MedKoo Biosciences Product Quality Control Data

Transcription

1 Compound ID: GSK83875A-DMSO DMSO 4.3MHz Acquisition Parameters Date: 4-3-6T9:34: Pulse Sequence: zg3 Temperature: 96.7 C Number of Scans: 6 Frequency: 4.3 MHz Spectral Width: 8.8 Hz Nucleus: H Data Points: 3768 Relaxation Delay: s Pulse Width: 4.5 us F - Processing Parameters Data Points: DC:.5 LB:.3 Hz First Point:.5 FT: Hyper Quadrature Phase: Global f (ppm)

2 :5: / GSK83875A HPLC analysis ==== GSK83875A HPLC Report ==== Name : GSK83875A ID :GSK83875A Tray# : e : ul InjectionVail# Volum Information : 48 Data Filename : GSK83875A_7.lcd Method Filename : AB---MIN-45C.lcm Date Acquired : :35:4 Description : METHOD: - COLUMN: XBRIDGE 3.5UM.*5MM MOBILE: HO(.5%TFA)-ACN(.5%TFA) 7-8 MIN ACN FROM % TO % OVEN: 45C TOTAL FLOW RATE:.8ML/MIN -7 MIN ACN FROM % TO % <Chromatogram> GSK83875A.664 C:\acdata\43\4\LC-3\GSK83875A_7.lcd mv 5 Det.A Ch Det.A Ch / 4nm <Result> Area Height MedKoo Cat#: 4475 Name: GSK83875A CAS#: Lot#BBC436 Chemical Formula: C7H9FN8O3 Exact Mass: Molecular Weight: Area %.. PeakTable Detector A Ch 4nm Peak# Ret. Time.664 Total C:\acdata\43\4\LC-3\GSK83875A_7.lcd

3 GSK83875A HPLC analysis :5: / ==== GSK83875A HPLC Report ==== Information Name : GSK83875A ID : GSK83875ATray# : Injection Volume : ul : 48 Vail# Data Filename : GSK83875AA_7.lcd Method Filename : AB---MIN-45C.lcm Date Acquired : :35:4 Description : METHOD: - COLUMN: XBRIDGE 3.5UM.*5MM MOBILE: HO(.5%TFA)-ACN(.5%TFA) 7-8 MIN ACN FROM % TO % OVEN: 45C TOTAL FLOW RATE:.8ML/MIN -7 MIN ACN FROM % TO % <Chromatogram> B37-93A C:\acdata\43\4\LC-3\GSK83875A_7.lcd.664 Det.A Ch mv 7.5 Det.A Ch / 54nm <Result> PeakTable Area Height MedKoo Cat#: 4475 Name: GSK83875A CAS#: Lot#BBC436 Chemical Formula: C7H9FN8O3 Exact Mass: Molecular Weight: Area %.. Detector A Ch 54nm Peak# Ret. Time.664 Total C:\acdata\43\4\LC-3\GSK83875A_7.lcd

4 : C:\QC\GSK83875A.D : B-8A GSK83875A LCMS analysis : IMM-FTE : AGILENT LCMS E : P-B-5 : 4/3/4 :6:34 : :.8 µl : D:\CHEM3_\METHOD\P-.M : 4/3/4 :5:59 : IMM-FTE ( ) : C:\Chem3\\METHODS\DEF_LC.M : 6// 6:4:44 : Easy-Access Method: 'P-'. DAD A, Sig=54,6 Ref=off (C:\QC\GSK83875A.D) mau DAD C, Sig=4,6 Ref=off (C:\QC\GSK83875A.D) mau ES-API, Pos, Scan, Frag: MSD TIC, MS File (C:\QC\GSK83875A.D) ES-API, Pos, Scan, Frag: /3/4 :33:9.5 MedKoo Cat#: 4475 Name: GSK83875A CAS#: Lot#BBC436 Chemical Formula: C7H9FN8O MSD 533, EIC=53.7:533.7 (C:\QC\GSK83875A.D) /

5 : C:\QC\GSK83875A.D : B-8A : :. :. : DAD A, Sig=54,6 Ref=off # [] [] [mau*s] [mau] %. VV : : DAD C, Sig=4,6 Ref=off # [] [] [mau*s] [mau] %. VV : : MSD TIC, MS File # [] [] %.5 VV e7.3353e6. :.5377e7.3353e6 4: MSD 533, EIC=53.7:533.7 # [] [] %.43 BV e e5. :.8687e e5 *** *** 4/3/4 :33:9 /

6 79: MS Spectrum MS Spectrum *MSD SPC, time=.4 of C:\QC\GSK83875A.D ES-API, Pos, Scan, Frag: 7 Max: /3/4 :33:58 / m/z