Supporting Information. Synthesis of heteroglycoclusters by using orthogonal
|
|
|
- Anthony Nicholson
- 5 years ago
- Views:
Transcription
1 Supporting Information for Synthesis of heteroglycoclusters by using orthogonal chemoselective ligations Baptiste Thomas 1, Michele Fiore 1, Isabelle Bossu 1, Pascal Dumy 1 and Olivier Renaudet* 1,2 Address: 1 Département de Chimie Moléculaire, UMR-CNRS 5250 & ICMG FR 2607, Université Joseph Fourier, PB 53, Grenoble Cedex 9, France and 2 Institut Universitaire de France, 103 boulevard Saint-Michel, Paris, France. Olivier Renaudet* - olivier.renaudet@ujf-grenoble.fr *Corresponding author Crude RP-HPLC profiles and ESI-MS spectra for the heteroglycoclusters Table of contents: 1. Analytical data for compound 5-Man S3 2. Analytical data for compound 5-Fuc S4 3. Analytical data for compound 5-Lac S5 4. Analytical data for compound 6-Man/Fuc S6 5. Analytical data for compound 6-Man/Lac S7 6. Analytical data for compound 6-Fuc/Man S8 S9 7. Analytical data for compound 6-Fuc/Lac S10 8. Analytical data for compound 6-Lac/Man S11 S1
2 9. Analytical data for compound 6-Lac/Fuc S Analytical data for compound 7-Man S Analytical data for compound 7-Fuc S Analytical data for compound 7-Lac S Analytical data for compound 8-Man/Fuc S Analytical data for compound 8-Man/Lac S Analytical data for compound 8-Fuc/Man S18 S Analytical data for compound 8-Fuc/Lac S Analytical data for compound 8-Lac/Man S Analytical data for compound 8-Lac/Fuc S22 General details All chemical reagents were purchased from Aldrich (Saint Quentin Fallavier, France) or Acros (Noisy-Le-Grand, France) and were used without further purification. Protected amino acids and Fmoc-Gly-Sasrin resin were obtained from Advanced ChemTech Europe (Brussels, Belgium), Bachem Biochimie SARL (Voisins-Les-Bretonneux, France) and France Biochem S.A. (Meudon, France). PyBOP was purchased from France Biochem. Reaction progress was monitored by reverse-phase HPLC on Waters equipment by using C 18 columns. Analytical and preparative separation was carried out at 1.0 ml/min (EC 125/3 nucleosil C 18 ) and at 22 ml/min (VP 250/21 nucleosil C 18 ) with UV monitoring at 214 nm and 250 nm by using a linear A B gradient (buffer A: 0.09% CF 3 CO 2 H in water; buffer B: 0.09% CF 3 CO 2 H in 90% acetonitrile). Each glycopeptide was analyzed by mass spectrometry by using electrospray ionization on an Esquire Bruker Daltonics in positive mode. 1 H NMR and G-COSY were recorded in D 2 O at 400 MHz with a Bruker Avance 400 spectrometer. S2
3 1. Analytical data for compound 5-Man ESI-MS (positive mode): calcd for C 60 H 97 N 20 O , found: m/z [M + H] + S3
4 2. Analytical data for compound 5-Fuc ESI-MS (positive mode): calcd for C 60 H 96 N 20 O 22 Na , found: m/z [M + Na] + S4
5 3. Analytical data for compound 5-Lac ESI-MS (positive mode): calcd for C 72 H 117 N 20 O , found: m/z [M + H] + S5
6 4. Analytical data for compound 6-Man/Fuc ESI-MS (positive mode): calcd for C 78 H 124 N 20 O , found: m/z [M + H] + S6
7 5. Analytical data for compound 6-Man/Lac ESI-MS (positive mode): calcd for C 90 H 144 N 20 O , found: m/z [M + H] + S7
8 6. Analytical data for compound 6-Fuc/Man ESI-MS (positive mode): calcd for C 78 H 124 N 20 O , found: m/z [M + H] + S8
9 1 H NMR (D 2 O, 400 MHz) ppm (t1) G-COSY (D 2 O, 400 MHz) 8.0 ppm (t2) S9
10 7. Analytical data for compound 6-Fuc/Lac ESI-MS (positive mode): calcd for C 90 H 144 N 20 O , found: m/z [M + H] + S10
11 8. Analytical data for compound 6-Lac/Man ESI-MS (positive mode): calcd for C 90 H 145 N 20 O , found: m/z [M + H] + S11
12 9. Analytical data for compound 6-Lac/Fuc ESI-MS (positive mode): calcd for C 90 H 145 N 20 O , found: m/z [M + H] + S12
13 10. Analytical data for compound 7-Man ESI-MS (positive mode): calcd for C 52 H 84 N 21 O , found: m/z [M + H] + S13
14 11. Analytical data for compound 7-Fuc ESI-MS (positive mode): calcd for C 52 H 84 N 21 O , found: m/z [M + H] + S14
15 12. Analytical data for compound 7-Lac ESI-MS (positive mode): calcd for C 58 H 94 N 21 O , found: m/z [M + H] + S15
16 13. Analytical data for compound 8-Man/Fuc ESI-MS (positive mode): calcd for C 79 H 126 N 21 O , found: m/z [M + H] + S16
17 14. Analytical data for compound 8-Man/Lac ESI-MS (positive mode): calcd for C 97 H 156 N 21 O , found: m/z [M + H] + S17
18 15. Analytical data for compound 8-Fuc/Man ESI-MS (positive mode): calcd for C 79 H 126 N 21 O , found: m/z [M + H] + S18
19 1 H NMR (D 2 O, 400 MHz) ppm (t1) G-COSY (D 2 O, 400 MHz) 8.0 ppm (t2) S19
20 16. Analytical data for compound 8-Fuc/Lac ESI-MS (positive mode): calcd for C 97 H 156 N 21 O , found: m/z [M + H] + S20
21 17. Analytical data for compound 8-Lac/Man ESI-MS (positive mode): calcd for C 85 H 136 N 21 O , found: m/z [M + H] + S21
22 18. Analytical data for compound 8-Lac/Fuc ESI-MS (positive mode): calcd for C 85 H 136 N 21 O , found: m/z [M + H] + S22
Electronic Supplementary Information. Multivalency: Influence of the Residence Time and the Retraction Rate on. Rupture Forces Measured by AFM
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry B. This journal is The Royal Society of Chemistry 2015 Electronic Supplementary Information Multivalency: Influence of the Residence
Supplementary Information: Click-click chemistry on a peptidic scaffold for the easy access to tetrameric DNA structures
Supplementary Information: Click-click chemistry on a peptidic scaffold for the easy access to tetrameric DNA structures Romaric Bonnet, a Pierre Murat, a Nicolas Spinelli, a and Eric Defrancq* a a Département
Supplementary Information
Supplementary Information Efficient use of the Dmab Protecting Group: Applications for the Solid-Phase Synthesis of N- Linked Glycopeptides Trent Conroy, Katrina A. Jolliffe and Richard J. Payne* School
Study of On-Resin Convergent Synthesis of N-Linked. Glycopeptides Containing a Large High Mannose N- Linked Oligosaccharide
Supporting Information Study of On-Resin Convergent Synthesis of N-Linked Glycopeptides Containing a Large High Mannose N- Linked Oligosaccharide Rui Chen and Thomas J. Tolbert* Department of Chemistry,
Supplementary Materials for
advances.sciencemag.org/cgi/content/full/2/1/e1500678/dc1 Supplementary Materials for Chemical synthesis of erythropoietin glycoforms for insights into the relationship between glycosylation pattern and
Supporting Information
Supporting Information Wiley-VCH 2008 69451 Weinheim, Germany Chemoselective Peptide Cyclization via Induced Traceless Staudinger Ligation Rolf Kleineweischede, Christian P.R. Hackenberger* Institute for
Triptycene-Based Small Molecules Modulate (CAG) (CTG) Repeat Junctions
Electronic Supplementary Material (ESI) for Chemical Science. This journal is The Royal Society of Chemistry 2015 Triptycene-Based Small Molecules Modulate (CAG) (CTG) Repeat Junctions Stephanie A. Barros
A pillar[2]arene[3]hydroquinone which can self-assemble to a molecular zipper in the solid state
![A pillar[2]arene[3]hydroquinone which can self-assemble to a molecular zipper in the solid state](/thumbs/86/93673402.jpg "A pillar[2]arene[3]hydroquinone which can self-assemble to a molecular zipper in the solid state")
A pillar[2]arene[3]hydroquinone which can self-assemble to a molecular zipper in the solid state Mingguang Pan, Min Xue* Department of Chemistry, Zhejiang University, Hangzhou 310027, P. R. China Fax:
Microwave heating in peptide side chain modification via sulfhydryl reaction
Microwave heating in peptide side chain modification via sulfhydryl reaction E. Calce and S. De Luca* Institute of Biostructures and Bioimaging, National Research Council, 80134 Naples, Italy stefania.deluca@cnr.it
Solid Phase Peptide Synthesis (SPPS) and Solid Phase. Fragment Coupling (SPFC) Mediated by Isonitriles
Solid Phase Peptide Synthesis (SPPS) and Solid Phase Fragment Coupling (SPFC) Mediated by Isonitriles Ting Wang a and Samuel J. Danishefsky a,b,* alaboratory for Bioorganic Chemistry, Sloan- Kettering
Synthesis and Polymerization of Cyclobutenyl-Functionalized. Polylactide and Polycaprolactone: A Consecutive ROP/ROMP
Electronic Supplementary Material (ESI) for Polymer Chemistry. This journal is The Royal Society of Chemistry 2014 Supporting Information Synthesis and Polymerization of Cyclobutenyl-Functionalized Polylactide
Electronic Supplementary Information
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2015 Electronic Supplementary Information ovel pseudo[2]rotaxanes constructed by selfassembly of dibenzyl
Electronic Supporting Information for
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2015 Electronic Supporting Information for Rhodamine based Turn-On Fluorescent Probe for Pb(II)
Supporting Information
Electronic Supplementary Material (ESI) for Chemical Communications. This journal is The Royal Society of Chemistry 2015 Supporting Information A Dentritic -Galactosidase-Responsive Folate- Monomethylauristatin
Supporting Information
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2014 Supporting Information 1. General Information...S2 a. Materials b. HPLC
An Unusual Glycosylation Product from a Partially Protected Fucosyl Donor. under Silver Triflate activation conditions. Supporting information
An Unusual Glycosylation Product from a Partially Protected Fucosyl Donor under Silver Triflate activation conditions Robin Daly a and Eoin M. Scanlan* a e-mail: eoin.scanlan@tcd.ie a Trinity Biomedical
Supplementary information Oxaliplatin reacts with DMSO only in the presence of water
Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 2017 Supplementary information Oxaliplatin reacts with DMSO only in the presence of water
Electronic Supplementary Information. Table of Contents
Electronic Supplementary Information Examination of native chemical ligation using peptidyl prolyl thioester Takahiro Nakamura, Akira Shigenaga, Kohei Sato, Yusuke Tsuda, Ken Sakamoto, and Akira Otaka*
Supporting information
Supporting information Rhabdopeptide/Xenortide-like Peptides from Xenorhabdus innexi with Terminal Amines Showing Potent Anti-protozoal Activity Lei Zhao,, Marcel Kaiser,, Helge B. Bode *,, Molekulare
ph Switchable and Fluorescent Ratiometric Squarylium Indocyanine Dyes as Extremely Alkaline Sensors
ph Switchable and Fluorescent Ratiometric Squarylium Indocyanine Dyes as Extremely Alkaline Sensors Jie Li, Chendong Ji, Wantai Yang, Meizhen Yin* State Key Laboratory of Chemical Resource Engineering,
Toxins 2016, 8, 222; doi: /toxins
S1 of S8 Supplementary Materials: Mapping Protein Protein Interactions of the Resistance Related Bacterial Zeta Toxin Epsilon Antitoxin Complex (ε2ζ2) with High Affinity Peptide Ligands Using Fluorescence
SUPPORTING INFORMATION
SUPPORTING INFORMATION Phosphine-Mediated Disulfide Metathesis in Aqueous Media Rémi Caraballo, Morakot Sakulsombat, and Olof Ramström* KTH - Royal Institute of Technology, Department of Chemistry Teknikringen
A Stable Evans Blue Derived Exendin-4 peptide for Type 2 Diabetes Treatment
Supporting Information A Stable Evans Blue Derived Exendin-4 peptide for Type 2 Diabetes Treatment Yi Liu, Guohao Wang, Huimin Zhang, Ying Ma, Lixin Lang, Orit Jacobson, Dale O. Kiesewetter, Lei Zhu, Shi
Supporting Information for
Supporting Information for Ligand-directed chemistry of AMPA receptors confers live-cell fluorescent biosensors under natural habitat Shigeki Kiyonaka*, Seiji Sakamoto, Sho Wakayama, Yuma Morikawa, Muneo
Synthesis of cationic porphyrin modified amino. acids
Synthesis of cationic porphyrin modified amino acids Eric Biron and Normand Voyer* Département de chimie and CREFSIP, Faculté des sciences et de génie, Université Laval, Québec, Québec, Canada G1K 7P4
Supporting Information
Supporting Information Wiley-VCH 2007 69451 Weinheim, Germany Free Radical Based, Specific Desulfurization of Cysteine: A Powerful Advance in the Synthesis of Polypeptides and Glycopolypeptides Qian Wan
SUPPORTING INFORMATION TO: Oligonucleotide cyclization: The thiol-maleimide reaction revisited. Albert Sánchez, Enrique Pedroso, Anna Grandas*
SUPPRTIG IFRMATI T: ligonucleotide cyclization: The thiol-maleimide reaction revisited. Albert Sánchez, Enrique Pedroso, Anna Grandas* 1. General materials and methods, and abbreviations. 2. Solid phase
Enabling N-to-C Ser/Thr Ligation for Convergent Protein Synthesis via Combining Chemical Ligation Approaches. Supplementary Information
Enabling N-to-C Ser/Thr Ligation for Convergent Protein Synthesis via Combining Chemical Ligation Approaches Chi Lung Lee, Han Liu, Clarence T. T. Wong, Hoi Yee Chow and Xuechen Li* Department of Chemistry,
Application Note # FTMS-46 solarix XR: Analysis of Complex Mixtures
Application Note # FTMS-46 solarix XR: Analysis of Complex Mixtures Introduction Natural organic matter (NOM) as well as crude oil and crude oil fractions are very complex mixtures of organic compounds
MS/MS as an LC Detector for the Screening of Drugs and Their Metabolites in Race Horse Urine
Application Note: 346 MS/MS as an LC Detector for the Screening of Drugs and Their Metabolites in Race Horse Urine Gargi Choudhary and Diane Cho, Thermo Fisher Scientific, San Jose, CA Wayne Skinner and
New Solvent Grade Targeted for Trace Analysis by UHPLC-MS
New Solvent Grade Targeted for Trace Analysis by UHPLC-MS Subhra Bhattacharya, Deva H. Puranam, and Stephen C. Roemer Thermo Fisher Scientific Fisher Chemical, One Reagent Lane, Fair Lawn, NJ Material
Simple copper/tempo catalyzed aerobic dehydrogenation. of benzylic amines and anilines
Simple copper/tempo catalyzed aerobic dehydrogenation of benzylic amines and anilines Zhenzhong Hu and Francesca M. Kerton,* Department of Chemistry, Memorial University of Newfoundland, St. John s, NL,
Synthesis and Conformational Study of Water-Soluble, Rigid, Rod-like Oligopiperidines
Synthesis and Conformational Study of Water-Soluble, Rigid, Rod-like Oligopiperidines Vincent Semetey, Demetri Moustakas and George M. Whitesides* Department of Chemistry and Chemical Biology, Harvard
SUPPLEMENTARY INFORMATION
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 218 SUPPLEMENTARY INFORMATION Structural elucidation of major selective androgen
Supporting Information. for. Synthesis of dye/fluorescent functionalized. dendrons based on cyclotriphosphazene
Supporting Information for Synthesis of dye/fluorescent functionalized dendrons based on cyclotriphosphazene Aurélien Hameau 1,2, Sabine Fuchs 1,2, Régis Laurent 1,2, Jean-Pierre Majoral* 1,2 and Anne-Marie
Electronic Supplementary Information
Electronic Supplementary Information PHIP-Label: Parahydrogen-Induced Polarization in Propargylglycine-Containing Synthetic Oligopeptides Marco Körner, Grit Sauer, Andreas Heil, Daichi Nasu, Daniel Tietze,
Application of LC/Electrospray Ion Trap Mass Spectrometry for Identification and Quantification of Pesticides in Complex Matrices
Application ote #LCMS-2 esquire series Application of LC/Electrospray Ion Trap Mass Spectrometry for Identification and Quantification of Pesticides in Complex Matrices Introduction The simple monitoring
Supporting Information. Recyclable hypervalent-iodine-mediated solid-phase peptide
Supporting Information Recyclable hypervalent-iodine-mediated solid-phase peptide synthesis and cyclic peptide synthesis Dan Liu, Ya-Li Guo, Jin Qu and Chi Zhang* for Address: State Key Laboratory of Elemento-Organic
Development of a near-infrared fluorescent probe for monitoring hydrazine in serum and living cells
Supporting Information for Development of a near-infrared fluorescent probe for monitoring hydrazine in serum and living cells Sasa Zhu, Weiying Lin,* Lin Yuan State Key Laboratory of Chemo/Biosensing
Supporting Information for. Boronic Acid Functionalized Aza-Bodipy (azabdpba) based Fluorescence Optodes for the. analysis of Glucose in Whole Blood
Supporting Information for Boronic Acid Functionalized Aza-Bodipy (azabdpba) based Fluorescence Optodes for the analysis of Glucose in Whole Blood Yueling Liu, Jingwei Zhu, Yanmei Xu, Yu Qin*, Dechen Jiang*
Supporting Information
Supporting Information Cyclic Peptidyl Inhibitors against Human Peptidyl-Prolyl Isomerase Pin1 Tao Liu, Yu Liu, Hung-Ying Kao, *,, and Dehua Pei Table of Contents: Table S1. Structures of amino acid building
Electronic supplementary information Poly(vinyl)chloride supported palladium nanoparticles: Catalyst for rapid hydrogenation reactions
Electronic supplementary information Poly(vinyl)chloride supported palladium nanoparticles: Catalyst for rapid hydrogenation reactions Hosahalli P. Hemantha and Vommina V. Sureshbabu* Peptide Research
Synthesis of Sequence-Controlled Acrylate Oligomers. via Consecutive RAFT Monomers Additions
Supporting Information Synthesis of Sequence-Controlled Acrylate ligomers via Consecutive RAFT Monomers Additions Joke Vandenbergh a, Gunther Reekmans, b Peter Adriaensens b and Thomas Junkers a * a Polymer
A Self-Immolative Dendritic Glucuronide Prodrug of Doxorubicin
A Self-Immolative Dendritic Glucuronide Prodrug of Doxorubicin Grinda et al S1 Supporting Information A Self-Immolative Dendritic Glucuronide Prodrug of Doxorubicin Marion Grinda, a Jonathan Clarhaut,
Analysis of Pesticides (II) Metribuzin & their metabolites in Rice Jun Yonekubo, Nihon Waters, JAPAN
Waters Alliance LC/MS System Analytical Conditions Chromatograms Mass Spectra Calibration Quantitation Analysis of Pesticides (II) Metribuzin & their metabolites in Rice Jun Yonekubo,, JAPAN Key Words
Automated synthesis of backbone protected peptides
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2014 Electronic Supplementary Information Automated synthesis of backbone protected peptides Abu-Baker
Supporting Information
Supporting Information A single design strategy for dual sensitive ph probe with a suitable range to map ph in living cells Kang-Kang Yu, Ji-Ting Hou, Kun Li, * Qian Yao, Jin Yang, Ming-Yu Wu, Yong-Mei
Supplementary Information
Supplementary Information ne-step Synthesis of Novel Glycosyltransferase Inhibitors Andrew Evitt [a], Lauren M. Tedaldi [a] and Gerd K. Wagner* [a,b] [a] Institute of Pharmaceutical Science, School of
Development of a Cell-penetrating Peptide that Exhibits Responsive. Changes in its Secondary Structure in the Cellular Environment
Development of a Cell-penetrating Peptide that Exhibits Responsive Changes in its Secondary Structure in the Cellular Environment iroko Yamashita, 1 Takuma Kato, 2 Makoto ba, 2 Takashi Misawa, 1 Takayuki
A NOVEL METHOD OF M/Z DRIFT CORRECTION FOR OA-TOF MASS SPECTROMETERS BASED ON CONSTRUCTION OF LIBRARIES OF MATRIX COMPONENTS.
A NOVEL METHOD OF M/Z DRIFT CORRECTION FOR OA-TOF MASS SPECTROMETERS BASED ON CONSTRUCTION OF LIBRARIES OF MATRIX COMPONENTS. Martin R Green*, Keith Richardson, John Chipperfield, Nick Tomczyk, Martin
Time-of-Flight LC/MS Identification and Confirmation of a Kairomone in Daphnia magna Cultured Medium. Application. Authors. Abstract.
Time-of-Flight LC/MS Identification and Confirmation of a Kairomone in Daphnia magna Cultured Medium Application Natural Product Chemistry Authors Hideaki Uchida Agilent Technologies Japan, Ltd. Tokyo
p-toluenesulfonic Acid-Mediated 1,3-Dipolar Cycloaddition of
Supporting Information for: p-toluenesulfonic Acid-Mediated 1,3-Dipolar Cycloaddition of Nitroolefins with NaN 3 for Synthesis of 4-Aryl-NH-1,2,3-triazoles Xue-Jing Quan, Zhi-Hui Ren, Yao-Yu Wang, and
Electronic Supplementary Information (ESI)
Electronic Supplementary Information (ESI) Green and recyclable glycine nitrate (GlyN 3 ) ionic liquid triggered multicomponent Biginelli reaction for the efficient synthesis of dihydropyrimidinones. Nandini
Supporting Information. Copyright Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, 2008
Supporting Information Copyright Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, 2008 Copyright Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, 2008 Supporting Information for Efficient N-Terminal
Authors. Abstract. Introduction. Environmental
Determination of Ultratrace Amitrol in Water Samples by in situ Derivatization-Solid Phase Extraction-Liquid Chromatography-Mass Selective Detector Application Environmental Authors Gerd Vanhoenacker,
Supporting information
Supporting information Figure legends Supplementary Table 1. Specific product ions obtained from fragmentation of lithium adducts in the positive ion mode comparing the different positional isomers of
SUPPORTING INFORMATION:
1S SUPPORTING INFORMATION: The discovery of the once weekly glucagon like peptide 1 (GLP-1) analog semaglutide Jesper Lau*, Paw Bloch, Lauge Schäffer, Ingrid Pettersson, Jane Spetzler, Jacob Kofoed, Kjeld
Singlet oxygen photosensitisation by the fluorescent probe Singlet Oxygen Sensor Green
Singlet oxygen photosensitisation by the fluorescent probe Singlet Oxygen Sensor Green Xavier Ragàs, Ana Jiménez-Banzo, David Sánchez-García, Xavier Batllori and Santi Nonell* Grup d Enginyeria Molecular,
Supplementary Material (ESI) for Chemical Communications This journal is (c) The Royal Society of Chemistry 2008
Experimental Details Unless otherwise noted, all chemicals were purchased from Sigma-Aldrich Chemical Company and were used as received. 2-DOS and neamine were kindly provided by Dr. F. Huang. Paromamine
Supplementary Notes. HTS compatible FRET-based conformational sensors clarify membrane receptor activation
Supplementary otes TS compatible FRET-based conformational sensors clarify membrane receptor activation Pauline Scholler 1,2,3,4, David Moreno-Delgado 1,2,3, athalie Guillet-Lecat 1,2,3, Etienne Doumazane
An Electrophilic Reagent for the Synthesis of OCHFMe-containing Molecules
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2018 An Electrophilic Reagent for the Synthesis of OCHFMe-containing Molecules Elodie Carbonnel, a Xavier
Novel D-erythro N-Octanoyl Sphingosine Analogs As Chemo- and Endocrine. Resistant Breast Cancer Therapeutics
Page 11 of 32 Cancer Chemotherapy and Pharmacology Novel D-erythro N-Octanoyl Sphingosine Analogs As Chemo- and Endocrine Resistant Breast Cancer Therapeutics James W. Antoon, Jiawang Liu, Adharsh P. Ponnapakkam,
Manganese powder promoted highly efficient and selective synthesis of fullerene mono- and biscycloadducts at room temperature
Supplementary Information Manganese powder promoted highly efficient and selective synthesis of fullerene mono- and biscycloadducts at room temperature Weili Si 1, Xuan Zhang 1, Shirong Lu 1, Takeshi Yasuda
STANDARD OPERATING PROTOCOL (SOP)
1 STANDARD PERATING PRTCL (SP) Subject: To determine the Contents of isoflavone in soybean products by HPLC Analysis Project/Core No.: Core B Total 9 Pages SP No.: CB0102 Modified Date: 05/15/01 BTANICAL
L-Carnosine-Derived Fmoc-Tripeptides Forming ph- Sensitive and Proteolytically Stable Supramolecular
Supporting Information: L-Carnosine-Derived Fmoc-Tripeptides Forming ph- Sensitive and Proteolytically Stable Supramolecular Hydrogels Rita Das Mahapatra, a Joykrishna Dey* a, and Richard G. Weiss b a
Chukvelutins A-C, 16-norphragmalin limonoids with unprecedented skeletons from Chukrasia tabularis var. velutina
Chukvelutins A-C, 16-norphragmalin limonoids with unprecedented skeletons from Chukrasia tabularis var. velutina Jun Luo, Jun-Song Wang, Jian-Guang Luo, Xiao-Bing Wang, and Ling-Yi Kong* Department of
Supporting Information for:
Supporting Information for: Indocyanine-Based Activatable Fluorescence Turn-On Probe for -Glutamyltranspeptidase and Its Application to the Mouse Model of Colon Cancer Seokan Park, a Soo-Yeon Lim, a Sang
Catalytic decarboxylative alkylation of β-keto acids with sulfonamides via the cleavage of carbon nitrogen and carbon carbon bonds
Catalytic decarboxylative alkylation of β-keto acids with sulfonamides via the cleavage of carbon nitrogen and carbon carbon bonds Cui-Feng Yang, Jian-Yong Wang and Shi-Kai Tian* Joint Laboratory of Green
Directed flexibility: Self-assembly of a supramolecular tetrahedron
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2015 Electronic Supplemental Information Directed flexibility: Self-assembly of a supramolecular tetrahedron
SUPPORTING INFORMATION FOR:
SUPPORTING INFORMATION FOR: Metabolomics and lipidomics profiling of a combined mitochondrial plus endoplasmic reticulum fraction of human fibroblasts: a robust tool for clinical studies Charlotte Veyrat-Durebex
Supporting Information. 58 Pages. 6 Figures 4 Tables
Light-Source-Dependent Effects of Main Water Constituents on Photodegradation of Phenicol Antibiotics: Mechanism and Kinetics Linke Ge, Jingwen Chen, * Xianliang Qiao, Jing Lin, Xiyun Cai Key Laboratory
Supporting Information. Copyright Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, 2007
Supporting Information Copyright Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, 2007 Organocatalytic Asymmetric Sulfa-Michael Addition to α,β- Unsaturated Ketones Paolo Ricci, Armando Carlone, Giuseppe
Zinc Chloride Promoted Formal Oxidative Coupling of Aromatic Aldehydes and Isocyanides to α- Ketoamides
Supporting information for Zinc Chloride Promoted Formal xidative Coupling of Aromatic Aldehydes and Isocyanides to α- Ketoamides Marinus Bouma, Géraldine Masson* and Jieping Zhu* Institut de Chimie des
Supporting Information. First synthetic entry to the trimer stage of 5,6-dihydroxyindole polymerization: orthoalkynylaniline-based
Supporting Information First synthetic entry to the trimer stage of 5,6-dihydroxyindole polymerization: orthoalkynylaniline-based access to the missing 2,7 :2,7 -triindole Luigia Capelli, Paola Manini,*
Electronic Supplementary Information
Electronic Supplementary Material (ESI) for Chemical Communications. This journal is The Royal Society of Chemistry 2018 Electronic Supplementary Information A ratiometric fluorescence probe for peroxynitrite
Supporting Information
Supporting Information Visible-Light-Induced Specific Desulfurization of Cysteinyl Peptide and Glycopeptide in Aqueous Solution Xiao-Fei Gao, Jing-Jing Du, Zheng Liu and Jun Guo* Key Laboratory of Pesticide
2,6,9-Triazabicyclo[3.3.1]nonanes as overlooked. amino-modification products by acrolein
![2,6,9-Triazabicyclo[3.3.1]nonanes as overlooked. amino-modification products by acrolein](/thumbs/86/94743397.jpg "2,6,9-Triazabicyclo[3.3.1]nonanes as overlooked. amino-modification products by acrolein")
Supplementary Information 2,6,9-Triazabicyclo[3.3.1]nonanes as overlooked amino-modification products by acrolein Ayumi Tsutsui and Katsunori Tanaka* Biofunctional Synthetic Chemistry Laboratory, RIKEN
Supporting information
Supporting information Diversity Oriented Asymmetric Catalysis (DOAC): Stereochemically Divergent Synthesis of Thiochromanes Using an Imidazoline-aminophenol aminophenol (IAP)-Ni Catalyzed Michael/Henry
High-Throughput Analysis of Oligonucleotides using Automated Electrospray Ionization Mass Spectrometry
High-Throughput Analysis of Oligonucleotides using Automated Electrospray Ionization Mass Spectrometry Mark E. Hail 1, Brian Elliott 2, Kerry Nugent 3, Jeffrey L. Whitney 1, and David J. Detlefsen 1 1
Supporting Information
Supporting Information Wiley-VCH 2006 69451 Weinheim, Germany A Convergent Synthesis of N-Linked Glycopeptides Clyde M. Kaneshiro, Katja Michael* 1. LC-MS analysis of crude glycopeptide 16. 2. ESI-TOF
Thiol-Ene Photoimmobilization of Chymotrypsin on Polysiloxane Gels for Enzymatic Peptide Synthesis
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2018 Supporting information for: Thiol-Ene Photoimmobilization of Chymotrypsin on Polysiloxane Gels
Antoine Bouchoux, Pierre-Emerson Cayemitte, Julien Jardin, Geneviève Gésan-Guiziou, and Bernard Cabane
Biophysical Journal, Volume 96 Supplementary Material Casein Micelle Dispersions under Osmotic Stress Antoine Bouchoux, Pierre-Emerson Cayemitte, Julien Jardin, Geneviève Gésan-Guiziou, and Bernard Cabane
Comparison of mass spectrometers performances
Comparison of mass spectrometers performances Instrument Mass Mass Sensitivity resolution accuracy Quadrupole 1 x 10 3 0.1 Da* 0.5-1.0 pmol DE-MALDI 2 x 10 4 20 ppm 1-10 fmol peptide 1-5 pmol protein Ion
SUPPORTING INFORMATION. Transition metal-promoted synthesis of 2-aryl/heteroaryl-thioquinazoline: C-S
1 SUPPORTING INFORMATION Transition metal-promoted synthesis of 2-aryl/heteroaryl-thioquinazoline: C-S Bond formation by Chan-Lam Cross-Coupling Reaction SATYA KARUNA PULAKHANDAM a, NARESH KUMAR KATARI
Ynamides as racemization-free coupling reagents for amide and peptide synthesis
Ynamides as racemization-free coupling reagents for amide and peptide synthesis Long Hu, Silin Xu, Zhenguang Zhao, Yang Yang, Zhiyuan Peng, Ming Yang, Changliu Wang, Junfeng Zhao* Key Laboratory of Chemical
Automated Purification and Analytical Reinjection of a Small Molecule Drug, Probenecid, on a Gilson LC/MS Dual Function System
Automated Purification and Analytical Reinjection of a Small Molecule Drug, Probenecid, on a Gilson LC/MS Dual Function System Keywords Introduction Application Note PHA0413 High Pressure Liquid Chromatography
Supporting information for the article
Supporting information for the article S1 Exceptional behavior of Ni 2 O 2 species revealed by ESI-MS and MS/MS studies in solution. Application of superatomic core to facilitate new chemical transformations
Isolation, Identification and Characterization of Unknown Impurity in Fermentation Based Active Pharmaceutical Ingredient Lovastatin.
Research and Reviews: Journal of Pharmaceutical Analysis Isolation, Identification and Characterization of Unknown Impurity in Fermentation Based Active Pharmaceutical Ingredient Lovastatin. Chandrakant
Cytosolic targeting of macromolecules using a ph-dependent fusogenic peptide in. combination with cationic liposomes
Cytosolic targeting of macromolecules using a ph-dependent fusogenic peptide in combination with cationic liposomes Sachiko Kobayashi, Ikuhiko Nakase, Noriko Kawabata, Hao-hsin Yu, Silvia Pujals, Miki
Convenient Synthesis of Thiohydantoins, Imidazole-2-thiones and Imidazo
Convenient Synthesis of Thiohydantoins, Imidazole-2-thiones and Imidazo [2,1-b]thiazol-4-iums from Polymer-supported -Acylamino Ketones Petra Králová a, Michal Maloň b, Hiroyuki Koshino c and Miroslav
An Investigative Study of Reactions Involving Glucosinolates and Isothiocyanates
An Investigative Study of Reactions Involving Glucosinolates and Isothiocyanates Alzea Chrisel H. Alea 1, Diane Elaine T. Co 2 and Marissa G Noel 3* 1,2,3Chemistry Department, De La Salle University, 2401
2D-LC as an Automated Desalting Tool for MSD Analysis
2D-LC as an Automated Desalting Tool for MSD Analysis Direct Mass Selective Detection of a Pharmaceutical Peptide from an MS-Incompatible USP Method Application Note Biologics and Biosimilars Author Sonja
Supporting Information
Supporting Information B(C 6 F 5 ) 3 -catalyzed Regioselective Deuteration of Electronrich Aromatic and Heteroaromatic compounds Wu Li, Ming-Ming Wang, Yuya Hu and Thomas Werner* Leibniz-Institute of Catalysis
UniChemo Protection: A Novel Concept For Chemical Synthesis. Les P. Miranda and Morten Meldal
Copyright WILEY-VCH Verlag GmbH, D-69451 Weinheim, 2001. Supporting Information for Angew. Chem. Int. Ed. Z17269 UniChemo Protection: A ovel Concept For Chemical Synthesis Les P. Miranda and Morten Meldal
Site-specific traceless coupling of potent cytotoxic drugs to recombinant antibodies for pharmacodelivery.
S1 Site-specific traceless coupling of potent cytotoxic drugs to recombinant antibodies for pharmacodelivery. Giulio Casi, Nicolas Huguenin-Dezot, Kathrin Zuberbühler, Jörg Scheuermann & Dario Neri,* Philochem
Supporting Information
Supporting Information Developing novel activity-based fluorescent probes that target different classes of proteases Qing Zhu, Aparna Girish, Souvik Chattopadhaya and Shao Q Yao * Departments of Chemistry
Supporting Information. Nitrodibenzofuran: a One- and Two-Photon Sensitive Protecting Group that is Superior to
Supporting Information Nitrodibenzofuran: a One- and Two-Photon Sensitive Protecting Group that is Superior to Brominated Hydroxycoumarin for Thiol Caging in Peptides M. Mohsen Mahmoodi, Daniel Abate-Pella,
Key Words: Brassica oleraceae, glucosinolate, liquid chromatography mass spectrometry, FNH-I-003
IDENTIFICATION OF MAJOR GLUCOSINOLATES IN BROCCOLI (Brassica oleracea var. italica) BY LIQUID CHROMATOGRAPHY MASS SPECTROMETRY (LC-MS) AND DETERMINATION OF ANTICANCER PROPERTIES OF BROCCOLI EXTRACTS Carlos
Supporting Information
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2018 Supporting Information Facile Three-Step Synthesis and Photophysical Properties of [8]-, [9]-,
Allenylphosphine oxides as simple scaffolds for. phosphinoylindoles and phosphinoylisocoumarins
Supporting Information for Allenylphosphine oxides as simple scaffolds for phosphinoylindoles and phosphinoylisocoumarins G. Gangadhararao, Ramesh Kotikalapudi, M. Nagarjuna Reddy and K. C. Kumara Swamy*