres Seal Analysis L A Plastic 250ml HNO3 preserved A <2 2.3C Y Absent MCP-AS-6010S L A Plastic 250ml HNO3 preserved A <2 2.3C Y Absent MCP-AS-6010S L B Plastic 250ml HNO3 preserved Y Absent MCP-AS-6010S L C Plastic 250ml HNO3 preserved Y Absent MCP-AS-6010S L A Plastic 250ml HNO3 preserved A <2 2.3C Y Absent MCP-AS-6010S L A Plastic 250ml HNO3 preserved A <2 2.3C Y Absent MCP-AS-6010S L A Plastic 250ml HNO3 preserved A <2 2.3C Y Absent MCP-AS-6010S L A Plastic 250ml HNO3 preserved A <2 2.3C Y Absent MCP-AS-6010S L A Plastic 250ml HNO3 preserved A <2 2.3C Y Absent MCP-AS-6010S L A Plastic 250ml HNO3 preserved A <2 2.3C Y Absent MCP-AS-6010S L A Plastic 250ml HNO3 preserved A <2 2.3C Y Absent MCP-AS-6010S L A Plastic 250ml HNO3 preserved A <2 2.3C Y Absent MCP-AS-6010S L A Plastic 250ml HNO3 preserved A <2 2.3C Y Absent MCP-AS-6010S L A Plastic 250ml HNO3 preserved A <2 2.3C Y Absent MCP-AS-6010S Container Comments Container ID Comments :39 Page 20 of 20
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