Test Report No.: GZHG CW Date: Feb 11, 2015 Page 1 of 9
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1 Test Report No.: GZHG CW Date: Feb 11, 2015 Page 1 of 9 ANDRIOLO SRL VIA VECCHIA MILANESE, 2 VENEGONO INFERIORE The following sample(s) was/were submitted and identified on behalf of the client as: Sample Description : SPORT BOTTLE SGS Ref No. : CANHG Style / Item No. : FOX 500C P.O. / Ref. No. : ANNUAL TEST Manufacturer : ANDRIOLO SRL Country of Destination : EU Sample Receiving Date : Feb 05, 2015 Test Performing Date : Feb 05, 2015 to Feb 11, 2015 Result Summary : Test Requested Commission Regulation (EU) No 10/2011 of 14 January 2011 with amendments Overall migration Council of Europe Resolution AP (2004) 4 Overall migration German Food, Articles of Daily Use and Feed Code of September 1, 2005 (LFGB), Section 30 & 31 with amendments Sensorial examination odour and taste test Council of Europe Resolution AP (2004) 4 Specific Migration of Primary Aromatic Amine Commission Regulation (EU) No 10/2011 of 14 January 2011 with amendments Specific Migration of Heavy Metal Council of Europe Resolution AP (2004) 4 Specific Migration of N-Nitrosamines and N-Nitrosatable substances Verification for label claim validity - Bisphenol A free by Total Content of Bisphenol A Signed for and on behalf of Guangzhou Branch, SGS-CSTC Ltd. Conclusion Johnny Lee Approved Signatory
2 Test Report No.: GZHG CW Date: Feb 11, 2015 Page 2 of 9 Test Results : Test Part Description : Specimen No. SGS Sample ID Description Material (claimed by the client) SN1 CAN Blue plastic lid PP SN2 CAN Translucent rubber rubber SN3 CAN Sport bottle whole product SN4 CAN White plastic bottle PE Commission Regulation (EU) No 10/2011 of 14 January 2011 with amendments Overall migration As specified by client, to determine Overall migration from plastic used in contact with food for compliance with Commission Regulation (EU) No 10/2011 of 14 January 2011 with amendments. Annex V for selection of condition and EN :2002 for selection of test methods; or EN :2002 aqueous food simulants by total immersion method; or EN :2002 aqueous food simulants by article filling method; Simulant Used Time Temperature Max. Permissible Result of 001 Limit Overall Migration 10% Ethanol (V/V) Aqueous 2.0hr(s) 70 10mg/dm² <3.0mg/dm² 3% Acetic Acid (W/V) 2.0hr(s) 70 10mg/dm² <3.0mg/dm² Aqueous 50% Ethanol (V/V) Aqueous 2.0hr(s) 70 10mg/dm² <3.0mg/dm² Simulant Used Time Temperature Max. Permissible Result of 004 Limit Overall Migration 10% Ethanol (V/V) Aqueous 2.0hr(s) 70 10mg/dm² <3.0mg/dm² 3% Acetic Acid (W/V) 2.0hr(s) 70 10mg/dm² <3.0mg/dm² Aqueous 50% Ethanol (V/V) Aqueous 2.0hr(s) 70 10mg/dm² <3.0mg/dm² 1. mg/dm² =milligram per square decimeter
3 Test Report No.: GZHG CW Date: Feb 11, 2015 Page 3 of 9 2. C = degree Celsius 3. Permissible Limit is according to Commission Regulation (EU) No 10/2011 of 14 January 2011 with amendments. 4. The test data is obtained by considering the articles intended for repeated use as per described in Commission Regulation (EU) No 10/2011 of 14 January 2011 Annex V. Report the 3rd extractive result. 5.Result(s) of 001 was/were calculated based on the total contact surface of the sealing article and sealed container provided by client. Council of Europe Resolution AP (2004) 4 Overall migration As specified by client, to determine Overall migration from rubber used in contact with food for compliance with Council of Europe Resolution AP (2004) 4. Annex V for selection of condition and EN :2002 for selection of test methods; or EN :2002 aqueous food simulants by total immersion method; Simulant Used Time Temperature Max. Permissible Result of 002 Limit Overall Migration 10% Ethanol (V/V) Aqueous 2.0hr(s) 70 60mg/kg <20mg/kg 50% Ethanol (V/V) Aqueous 2.0hr(s) 70 60mg/kg <20mg/kg 3% Acetic Acid (W/V) 2.0hr(s) 70 60mg/kg <20mg/kg Aqueous 1. mg/kg = milligram per kilogram of foodstuff in contact with 2. C = degree Celsius 3. Permissible Limit is according to Council of Europe Resolution AP (2004) The test data is obtained by considering the articles intended for repeated use as per described in Commission Regulation (EU) No 10/2011 of 14 January 2011 Annex V. Report the 3rd extractive result. 5.Test sample was applied to container with capacity of 0.58 L. German Food, Articles of Daily Use and Feed Code of September 1, 2005 (LFGB), Section 30 & 31 with amendments Sensorial examination odour and taste test As specified by client, to determine Sensorial examination odour and taste from the submitted sample used in contact with food for compliance with German Food, Articles of Daily Use and Feed Code of September 1, 2005 (LFGB), Section 30 & 31 with amendments.
4 Test Report No.: GZHG CW Date: Feb 11, 2015 Page 4 of 9 With reference to DIN10955:2004. Test condition: hr(s); Test media: Distilled water; No.of panelist: 6 Test Item(s) Limit 003 Sensorial examination odour (Point scale) Sensorial examination taste (Point scale) Scale evaluation: 0: No perceptible odour 1: Odour just perceptible (still difficult to define) 2: Moderate odour 3: Moderately strong odour 4: Strong odour Council of Europe Resolution AP (2004) 4 Specific Migration of Primary Aromatic Amine As specified by client, to determine Specific Migration of Primary Aromatic Amine from rubber used in contact with food for compliance with Council of Europe Resolution AP (2004) 4. Annex V for selection of condition and EN :2004 for selection of test method and BfR Recommendation XXI. Analysis was performed by UV-Vis. Sample 002 Simulant Used : 3% Acetic Acid (W/V) Aqueous Test Condition : hr(s) Test Item(s) Max. Permissible Unit MDL Test result Limit Specific migration of primary aromatic amine 0.01 mg/kg 0.01 ND 1. mg/kg = milligram per kilogram of foodstuff in contact with 2. C = degree Celsius 3. MDL=Method Detection Limit 4. ND = Not Detected(less than MDL) 5. Permissible Limit is according to Council of Europe Resolution AP (2004) 4.
5 Test Report No.: GZHG CW Date: Feb 11, 2015 Page 5 of 9 Commission Regulation (EU) No 10/2011 of 14 January 2011 with amendments Specific Migration of Heavy Metal As specified by client, to determine Specific Migration of Heavy Metal from plastic used in contact with food for compliance with Commission Regulation (EU) No 10/2011 of 14 January 2011with amendments. Annex V for selection of condition and EN :2004 for selection of test method, analysis was performed by ICP-OES. Sample 001 Simulant Used : 3% Acetic Acid (W/V) Aqueous Test Condition : hr(s) Test Item(s) Max. Permissible Unit MDL Test result Limit Extractable Barium 1 mg/kg 0.25 ND Extractable Cobalt 0.05 mg/kg 0.01 ND Extractable Copper 5 mg/kg 0.25 ND Extractable Iron 48 mg/kg 0.25 ND Extractable Lithium 0.6 mg/kg 0.5 ND Extractable Manganese 0.6 mg/kg 0.25 ND Extractable Zinc 25 mg/kg 0.5 ND Sample 004 Simulant Used : 3% Acetic Acid (W/V) Aqueous Test Condition : hr(s) Test Item(s) Max. Permissible Unit MDL Test result Limit Extractable Barium 1 mg/kg 0.25 ND Extractable Cobalt 0.05 mg/kg 0.01 ND Extractable Copper 5 mg/kg 0.25 ND Extractable Iron 48 mg/kg 0.25 ND Extractable Lithium 0.6 mg/kg 0.5 ND Extractable Manganese 0.6 mg/kg 0.25 ND Extractable Zinc 25 mg/kg 0.5 ND
6 Test Report No.: GZHG CW Date: Feb 11, 2015 Page 6 of 9 1. mg/kg = milligram per kilogram of foodstuff in contact with 2. C = degree Celsius 3. MDL=Method Detection Limit 4. ND= Not Detected(less than MDL) 5. Permissible Limit is according to Commission Regulation (EU) No 10/2011 of 14 January 2011 with amendments. 6. The test data is obtained by considering the articles intended for repeated use as per described in Commission Regulation (EU) No 10/2011 of 14 January 2011 Annex V. Report the 3rd extractive result. Council of Europe Resolution AP (2004) 4 Specific Migration of N-Nitrosamines and N-Nitrosatable substances As specified by client, to determine Specific Migration of N-Nitrosamines and N-Nitrosatable substances from rubber used in contact with food for compliance with Council of Europe Resolution AP (2004) 4. Annex V for selection of condition and EN :2004 for selection of test method, analysis was performed by GC-NPD & GC-MS. Sample 002 Simulant Used : 3% Acetic acid (W/V) aqueous solution Test Condition : hr(s) Test Item(s) Max. Permissible Unit MDL Test result Limit Specific migration of N-Nitrosamines 0.01 mg/kg ND Specific migration of N-Nitrosatable substances 0.1 mg/kg 0.10 ND 1. N-Nitrosamines tested : N-nitrosondimethylamine (NDMA), N-nitrosodiethylamine (NDEA), N-nitrosodipropylamine (NDPA), N-nitrosodibutylamine (NDBA), N-nitrosopiperdine (NPIP), N-nitrosopyrrolidine (NPYR), N-nitrosomorpholine (NMOR), N-nitrosodibenzylamine (NDBzA), N-nitroso-N-methyl-N-phenylamine (NMPhA), N-nitroso-N-ethyl-N-phenylamine (NEPhA) and N- nitrosodisonylamine (NDiNA). 2. mg/kg = milligram per kilogram 3. MDL=Method Detection Limit 4. ND = Not Detected(less than MDL) 5. Permissible Limit is according to Council of Europe Resolution AP (2004) 4.
7 Test Report No.: GZHG CW Date: Feb 11, 2015 Page 7 of 9 Verification for label claim validity - Bisphenol A free by Total Content of Bisphenol A As specified by client, to determine Total Content of Bisphenol A from submitted sample(s) used in contact with food for Verification for label claim validity. With reference to Part Ⅱ Section D2 of Testing Methods for Foodstuffs, Implements, Containers and Packaging, Toys, Detergents, JETRO, Japan External Trade Organization, 2009, analysis was performed by HPLC-MS. Test Item(s) Unit MDL Total content of Bisphenol A mg/kg 0.1 ND ND ND 1. mg/kg = milligram per kilogram 2. MDL=Method Detection Limit 3. ND= Not Detected(less than MDL) Remark: 1. Test condition & simulant were specified by client. 2. Results and photo(s) of 004 in this report refer to test report CANHG Sample photo: CAN
8 Test Report No.: GZHG CW Date: Feb 11, 2015 Page 8 of 9 CAN CAN
9 Test Report No.: GZHG CW Date: Feb 11, 2015 Page 9 of 9 CAN ***End of Report***
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