Research in Food Science and FormulaNon : From raw material to final product

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1 Research in Food Science and FormulaNon : From raw material to final product Christophe BLECKER Full Professor, University of Liège Gembloux Agro-Bio Tech Beijing, May 23th 2017

2 University of Liège Gembloux Agro-Bio Tech Department AgroBioChem Food Science and FormulaNon ANsa

3 Human forces Academics : - Dr Ir Christophe Blecker - Dr Ir Sabine Danthine and a team of MSc. and Ph.D graduate students, postdoctoral fellows, research associates and technicians make up the lab

4 FoodIsLife R&D plaworm in food science and biotechnology

5 FoodIsLife : R&D pla8orm - ExperNse in the area of food science and biotechnology - CuXng-edge lab-scale equipments - Access to pilot-scale equipments - Reinforcement of the links between university and private partners - PromoNon of the Walloon expernse in food science research at an nanonal and internanonal level

6 Skills - Research acnvines in food science, microbial biotechnology, biological chemistry Equipments - Lab equipments - Pilot scale equipements : for the producnon of small quannnes (as test sample) to medium quannnes (10 Kg for preproducnon to several hundreds of Kg for scaling-up demonstranon)

7 Cracking and valorisanon of bioproducts (bioreffinery concept) Downstream processing Oils and fat processing Industrial biotechnology Bioreactor (medium capacity) Industrial biotechnology Bioreactor (large capacity)

8 Cracking Use of physical treatments By-products valorizanon ExtracNon TransformaNons TechnofuncBonal properbes Physical or enzymanc modificanons FormulaBon engineering Study of interacnons between ingredients Food model development Full characterisanon (physico-chemical and sensory analysis) Final products

9 Examples of acbvibes carried out in the field of cracking and valorizabon of bioproducts Cracking of agricultural raw materials allows us to produce new ingredients Cracking can lead to clean label ingredients and provide added values to agricultural producnons

10 Cracking : what does it mean? A long tradibon of by-product valorizabon exists in Gembloux : more than 20 years! (different fields)

11 Cracking in Gembloux Agro-Bio Tech Some examples of starnng raw materials - Milk - Egg yolk - Insects - Cereals (wheat, spelt, oats) - Sugar beet leaves - Date - Flax seed - Pea

12 Milk fracbonabon Proteins - Proteose-peptone fracnon Lipids - Anhydrous milk fat - Polar lipids

13 Date fracbonabon Seed (pit) - Oil, phenolic compounds Flesh - Dietary fiber, pecnn - Proteins

14 Industrial fracbonabon of pea Dry Pea Seeds Grinding Bagging External Pea Fibre Cleaning ClassificaNon Dehulling Grinding ExtracNon Sieving DecantaNon PasteurizaNon UltrafiltraNon ConcentraNon Drying Bagging Pea Protein Isolate PurificaNon ConcentraNon Drying Bagging NaBve Starch Heat treatment ConcentraNon Drying Bagging Internal Pea Fibre Grinding Instant Starch Micronized Fibre

15 Industrial valorisabon of our research

16 Product characterizabon Techno funcnonal propernes Physical state of powders Interfacial propernes Physico-chemical propernes of lipids

17 Equipment (1) Interfacial properbes AdsorpNon kinencs, monolayers, CMC Spinning drop Bubble pressure Hanging drop Tensiometer Langmuir film wage

18 Equipment (2) - Emulsions, foams, Turbiscan Foam scan

19 Equipment (3) Rheology, texture analysis, parncule/globule sizer, Master sizer Rheometer Texturometer Beckman coulter-delsa Nano

20 Microscopy: Equipment (4)

21 Equipment (5) Thermal properbes: MDSC Q1000 TGA MDSC TA2920

22 Equipment (6) Oils & fats : Megler (CP-DP- ) P NMR Rancimat

23 Equipment (7) Oils & fats : polymorphism XRD with controlled temperature

24 From Fundamental research To ApplicaNons Example : MFGM Fundamental understanding : last MFGM models (2000 & 2010) Scaling-up (industrial level) By-product valorizanon (bugermilk) FormulaNon of new products Patent : Dalemans D., Blecker C., Bodson P., Danthine S., Deroanne C., Paquot M. (2008). Milk ingredient enriched in polar lipids and uses thereof. InternaNonal Patent, WO/ 2008/ Specific research towards purificanon & fracnonanon to get new products with added value

25 «ExtracNon, transformanon, valorizanon and unlizanon of lipids (& by or co-products)» Fundamental understanding of lipid crystallizanon (phase behavior diagrams ) Fundamental understanding of lipid networks building ElucidaNon of lipid structures for diversified physical funcnonalines Development and/or improvement of som modificanon processes (physical/enzymanc) directed towards modulanon of lipids funcnonality Studies of extracnon and refining pracnces (with valorizanon of co-products ). PreservaNve strategies (oxidanon) Extrac/on Refining Thermal proper/es Crystalliza/on Fat modifica/ons Polymorphism d=4,57394 B d=3,69273 d=4,50085 d=3,65550 d=3, d=3,73653 Lin (Counts) d=5, Theta - Scale sabine.danthine@ulg.ac.be

26 Example : Puff pastry margarines

27 Conclusion We can do : - Food technology - Pilot-scale development - FormulaNon - Physico-chemical analysis We can not do : - Chemical analysis (chromatography) - NutriNon

28 Link to full publicanons report hgp://orbi.ulg.ac.be/orbi-report?query=%28%28uid %3Au300145%29%29&model=a&format=apa&data=metric&data=metri cs&data=pr&sort_by0=1&order0=desc&sort_by1=3&order1=asc&sort _by2=2&order2=asc&output=html&language=fr&ntle=publicanons+et +communicanons+de+christophe+blecker+%5bu300145%5d

29 We are open to internabonal collaborabons PublicaBons this year with University of Ghent, Catholic University of Leuven, University of Sfax, University of Tunis, University of Cluj-Napoca

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