1 st Workshop on Multi-User-Equipment and Facilities High Resolution Mass Spectrometry Lab IQSC-USP-São Carlos Principal Investigator and Presenter: Emanuel Carrilho
HRMS LTQ Orbitrap Velos
EMU PROC No. 2009/54040-8 http://lcms.iqsc.usp.br/about/ http://lcms.iqsc.usp.br http://lcms.iqsc.usp.br/eventos/ http://lcms.iqsc.usp.br/infraestrutura/
Original Proponents - IQSC/USP Coordenador: Emanuel Carrilho Pesquisadores Associados: André Luiz Meleiro Porto Antonio Carlos Bender Burtoloso Eny Maria Vieira Daniel Rodrigues Cardoso Júlio Cesar Borges Pesquisadores Colaboradores: Agnieszka Joanna Pawlicka Maule Benedito dos Santos Lima Neto Douglas Wagner Franco Janete Harumi Yariwake Marcos Roberto de Vasconcelos Lanza Roberto Gomes de Souza Berlinck Ubirajara Pereira Rodrigues Filho Vitor Marcelo DeMlon
Steering Committee Emanuel Carrilho (IQSC) Edson Rodrigues Filho (UFSCar) Daniel Rodrigues Cardoso (IQSC)
USER s Committee Antonio Carlos Bender Burtoloso (IQSC) João Batista Fernandes (UFSCar) Quézia Bezerra Cass (UFSCar) Janete Harumi Yariwake (IQSC) Maria de Fátima G. F. da Silva (UFSCar) Regina Vincenzi Oliveira (UFSCar)
High Resolution Mass Spectrometer LTQ Orbitrap Velos Ionization sources: electrospray ionization (ESI) nanoelectrospray (nanoesi) atmospheric pressure chemical ionization (APCI) desorption electrospray ionization (DESI) Separation units: ultra-performance liquid chromatography (UPLC) Accela High Speed LC (Thermo Scientifc) nano-lc EASY-nLc II (Thermo Scientific) Sample Prep Accessories: Akta Prime GE (preparative scale sample prep) Liophilizer Alpha 2-4 LDplus Christ Concentrator model RVC 2-33IR CD Plus Christ.
Location & Installations
Location & Installations
Location & Installations
Location & Installations
Location & Installations
Equipment
Supplies
Accessories @ UFSCar
Accessories @ UFSCar
Separations Units
Separations Units
Ionization Sources
Ionization Sources - DESI
Ionization Sources - NanoMate CAPES - Pro-Equipamentos
RT#Expenditure# training' so*ware' reagent' infra' consumables' accessory'
Scheduling & Usage!! 5!! 10!! 15!! 20!! 25!! 30!! 35!! Taicia!Pacheco!Fill!/!Edson!Rodrigues!Filho!UFSCar! Emanuel!Carrilho!IQSC/USP! Vitor!Marcel!Faça!FMRP/USP! Undergraduate!Classes!IQSC/USP! Leadro!ArriveG!/!Daniel!Rodrigues!Cardoso!IQSC/USP! Roberto!GS!Berlinck!IQSC/USP! Daniel!Rodrigues!Cardoso!IQSC/USP! Edson!Rodrigues!Filho!UFSCar! Janete!Harumi!Yariwake! Natalia!EC!Almerida!/!Daniel!Rodrigues!Cardoso!IQSC/USP! Carlos!Galinaro!/!Eny!Maria!Vieira!IQSC/USP! Antonio!Carlos!B!Burtoloso! Lívia!S!Medeiros!/!Edison!Rodrigues!Filho!UFSCar! Arlene!Gonçalves!Corrêa!UFSCar! Helio!JA!Franco!/!Emanuel!Carrilho! José!Cesar!Rosa!FMRP/USP! Carlos!Alberto!Montanari!IQSC/USP! Ana!Rita!A!Nogueira!EMBRAPA! Alberto!Grossi!KU! Fernanda!F!Anibal!UFSCar! Marcols!RV!Lanza!IQSC/USP! Beatriz!NM!Miranda!/!Emanuel!Carrilho!IQSC/USP! Nilson!A!Assunção!UNIFESP! Adriano!Aquino!/!Emanuel!Carrilho!IQSC/USP! Juliana!Vieira!Alberice!/!Emanuel!Carrilho!IQSC/USP! Germano!Tremiliosi!Fo.!IQSC/USP! Eny!Maria!Vieira!IQSC/USP! Frank!N.!Crespilho!IQSC/USP! Pedro!Berci!IQSC/USP! Willy!Glen!Santos!/!Daniel!Rodrigues!Cardoso!IQSC/USP! Hong!Tran!/!Roberto!GS!Berlinck!IQSC/USP! André!LM!Porto!IQSC/USP! Tanare!CR!Ferreira!/!Alvaro!J!Santos!Neto! Timothy!J!Brockton!UFSCar! Magali!Monteiro!Silva!FCFAR!UNESP! Andrei!Leitão!IQSC/USP! Kleber!Thiago!de!Oliveira!UFSCar! Barbara!Bernardim!/!Antonio!Carlos!B!Burtoloso!IQSC/USP! Francisco!ER!Gomes!/!Germano!Tremiliosi!Fo.!IQSC/USP! Antonio!Gilberto!Ferreira!UFSCar! Carla!S!Cavalheiro!IQSC/USP! Victor!Deflon!IQSC/USP! Ubirajara!Rodrigues!Pereira!IQSC/USP! 165$$ 61$$ 23$$ 5$$ 5$$ 4$$2$$ iqsc$ ufscar$ fmrp$ embrapa$ exterior$ unifesp$ unesp$
Future Charges - After Final Report Direct Infusion - per Sample $ 10.00 (IQSC & UFSCar) $ 25.00 (Academic) $ 125.00 (Industry) NanoLC and UHPLC MS $ 75.00/day (IQSC & UFSCar) $ 125.00/day (Academic) $ 125.00/sample (Industry)
100% Granted EMU 2004: CE-MS (w/ Marina FM Tavares IQ/USP and Adelia R Amaya, UNICAMP) 2004: LC-QToF (Fernando M Lanças and Douglas W Franco, IQSC and Edson Rodrigues Fo, UFSCar) 2009: HRMS LTQ Orbitrap Velos (w/ Edson Rodrigues Fo, UFSCar) 2014/2015: Tribrid Orbitrap Fusion; MALDI/ToF Imaging; SEM-FEG; GCxGC/MS
Thanks