GC/MS BATCH NUMBER: J10101
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1 GC/MS BATCH NUMBER: J10101 ESSENTIAL OIL: JASMINE ABSOLUTE BOTANICAL NAME: JASMINUM SAMBAC ORIGIN: EGYPT KEY CONSTITUENTS PRESENT IN THIS BATCH OF JASMINE ABSOLUTE OIL (E,E)-α-FARNESENE 13.9 LINALOOL 9.5 % Comments from Robert Tisserand: A rich absolute with relatively high indole and linalool, making this a sedative jasmine. The constituents are within expected ranges for Egyptian Jasminum sambac oil. BENZYL ACETATE 8.4 INDOLE 7.3 GERMACRENE D-4-OL 6.1 CIS-9-TRICOSENE 5.8 (Z)-3-HEXENYL BENZOATE 5.5 METHYL ANTHRANILATE 4.4 METHYL α-linolenate 3.2 BENZYL ALCOHOL 2.8 SQUALENE 1.9 (Z)-3-HEXENYL ACETATE 1.7 PHENYLMETHYL α-linolenate 1.6 LINOLENIC ACID 1.6 (E,E)-GERANYL LINALOOL 1.4 PALMITIC ACID 1.2 PHENYLACETONITRILE 1.1 α-tocopherol nd St S. Twin Falls, ID * * planttherapy.com facebook.com/planttherapy * essentialoilblogging.com
2 Date : October 21, 2015 SAMPLE IDENTIFICATION Internal code : 15J20-PTH12-1-LC Customer identification : Jasmine Absolute - Egypt - J10101R Type : Absolute Source : Jasminum sambac Customer : Plant Therapy ANALYSIS Method : PC-PA E06, "Analysis of the composition of a liquid essential oil by GC-FID" (in French). Identifications double-checked by GC-MS. Analyst : Alexis St-Gelais, M. Sc. Analysis date : Page 1 of 6
3 Absolute, Jasminum sambac Customer Identification: Report prepared for IDENTIFIED COMPOUNDS Identification Column: BP5 Column: WAX R.T. R.I. % % R.I. R.T. Molecular Class Ethanol Aliphatic alcohol cis-hex-3-en-1-ol Aliphatic alcohol trans-hex-2-en-1-ol Aliphatic alcohol Hexanol Aliphatic alcohol cis-hex-3-en-1-yl acetate Aliphatic ester Hexyl acetate Aliphatic ester trans-hex-2-en-1-yl acetate Aliphatic ester trans-β-ocimene Monoterpene Benzyl alcohol * Simple phenolic cis-linalool oxide (fur.) Monoterp. alcohol trans-linalool oxide (fur.) * Monoterp. alcohol Methyl benzoate Phenolic ester Linalool Monoterp. alcohol Phenylethyl alcohol * Simple phenolic Phenylacetonitrile [1.74] * Simple phenolic Benzyl acetate Phenolic ester Ethyl benzoate 7.42* Phenolic ester Unknown (m/z = 43, 69 (50), 7.42* 1178 [0.95] (40), 41 (31), 56 (27) (1)... ) cis-linalool oxide (pyr.) Monoterp. alcohol cis-hex-3-en-1-yl butyrate [0.35] * Alihatic ester Methyl salicylate Phenolic ester cis-hex-3-en-1-yl Aliphatic ester isovalerate Phenylethyl acetate Phenolic ester Geraniol [3.07] * Monoterp. alcohol Chavicol Phenylpropanoid Indole 12.43* * Indole 1-Nitro-2-phenylethane 12.43* 1314 [4.37] Simple phenolic Bicycloelemene 12.43* 1314 [4.37] Sesquiterpene (E)-Cinnamyl alcohol Phenylpropanoid Methyl anthranilate 14.44* Phenolic ester α-copaene 14.44* 1350 [4.44] Sesquiterpene β-elemene Sesquiterpene Methyl (E)-cinnamate Phenylpropanoid ester (Z)-Jasmone Jasmonate β-caryophyllene Sesquiterpene Page 2 of 6
4 Absolute, Jasminum sambac Customer Identification: Report prepared for α-humulene Sesquiterpene Germacrene D 21.63* Sesquiterpene (E)-Cinnamyl acetate 21.63* 1457 [0.51] Phenylpropanoid ester Bicyclogermacrene Sesquiterpene (Z,E)-α-Farnesene * Sesquiterpene γ-cadinene Sesquiterpene (E,E)-α-Farnesene 25.35* Sesquiterpene δ-cadinene 25.35* 1505 [13.88] [0.29] * Sesquiterpene Germacrene D-4-ol 30.28* * Sesquiterp. alcohol (E)-Nerolidol 30.28* 1564 [6.45] Sesquiterp. alcohol (Z)-Hex-3-en-1-yl benzoate Phenolic ester Hexyl benzoate Phenolic ester (E)-Hex-2-en-1-yl benzoate Phenolic ester Methyl N-acetylanthranilate Phenolic ester τ-cadinol Sesquiterp. alcohol τ-muurolol Sesquiterp. alcohol α-cadinol Sesquiterp. alcohol Methyl (Z)-jasmonate Jasmonate (2E,6E)-Farnesol * Sesquiterp. alcohol Benzyl ester (m/z = 105, Phenolic ester (43), 1652 (20) (5) ? (t)) Benzyl benzoate * Phenolic ester (2E,6E)-Farnesyl acetate Sesquiterp. ester Phenylethyl benzoate Phenolic ester Methyl palmitate Fatty acid ester Palmitic acid Fatty acid (E,E)-Geranyllinalool Diterp. alcohol Methyl linoleate Fatty acid ester Heneicosane Alkane Methyl α-linolenate [3.26] * Fatty acid ester Methyl stearate Fatty acid ester Linoleic acid 50.69* Fatty acid Linolenic acid 50.69* 2165 [2.45] Fatty acid cis-9-tricosene [10.29] * Alkene trans-11-tricosene Alkene Tricosane [0.27] * Alkane Behenic alcohol Aliphatic alcohol Phenylmethyl palmitate Fatty acid ester Phenylmethyl α-linolenate Fatty acid ester Squalene Triterpene 2,3-Oxidosqualene Triterp. ether α-tocopherol Tocopherol Dimethyl anthranilate [6.10] * Phenolic ester Total identified 87.33% 86.81% Page 3 of 6
5 Absolute, Jasminum sambac Customer Identification: Report prepared for *: Two or more compounds are coeluting on this column [xx]: Duplicate percentage due to coelutions, not taken account in the identified total Note: no correction factor was applied OTHER DATA Physical aspect : Bright yellow-orange liquid Refractive index : ± (20 C) CONCLUSION No adulterant, contaminant or diluent were detected using this method. To the best of our knowledge and according to our retention indexes, the hex-3-en-1-yl benzoate isomer is (Z), not (E). Checked and approved by : Alexis St-Gelais, M. Sc., chimiste Note: This report may not be published, including online, without the written consent from Laboratoire PhytoChemia. This report is digitally signed, it is only considered valid if the digital signature is intact. Page 4 of 6
6 Page 5 of 6 Absolute, Jasminum sambac Customer Identification: Report prepared for
7 Page 6 of 6 Absolute, Jasminum sambac Customer Identification: Report prepared for
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