Pyrrolizidine Alkaloids from Onosma kaheirei Teppner (Boraginaceae)
|
|
|
- Solomon Baldwin Potter
- 5 years ago
- Views:
Transcription
1 Supporting Information Rec. Nat. Prod. 10:2 (2016) Pyrrolizidine Alkaloids from nosma kaheirei Teppner (Boraginaceae) Ioanna-Maria rfanou 1, Harilaos Damianakos 1, Ioannis Bazos 2, Konstantia Graikou1 and Ioanna Chinou1* 1 Department of Pharmacy, Division of Pharmacognosy and Natural Product Chemistry, University of Athens, University Campus of Zographou, Athens, Greece 2 Department of Biology, Division of Ecology and Systematics, University of Athens, University Campus of Zographou, Athens, Greece Table of Contents Page S1: ESI-MS Spectrum of Compound 7 ((-)-3 --acetylechinatine N-oxide) 3 S2: Expansion of ESI-MS Spectrum of Compound 7 ((-)-3 --acetylechinatine N- oxide) 4 S3: HR-ESI-MS Spectrum of Compound 7 ((-)-3 --acetylechinatine N-oxide) 5 S4: Expansion of HR-ESI-MS Spectrum of Compound 7 ((-)-3 --acetylechinatine N-oxide) S5: Expansion of HR-ESI-MS Spectrum of Compound 7 ((-)-3 --acetylechinatine N-oxide) S6: 1 H-NMR Spectrum (400 MHz, MeH-d 4 ) of Compound 7 ((-)-3 -acetylechinatine N-oxide) S7: Expansion of 1 H-NMR Spectrum of Compound 7 ((-)-3 --acetylechinatine N- oxide) (from 0.00 to 3.40 ppm) S8: Expansion of 1 H-NMR Spectrum of Compound 7 ((-)-3 --acetylechinatine N- 10 1
2 oxide) (from 3.40 to 6.00 ppm) S9: 13 C-NMR Spectrum (50 MHz, MeH-d 4 ) of Compound 7 ((-)-3 -acetylechinatine N-oxide) S10: CSY Spectrum (400 MHz) of Compound 7 ((-)-3 --acetylechinatine N- oxide) S11: Expansion of CSY Spectrum (400 MHz) of Compound 7 ((-)-3 -acetylechinatine N-oxide) (from 0.00 to 4.00 ppm) S12: Expansion of CSY Spectrum (400 MHz) of Compound 7 ((-)-3 -acetylechinatine N-oxide) (from 4.00 to 6.00 ppm) S13: HSQC-DEPT Spectrum (400 MHz) of Compound 7 ((-)-3 --acetylechinatine N-oxide) S14: HMBC Spectrum (400 MHz) of Compound 7 ((-)-3 --acetylechinatine N- oxide) S15: NESY Spectrum (400 MHz) of Compound 7 ((-)-3 --acetylechinatine N- oxide) 17 2
3 S1: ESI-MS Spectrum of Compound 7 ((-)-3 --acetylechinatine N-oxide) 3
4 S2: Expansion of ESI-MS Spectrum of Compound 7 ((-)-3 --acetylechinatine N-oxide) 4
5 Relative Abundance KM_30013B_H20_MeH_FTMS_2_ESI(+) #2-29 RT: AV: 28 NL: 4.37E7 F: FTMS + c ESI Full ms [ ] m/z m/z Intensity Relative Delta RDB Composition Abundance (ppm) equiv C14 H C14 H12 2 N Na C15 H26 5 N C16 H22 4 Na C16 H23 4 Na C15 H26 6 N C15 H27 6 N C15 H28 6 N C15 H28 6 N C15 H25 6 N Na C15 H26 6 N Na C15 H27 6 N Na C15 H20 7 N Na C16 H35 7 N C15 H25 7 N Na C15 H25 7 N Na C16 H33 7 N Na S3: HR-ESI-MS Spectrum of Compound 7 ((-)-3 --acetylechinatine N-oxide) 5
6 Relative Abundance KM_30013B_H20_MeH_FTMS_2_ESI(+) #2-29 RT: AV: 28 NL: 4.96E4 F: FTMS + c ESI Full ms [ ] m/z m/z Intensity Relative Delta RDB equiv. Composition Abundance (ppm) C16 H16 7 N Na C17 H28 7 N S4: Expansion of HR-ESI-MS Spectrum of Compound 7 ((-)-3 --acetylechinatine N-oxide) 6
7 Relative Abundance KM_30013B_H20_MeH_FTMS_2_ESI(+) #2-29 RT: AV: 28 NL: 9.94E4 F: FTMS + c ESI Full ms [ ] m/z m/z Intensity Relative Delta (ppm) RDB Composition Abundance equiv C17 H25 7 N Na C18 H37 7 N C17 H27 7 N Na S5: Expansion of HR-ESI-MS Spectrum of Compound 7 ((-)-3 --acetylechinatine N-oxide) 7
8 ' 7' H 3 C H 2' 3' 5' 6' CH3 4' CH H 7 8 H N H 3 C S6: 1 H-NMR Spectrum (400 MHz, MeH-d 4 ) of Compound 7 ((-)-3 --acetylechinatine N- oxide) (-)-3 --acetylechinatine N-oxide (7): Pale yellow gum. 1 H-NMR (MeH-d 4, 400 MHz), δ: 0.91 (3H, d, H-7 ), 0.97 (3H, d, H-6 ), 1.29 (3H, d, H-4 ), 2.04 (3H, s, CCH 3 ), 2.08 (1H, m, H-6β), 2.17 (1H, sept, H-5 ), 2.60 (1H, m, H-6α), 3.68 (1H, m, H-5β), 3.83 (1H, m, H-5α), 4.33 (1H, d, H-3β), 4.63 (1H, d, H-3α), 4.67 (1H, brs, H-8), 4.73 (1H, m, H-7), 4.85 (2H, brs, H-9), 5.18 (1H, q, H-3 ), 5.92 (1H, brs, H-2). 13 C-NMR (MeH-d 4, 50 MHz), δ: 16.6 (C-4 ), 17.5 (C-6 ), 18.3 (C-7 ), 18.5 (CCH 3 ), 33.9 (C-5 ), 35.7 (C-6), 62.4 (C-9), 70.2 (C-5), 70.8 (C-7), 71.9 (C-3 ), 79.1 (C-3), 82.0 (C-2 ), 97.2 (C-8), (C-2), (C-1), (C-1 ), (CCH 3 ). ESI-MS: m/z = [M+Na] + for formula C 17 H 27 N 7 Na. 8
9 ' 7' H 3 C H 2' 3' 5' 6' CH3 4' CH 3 H-4 H-6 H H 7 8 H N H 3 C H-6β + CCH3 200 H-6α H S7: Expansion of 1 H-NMR Spectrum of Compound 7 ((-)-3 --acetylechinatine N-oxide) (from 0.00 to 3.40 ppm) 9
10 ' 7' H 3 C H 2' 3' 5' 6' CH3 4' CH H 7 8 H N + 5 H H 3 C H-3 H-7 H-8 H-3α H-3β H-5α H-5β S8: Expansion of 1 H-NMR Spectrum of Compound 7 ((-)-3 --acetylechinatine N-oxide) (from 3.40 to 6.00 ppm) 10
11 ' 7' H 3 C H 2' 3' 5' 6' CH3 4' CH H 7 8 H 9 1 δc 172.0, CCH3 δc 170.6, C N + - C-1 3 C-2 2 H 3 C C-8 C-3 C-3 C-7 C-5 C-9 C-6 C-5 C-7, CH3C C-6 C S9: 13 C-NMR Spectrum (50 MHz, MeH-d 4 ) of Compound 7 ((-)-3 --acetylechinatine N- oxide) 11
12 ppm (f2) S10: CSY Spectrum (400 MHz) of Compound 7 ((-)-3 --acetylechinatine N-oxide) 12
13 ppm (f2) S11: Expansion of CSY Spectrum (400 MHz) of Compound 7 ((-)-3 --acetylechinatine N- oxide) (from 0.00 to 4.00 ppm) 13
14 ppm (f2) S12: Expansion of CSY Spectrum (400 MHz) of Compound 7 ((-)-3 --acetylechinatine N- oxide) (from 4.00 to 6.00 ppm) 14
15 Η-4 /C-4 Η-6 /C-6 Η-7 /C-7 50 Η-9/C-9 Η-7/C-7 Η-3 /C-3 Η-5α/C-5 Η-5β/C-5 Η-3α/C-3 Η-3β/C-3 Η-8/C-8 Η-2/C ppm (f2) S13: HSQC-DEPT Spectrum (400 MHz) of Compound 7 ((-)-3 --acetylechinatine N-oxide) 15
16 ppm (f2) S14: HMBC Spectrum (400 MHz) of Compound 7 ((-)-3 --acetylechinatine N-oxide) 16
17 5.0 ppm (f2) 5.0 S15: NESY Spectrum (400 MHz) of Compound 7 ((-)-3 --acetylechinatine N-oxide) 17
Supporting Information
Supporting Information A new series of cytotoxic pyrazoline derivatives as potential anticancer agents induces cell cycle arrest and apoptosis Hong Wang 1,, Jinhong Zheng 1,, Weijie Xu 1, Cheng Chen 1,
Two new sesquiterpenes from a kind of TCM Pieces, Curcumae Radix
Supporting Information Rec. Nat. Prod. 8:4 (2014) 334-341 Two new sesquiterpenes from a kind of TCM Pieces, Curcumae Radix onghua Wu *1,2, onghong Zheng 1,2, Yantong Xu 1,2, Peng Zhang 1,2, Gang Chen 3
Identification of novel endophenaside antibiotics produced by Kitasatospora sp. MBT66
SUPPORTING INFORMATION belonging to the manuscript: Identification of novel endophenaside antibiotics produced by Kitasatospora sp. MBT66 by Changsheng Wu 1, 2, Gilles P. van Wezel 1, *, and Young Hae
Supplementary Information
Supplementary Information New Highly Oxygenated Germacranolides from Carpesium divaricatum and their Cytotoxic Activity Tao Zhang, 1 Jin-Guang Si, 1, 2 Qiu-Bo Zhang, 1 Gang Ding, 1 and Zhong-Mei Zou 1*
Preparation of Fluorinated Tetrahydropyrans and Piperidines using a New Nucleophilic Fluorination Reagent DMPU/HF
Supporting information Preparation of Fluorinated Tetrahydropyrans and Piperidines using a New Nucleophilic Fluorination Reagent DMPU/HF Otome E. Okoromoba, a Gerald B. Hammond, a, * Bo Xu b, * a Department
SUPPORTING INFORMATION
SUPPORTING INFORMATION Phosphine-Mediated Disulfide Metathesis in Aqueous Media Rémi Caraballo, Morakot Sakulsombat, and Olof Ramström* KTH - Royal Institute of Technology, Department of Chemistry Teknikringen
Supplementary Information
Supplementary Information Synthesis and antioxidant evaluation of enantiomerically pure bis- (1,2,3-triazolylmethyl)amino esters from modified α-amino acids Juan I. Sarmiento-Sánchez a *, Adrián Ochoa-Teran
yellow coloured amorphous powder, which on crystallization from hot acetone resulted in pale
Supporting Information Hexane Extract. Compound I: Elution of column with hexane: dichloromethane (50:50 v/v; 200 ml), gave a pale yellow coloured amorphous powder, which on crystallization from hot acetone
Pt IV azido complexes undergo copper-free click reactions with alkynes
Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 208 Pt IV azido complexes undergo copper-free click reactions with alkynes Electronic Supplementary
Synthesis and Blastocyst Implantation Inhibition Potential of Lupeol Derivatives in Female Mice
Supporting Information Rec. Nat. Prod. 9:4 (2015) 561-566 Synthesis and Blastocyst Implantation Inhibition Potential of Lupeol Derivatives in Female Mice Anita Mahapatra 1*, Purvi Shah 1, Mehul Jivrajani
An Unusual Glycosylation Product from a Partially Protected Fucosyl Donor. under Silver Triflate activation conditions. Supporting information
An Unusual Glycosylation Product from a Partially Protected Fucosyl Donor under Silver Triflate activation conditions Robin Daly a and Eoin M. Scanlan* a e-mail: eoin.scanlan@tcd.ie a Trinity Biomedical
SUPPORTING INFORMATION
SUPPORTING INFORMATION Synthesis and Preliminary Pharmacological Evaluation of Aryl Dithiolethiones with Cyclooxygenase-2 Selective Inhibitory Activity and Hydrogen-Sulfide-Releasing Properties Shannon
First Detection of Unprotected 1,2-Anhydro Aldopyranoses
First Detection of Unprotected 1,2-Anhydro Aldopyranoses Kazunari Serizawa, Masato Noguchi, Gefei Li, and Shin-ichiro Shoda* Department of Biomolecular Engineering, Graduate School of Engineering, Tohoku
Development of a near-infrared fluorescent probe for monitoring hydrazine in serum and living cells
Supporting Information for Development of a near-infrared fluorescent probe for monitoring hydrazine in serum and living cells Sasa Zhu, Weiying Lin,* Lin Yuan State Key Laboratory of Chemo/Biosensing
Supporting Information
Supporting Information Wiley-VCH 2005 69451 Weinheim, Germany rganocatalytic, Asymmetric α-halogenation of 1,3- Dicarbonyl Compounds Giuseppe Bartoli,* Marcella Bosco, Armando Carlone, Manuela Locatelli,
Supporting information for. Synthesis of phenothiazines from cyclohexanones and. 2-aminobenzenethiols under transition-metal-free conditions
Supporting information for Synthesis of phenothiazines from cyclohexanones and 2-aminobenzenethiols under transition-metal-free conditions Yunfeng Liao, a Pengcheng Jiang, a Shanping Chen, a Fuhong Xiao,
Synthesis of Sequence-Controlled Acrylate Oligomers. via Consecutive RAFT Monomers Additions
Supporting Information Synthesis of Sequence-Controlled Acrylate ligomers via Consecutive RAFT Monomers Additions Joke Vandenbergh a, Gunther Reekmans, b Peter Adriaensens b and Thomas Junkers a * a Polymer
Supporting information
Supporting information Rhabdopeptide/Xenortide-like Peptides from Xenorhabdus innexi with Terminal Amines Showing Potent Anti-protozoal Activity Lei Zhao,, Marcel Kaiser,, Helge B. Bode *,, Molekulare
GRADUATE UNIVERSITY OF SCIENCE AND TECHNOLOGY VU THI QUYNH CHI
MINISTRY OF EDUCATION AND TRAINING VIETNAM ACADEMY OF SCIENCE AND TECHNOLOGY GRADUATE UNIVERSITY OF SCIENCE AND TECHNOLOGY ----------------------------- VU THI QUYNH CHI STUDY ON CHEMICAL CONSTITUENTS
NON TARGETED SEARCHING FOR FOOD
NON TARGETED SEARCHING FOR FOOD CONTAMINANTS USING ORBITRAP HIGH RESOLUTION MASS SPECTROMETRY Michal Godula 1, Adrian Charlton 2 and Klaus Mittendorf 1 1 Thermo Fisher Scientific, Dreieich, Germany 2 Food
Lysoquinone-TH1, a new polyphenolic tridecaketide produced by expressing the lysolipin minimal PKS II in Streptomyces albus
Supplemental Information Lysoquinone-TH1, a new polyphenolic tridecaketide produced by expressing the lysolipin minimal PKS II in Streptomyces albus Torben Hofeditz, 1 Claudia Eva-Maria Unsin 2, Jutta
Supplementary Information
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2018 Supplementary Information Synthesis of plasmodione metabolites and 13 C-enriched
Preparation and Characterization of Cysteine Adducts of Deoxynivalenol
Preparation and Characterization of Cysteine Adducts of Deoxynivalenol Ana Stanic, Silvio Uhlig, Anita Solhaug, Frode Rise, Alistair L. Wilkins, Christopher O. Miles S1 Figure S1. 1 H spectrum of 1 (DON)
Supporting Information
Supporting Information Developing Activity Localization Fluorescence Peptide Probe Using Thiol-Ene Click Reaction for Spatially Resolved Imaging of Caspase-8 in Live Cells Wei Liu,, Si-Jia Liu,, Yong-Qing
Supporting information for the article
S1 Supporting information for the article Efficient General Procedure To Access a Diversity of Gold(0) Particles and Gold(I) Phosphine Complexes from a Simple HAuCl 4 Source. Localization of Homogeneous/Heterogeneous
Direct Regioselective Esterification at O-2 of β- Cyclodextrin and Hydrolysis by Neighboring-group Participation
ISSN: 0973-4945; CDEN ECJHA E- Chemistry http://www.ejchem.net 2012, 9(3), 1562-1568 Direct Regioselective Esterification at -2 of β- Cyclodextrin and Hydrolysis by Neighboring-group Participation ZHI-ZHNG
Chemical Constituent from Roots of Garcinia Mangostana (Linn.)
Vol., No. Chemical Constituent from Roots of Garcinia Mangostana (Linn.) Sheikh Ahmad Izaddin Sheikh Mohd Ghazali (Corresponding author) Faculty of Applied Sciences, Universiti Teknologi MARA 000 Kuala
Self-organization of dipyridylcalix[4]pyrrole into a supramolecular cage for dicarboxylates
![Self-organization of dipyridylcalix[4]pyrrole into a supramolecular cage for dicarboxylates](/thumbs/94/118164746.jpg "Self-organization of dipyridylcalix[4]pyrrole into a supramolecular cage for dicarboxylates")
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 Electronic Supplementary Information Self-organization of dipyridylcalix[4]pyrrole into a supramolecular
Rapid Generation of Fatty Acid Methyl Ester Profiles using (Direct Analysis in Real Time) DART- Mass Spectrometry
Rapid Generation of Fatty Acid Methyl Ester Profiles using (Direct Analysis in Real Time) DART- Mass Spectrometry Brian Musselman, Jordan Krechmer, Tim Ng, and Joseph LaPoint IonSense, Inc. 999 Broadway
DEPARTMENT OF CHEMISTRY AND CHEMICAL ORGANIC CHEMISTRY II 202-BZG-05 03
DEPARTMENT OF CHEMISTRY AND CHEMICAL TECHNOLOGY ORGANIC CHEMISTRY II 202-BZG-05 03 TEST 1 11 MARCH 2010 INSTRUCTOR: I. DIONNE PRINT YOUR NAME: Answers INSTRUCTIONS: Answer all questions in the space provided.
Supporting Information
Supporting Information Wiley-VCH 2006 69451 Weinheim, Germany A Convergent Synthesis of N-Linked Glycopeptides Clyde M. Kaneshiro, Katja Michael* 1. LC-MS analysis of crude glycopeptide 16. 2. ESI-TOF
2,6,9-Triazabicyclo[3.3.1]nonanes as overlooked. amino-modification products by acrolein
![2,6,9-Triazabicyclo[3.3.1]nonanes as overlooked. amino-modification products by acrolein](/thumbs/86/94743397.jpg "2,6,9-Triazabicyclo[3.3.1]nonanes as overlooked. amino-modification products by acrolein")
Supplementary Information 2,6,9-Triazabicyclo[3.3.1]nonanes as overlooked amino-modification products by acrolein Ayumi Tsutsui and Katsunori Tanaka* Biofunctional Synthetic Chemistry Laboratory, RIKEN
A pillar[2]arene[3]hydroquinone which can self-assemble to a molecular zipper in the solid state
![A pillar[2]arene[3]hydroquinone which can self-assemble to a molecular zipper in the solid state](/thumbs/86/93673402.jpg "A pillar[2]arene[3]hydroquinone which can self-assemble to a molecular zipper in the solid state")
A pillar[2]arene[3]hydroquinone which can self-assemble to a molecular zipper in the solid state Mingguang Pan, Min Xue* Department of Chemistry, Zhejiang University, Hangzhou 310027, P. R. China Fax:
Bioactivity Based Molecular Networking for the Discovery of Drug Lead in Natural Product Bioassay-Guided Fractionation
Bioactivity Based Molecular Networking for the Discovery of Drug Lead in Natural Product Bioassay-Guided Fractionation Louis-Félix Nothias,,, Mélissa Nothias-Esposito,, # Ricardo da Silva,, Mingxun Wang,,,
Supplementary Figure 1. ESI/MS/MS analyses of native and de-acetylated S2A Supplementary Figure 2. Partial 1D 1H NMR spectrum of S2A
Supplementary Figure 1. ESI/MS/MS analyses of native and de-acetylated S2A. Panel A, Positive ESI mass spectra of native (N) and de-acetylated (DA) non-active S2A were obtained, and demonstrated a shift
Coordination-responsive Selenium-containing Polymer Micelles for. Supporting information
Electronic Supplementary Material (ESI) for Chemical Science Coordination-responsive Selenium-containing Polymer Micelles for Controlled Drug Release Wei Cao, a Yang Li, b Yu Yi, a Shaobo Ji, a Lingwu
A Hierarchy of Aryloxide Deprotection by Boron Tribromide. Supporting Information
A Hierarchy of Aryloxide Deprotection by Boron Tribromide Sreenivas Punna, Stéphane Meunier and M. G. Finn* Department of Chemistry and The Skaggs Institute for Chemical Biology, The Scripps Research Institute,
Revista Boliviana de Química ISSN: Universidad Mayor de San Andrés Bolivia
Revista Boliviana de Química ISSN: 020-0 revbolquim@outlook.com Universidad Mayor de San Andrés Bolivia Vila, Jose; Mollinedo, Patricia; Sterner, lov SPECTRSCPIC STUDIES F LICHEN DEPSIDES AND DEPSIDNES
Isolation and Identification of the Phenolic Compounds from the Roots of Sanguisorba officinalis L. and Their Antioxidant Activities
Molecules 2012, 17, 13917-13922; doi:10.3390/molecules171213917 PEN ACCESS molecules ISSN 1420-3049 www.mdpi.com/journal/molecules Article Isolation and Identification of the Phenolic Compounds from the
Mass Spectrometry Infrastructure
Mass Spectrometry Infrastructure Todd Williams, Ph.D. Director KU Mass Spectrometry and Analytical Proteomics Laboratory Mass Spectrometry Lab B025 Malott Hall Mission The Mass Spectrometry and analytical
Supporting Information. Efficient copper-catalyzed Michael addition of acrylic derivatives with primary alcohols in the presence of base
Supporting Information Efficient copper-catalyzed Michael addition of acrylic derivatives with primary alcohols in the presence of base Feng Wang, a Haijun Yang, b Hua Fu, b,c * and Zhichao Pei a * a College
Metabolomics A New Tool in Molecular Toxicology
Metabolomics A New Tool in Molecular Toxicology EU INFLAME Training, Birmingham 19 th January 2012 Mark Viant (Jinkang s co-supervisor) Overview 1. Setting the scene from Wednesday s talks 2. What is metabolomics?
Analysis of fatty acid metabolism using Click-Chemistry and HPLC-MS
Analysis of fatty acid metabolism using Click-Chemistry and HPLC-MS Alexander J. Pérez and Helge B. Bode -Supporting Information- Contents Experimental section Supplementary figures NMR spectra Page S2
Quantification of labile and stable non-polar arsenolipids in commercial fish meals and edible seaweed samples
Electronic Supplementary Material (ESI) for Journal of Analytical Atomic Spectrometry. This journal is The Royal Society of Chemistry 7 Quantification of labile and stable non-polar arsenolipids in commercial
EXPERIMENTAL PROCEDURES, OPTIMIZATION STUDIES, CHARACTERIZATION DATA and NMR SPECTRA
Supporting Information for Chemical Communications: S1 SUPPRTING INFRMATIN FR CHEM. CMMUN. Direct, facile synthesis of N-acyl-α-amino amides from α-keto esters and ammonia Rukundo Ntaganda, a Tamara Milovic,
NMR Analysis of Oligosaccharides Containing Fructopyranoside
Dynamic Biochemistry, Process Biotechnology and Molecular Biology 2009 Global Science Books NMR Analysis of ligosaccharides Containing Fructopyranoside Eri Fukushi 1* Hideki kada 2 Akira Yamamori 2 Naoki
Supporting Information. Copyright Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, 2007
Supporting Information Copyright Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, 2007 Organocatalytic Asymmetric Sulfa-Michael Addition to α,β- Unsaturated Ketones Paolo Ricci, Armando Carlone, Giuseppe
C 21 Steroidal Glycosides from Acidic Hydrolysate of Cynanchum otophyllum
Zhao YB et al. Chinese Herbal Medicines, 2014, 6(4): 319-323 319 Available online at SciVarse ScienceDirect Chinese Herbal Medicines (CHM) ISSN 1674-6384 Journal homepage: www.tiprpress.com E-mail: chm@tiprpress.com
Journal of Chemical and Pharmaceutical Research, 2013, 5(1): Research Article. Flavonoids from Astragalus propinquus
Available online www.jocpr.com Journal of Chemical and Pharmaceutical Research, 2013, 5(1):261-265 Research Article ISSN : 0975-7384 CODEN(USA) : JCPRC5 Flavonoids from Astragalus propinquus Venkata Sai
Supporting Information for. Boronic Acid Functionalized Aza-Bodipy (azabdpba) based Fluorescence Optodes for the. analysis of Glucose in Whole Blood
Supporting Information for Boronic Acid Functionalized Aza-Bodipy (azabdpba) based Fluorescence Optodes for the analysis of Glucose in Whole Blood Yueling Liu, Jingwei Zhu, Yanmei Xu, Yu Qin*, Dechen Jiang*
Ten Second DART -MS: Ultra-Fast QC Screening of Dietary Supplements and Pharmaceuticals with a Next Generation DART Source
Ten Second DART -MS: Ultra-Fast QC Screening of Dietary Supplements and Pharmaceuticals with a Next Generation DART Source Elizabeth Crawford, Joseph LaPointe,and Brian Musselman IonSense, Inc. 999 Broadway
Neuroprotective and Antioxidant Constituents from Curcuma zedoaria Rhizomes
Supporting Information Rec. Nat. Prod. 9:3 (2015) 349-355 Neuroprotective and Antioxidant Constituents from Curcuma zedoaria Rhizomes Omer Abdalla Ahmed Hamdi 1, Lo Jia Ye 2, Muhamad Noor Alfarizal Kamarudin
Cytotoxic and Antibacterial Activities of Constituents from Calophyllum ferrugineum Ridley
1 Supporting Information Rec. Nat. Prod. 10:5 (2016) 649-653 Cytotoxic and Antibacterial Activities of Constituents from Calophyllum ferrugineum Ridley Nurul Iman Aminudin 1, Farediah Ahmad 1*, Muhammad
Masatoshi Shibuya,Takahisa Sato, Masaki Tomizawa, and Yoshiharu Iwabuchi* Department of Organic Chemistry, Graduate School of Pharmaceutical Sciences,
Oxoammonium ion/naclo 2 : An Expedient, Catalytic System for One-pot Oxidation of Primary Alcohols to Carboxylic Acid with Broad Substrate Applicability Masatoshi Shibuya,Takahisa Sato, Masaki Tomizawa,
Amadeo R. Fernández-Alba
% of compounds % of compounds % of compounds % of compounds Amadeo R. Fernández-Alba LC-Orbitrap QExactive Focus Instrumental LOQ 1% 9% 8% 7% 6% 5% 4% 3% 2% 1% %.1 mg/g.2 mg/g Tomato.5 mg/g ddms2 Target
SUPPLEMENTARY MATERIAL
SUPPLEMENTARY MATERIAL Chemical constituents from Agrimonia pilosa Ledeb. and their chemotaxonomic significance Wei-jie Liu, Xue-qian Hou, Hao Chen, Jing-yu Liang*, Jian-bo Sun** Department of Natural
Biomass Oxidation to Formic Acid in Aqueous Media Using Polyoxometalate Catalysts Boosting FA Selectivity by In-situ Extraction
Electronic Supplementary Material (ESI) for Energy & Environmental Science. This journal is The Royal Society of Chemistry 2015 Biomass Oxidation to Formic Acid in Aqueous Media Using Polyoxometalate Catalysts
UPLC-HRMS: A tool for multi-residue veterinary drug methods
AOAC, Paris, November 23-24, 2009 UPLC-HRMS: A tool for multi-residue veterinary drug methods Anton Kaufmann Official Food Control Authority of the Canton of Zurich (Kantonales Labor Zürich) The challenge
Synthesis and Myocardial Ischemia Protective Effect of Ocotillol-Type Derivatives
RIGINAL ARTICLE Rec. Nat. Prod. 6:3 (2012) 242-254 Synthesis and Myocardial Ischemia Protective Effect of cotillol-type Derivatives Bi Yi 1, Wang Tian 2, Meng Qingguo 1 *, Zhang Jiangfen 1, Wang Liang
Supplementary Information: Liquid-liquid phase coexistence in lipid membranes observed by natural abundance 1 H 13 C solid-state NMR
Electronic Supplementary Material (ESI) for Physical Chemistry Chemical Physics. This journal is the wner Societies 28 Supplementary Information: Liquid-liquid phase coexistence in lipid membranes observed
L-Carnosine-Derived Fmoc-Tripeptides Forming ph- Sensitive and Proteolytically Stable Supramolecular
Supporting Information: L-Carnosine-Derived Fmoc-Tripeptides Forming ph- Sensitive and Proteolytically Stable Supramolecular Hydrogels Rita Das Mahapatra, a Joykrishna Dey* a, and Richard G. Weiss b a
Acaulins A and B, Trimeric Macrodiolides from Acaulium. Table of Contents
Supporting Information Acaulins A and B, Trimeric Macrodiolides from Acaulium sp. H-JQSF Ting Ting Wang, Ying Jie Wei, Hui Ming Ge, Rui Hua Jiao, Ren Xiang Tan* * Corresponding author. E-mail: rxtan@nju.edu.cn
Supporting Information for. Use of the Curtius Rearrangement of Acryloyl Azides in the Synthesis of. 3,5-Disubstituted Pyridines: Mechanistic Studies
Supporting Information for Use of the Curtius Rearrangement of Acryloyl Azides in the Synthesis of 3,5-Disubstituted Pyridines: Mechanistic Studies Ta-Hsien Chuang* a, Yu-Chi Chen b and Someshwar Pola
Supporting Information
Supporting Information Wiley-VCH 2008 69451 Weinheim, Germany Supporting Information Enantioselective Cu-catalyzed 1,4-Addition of Various Grignard Reagents to Cyclohexenone using Taddol-derived Phosphine-Phosphite
Two Novel Phenolic Compounds from the Rhizomes of Cyperus rotundus L.
Molecules 0, 7, 636-64; doi:0.3390/molecules7636 OPEN ACCESS molecules ISSN 40-3049 www.mdpi.com/journal/molecules Article Two Novel Phenolic Compounds from the Rhizomes of Cyperus rotundus L. Zhongliu
e. V Chemistry 262 Winter 2018 Exam 3
Chemistry 262 Winter 2018 Exam 3 The following 90 point exam contains 22 questions, valued at 4 points/question. There are also 3 unknown analysis problems, valued at 10 points/question, of which you are
Supporting Information
Supporting Information Asymmetric Catalysis of the Carbonyl-Amine Condensation: Kinetic Resolution of Primary Amines Sayantani Das, Nilanjana Majumdar, Chandra Kanta De, Dipti Sankar Kundu, Arno Döhring,
Supporting Information
Supporting Information B(C 6 F 5 ) 3 -catalyzed Regioselective Deuteration of Electronrich Aromatic and Heteroaromatic compounds Wu Li, Ming-Ming Wang, Yuya Hu and Thomas Werner* Leibniz-Institute of Catalysis
Chlorizidine, A Cytotoxic 5H-Pyrrolo[2,1-a]isoindol-5-one-Containing Alkaloid from a Marine Streptomyces sp.
![Chlorizidine, A Cytotoxic 5H-Pyrrolo[2,1-a]isoindol-5-one-Containing Alkaloid from a Marine Streptomyces sp.](/thumbs/88/115019181.jpg "Chlorizidine, A Cytotoxic 5H-Pyrrolo[2,1-a]isoindol-5-one-Containing Alkaloid from a Marine Streptomyces sp.")
Supporting Information Chlorizidine, A Cytotoxic 5-Pyrrolo[2,1-a]isoindol-5-one-Containing Alkaloid from a Marine Streptomyces sp. Xavier Alvarez-Mico, Paul R. Jensen, William Fenical, Chambers C. ughes*
Gade Hyldgaard, Mette; Purup, Stig; Bond, Andrew David; Frete, Xavier; Qu, Haiyan; Teglgaard Jensen, Katrine; Christensen, Lars Porskjær
Syddansk Universitet Guaianolides and a seco-eudesmane from the resinous exudates of cushion bush (Leucophyta brownii) and evaluation of their cytostatic and anti-inflammatory activity Gade Hyldgaard,
Characterization of an Unknown Compound Using the LTQ Orbitrap
Characterization of an Unknown Compound Using the LTQ rbitrap Donald Daley, Russell Scammell, Argenta Discovery Limited, 8/9 Spire Green Centre, Flex Meadow, Harlow, Essex, CM19 5TR, UK bjectives unknown
Supplementary Material. Efficient Synthesis of an Indinavir Precursor from Biomass Derived (-)- Levoglucosenone
1.171/CH17227_AC CSIRO 217 Australian Journal of Chemistry 217, 7(1), 1146-115 Supplementary Material Efficient Synthesis of an Indinavir Precursor from Biomass Derived (-)- Levoglucosenone Edward T. Ledingham,
SUPPORTING INFORMATION. Studies on antimicrobial evaluation of some 1-((1-(1H-benzo[d]imidazol-2-
![SUPPORTING INFORMATION. Studies on antimicrobial evaluation of some 1-((1-(1H-benzo[d]imidazol-2-](/thumbs/79/79646314.jpg "SUPPORTING INFORMATION. Studies on antimicrobial evaluation of some 1-((1-(1H-benzo[d]imidazol-2-")
SUPPORTIG IFORMATIO Studies on antimicrobial evaluation of some 1-((1-(1H-benzo[d]imidazol-2- yl)ethylidene)amino)-6-((arylidene)amino)-2-oxo-4-phenyl-1,2-dihydropyridine-3,5- dicarbonitriles C Desai*,
Advances in Hybrid Mass Spectrometry
The world leader in serving science Advances in Hybrid Mass Spectrometry ESAC 2008 Claire Dauly Field Marketing Specialist, Proteomics New hybrids instruments LTQ Orbitrap XL with ETD MALDI LTQ Orbitrap
Supporting Information. Bioactive Constituents of Glycyrrhiza uralensis (Licorice): Discovery of the Effective Components of a Traditional Herbal
Supporting Information Bioactive Constituents of Glycyrrhiza uralensis (Licorice): Discovery of the Effective Components of a Traditional Herbal Medicine Shuai Ji, Ziwei Li, Wei Song, Yongrui Wang, Wenfei
Study of On-Resin Convergent Synthesis of N-Linked. Glycopeptides Containing a Large High Mannose N- Linked Oligosaccharide
Supporting Information Study of On-Resin Convergent Synthesis of N-Linked Glycopeptides Containing a Large High Mannose N- Linked Oligosaccharide Rui Chen and Thomas J. Tolbert* Department of Chemistry,
Chukvelutins A-C, 16-norphragmalin limonoids with unprecedented skeletons from Chukrasia tabularis var. velutina
Chukvelutins A-C, 16-norphragmalin limonoids with unprecedented skeletons from Chukrasia tabularis var. velutina Jun Luo, Jun-Song Wang, Jian-Guang Luo, Xiao-Bing Wang, and Ling-Yi Kong* Department of
A Self-Immolative Dendritic Glucuronide Prodrug of Doxorubicin
A Self-Immolative Dendritic Glucuronide Prodrug of Doxorubicin Grinda et al S1 Supporting Information A Self-Immolative Dendritic Glucuronide Prodrug of Doxorubicin Marion Grinda, a Jonathan Clarhaut,
Schwartz s reagent-mediated regiospecific synthesis of 2,3-disubstituted indoles from isatins
Electronic Supplementary Information (ESI) Schwartz s reagent-mediated regiospecific synthesis of 2,3-disubstituted indoles from isatins A. Ulikowski and B. Furman* Institute of Organic Chemistry, Polish
Facile Cu(II) mediated conjugation of thioesters and thioacids to peptides and proteins under mild conditions
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2018 Facile Cu(II) mediated conjugation of thioesters and thioacids to peptides
Supporting information for the article
Supporting information for the article S1 Exceptional behavior of Ni 2 O 2 species revealed by ESI-MS and MS/MS studies in solution. Application of superatomic core to facilitate new chemical transformations
Stereoselective Aza-Darzens Reactions of Tert- Butanesulfinimines: Convenient Access to Chiral Aziridines
Stereoselective Aza-Darzens Reactions of Tert- Butanesulfinimines: Convenient Access to Chiral Aziridines Toni Moragas Solá, a Ian Churcher, b William Lewis a and Robert A. Stockman* a Supplementary Information
Electronic Supporting Information for
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2015 Electronic Supporting Information for Rhodamine based Turn-On Fluorescent Probe for Pb(II)
Characterizing fatty acids with advanced multinuclear NMR methods
Characterizing fatty acids with advanced multinuclear NMR methods Fatty acids consist of long carbon chains ending with a carboxylic acid on one side and a methyl group on the other. Most naturally occurring
Electronic supplementary information Poly(vinyl)chloride supported palladium nanoparticles: Catalyst for rapid hydrogenation reactions
Electronic supplementary information Poly(vinyl)chloride supported palladium nanoparticles: Catalyst for rapid hydrogenation reactions Hosahalli P. Hemantha and Vommina V. Sureshbabu* Peptide Research
Supporting Information. Ruthenium(II)-Catalyzed C H Alkynylation of Weakly-Coordinating Benzoic Acids. Ruhuai Mei, Shou-Kun Zhang, and Lutz Ackermann*
Supporting Information Ruthenium(II)-Catalyzed C H Alkynylation of Weakly-Coordinating Benzoic Acids Ruhuai Mei, Shou-Kun Zhang, and Lutz Ackermann* Institut für Organische und Biomolekulare Chemie, Georg-August-Universität
Genomics-driven discovery of taiwachelin, a lipopeptide siderophore from Cupriavidus taiwanensis
Supporting information Genomics-driven discovery of taiwachelin, a lipopeptide siderophore from Cupriavidus taiwanensis Martin F. Kreutzer and Markus Nett * Table of contents SI-2, SI-3 SI-4 SI-5 SI-6
Supporting Information. were prepared from commercially available ethyl acetoacetate by alkylation with the
ighly Stereoselective Reductions of α-alkyl-1,3-diketones and α- Alkyl-β-keto esters Catalyzed by Isolated NADP-dependent Ketoreductases Dimitris Kalaitzakis, a David J. Rozzell b, Spiros Kambourakis *b
Supplementary Figure 1: UV-Vis absorption (a) and excitation emission matrix (EEM) (b) spectra of the SN medium (Cyanosite ) used to grow
Supplementary Figure 1: UV-Vis absorption (a) and excitation emission matrix (EEM) (b) spectra of the SN medium (Cyanosite ) used to grow Synechococcus cultures. Note: The same scale used in Figure 1 was
Electronic Supplementary Information
Electronic Supplementary Information A Novel and Facile Zn-mediated Intramolecular Five-membered Cyclization of β-tetraarylporphyrin Radicals from β-bromotetraarylporphyrins Dong-Mei Shen, Chao Liu, Qing-Yun
Development of Pyridine Based o-aminophenolate Zinc Complexes as Structurally Tunable Catalysts for CO 2 Fixation into Cyclic Carbonates
Electronic Supplementary Material (ESI) for New Journal of Chemistry. This journal is The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2017 Electronic Supporting Information
VOL. 56 NO. 2, FEB THE JOURNAL OF ANTIBIOTICS pp YM and YM , Novel Thiopeptide Antibiotics Produced
VOL. 56 NO. 2, FEB. 2003 THE JOURNAL OF ANTIBIOTICS pp. 129-134 YM-266183 and YM-266184, Novel Thiopeptide Antibiotics Produced by Bacillus cereus Isolated from a Marine Sponge II. Structure Elucidation
Chemo- and Enantioselective Rh-Catalyzed Hydrogenation of 3-Methylene-1,2-diazetidines: Application to Vicinal Diamine Synthesis
Chemo- and Enantioselective Rh-Catalyzed Hydrogenation of 3-Methylene-1,2-diazetidines: Application to Vicinal Diamine Synthesis Greg P. Iacobini, a David W. Porter, b and Michael Shipman* a a Department
Direct Synthesis of a Copper(II) N-heterocyclic Carbene Complex in Air
Supporting Information for Direct Synthesis of a Copper(II) N-heterocyclic Carbene Complex in Air Daniel J. O Hearn and Robert D. Singer* Atlantic Centre for Green Chemistry, Department of Chemistry, Saint
Preparation of Stable Aziridinium Ions and Their Ring Openings
Supplementary Information Preparation of Stable Aziridinium Ions and Their Ring Openings Yongeun Kim a Hyun-Joon Ha*, a Sae Young Yun b and Won Koo Lee,*,b a Department of Chemistry and Protein Research
All chemicals were obtained from Aldrich, Acros, Fisher, or Fluka and were used without
Supplemental Data Alexander et al. Experimental Procedures General Methods for Inhibitor Synthesis All chemicals were obtained from Aldrich, Acros, Fisher, or Fluka and were used without further purification,
Overproduction of ristomycin A by activation of a silent gene cluster in Amycolatopsis japonicum MG417-CF17
Supplemental Material for verproduction of ristomycin A by activation of a silent gene cluster in Amycolatopsis japonicum MG417-CF17 Marius Spohn, a orbert Kirchner, b,c Andreas Kulik, a, Angelika Jochim,
Synthesis of an Alleged Byproduct Precursor in Iodixanol Preparation
SUPPORTING INFORMATION Synthesis of an Alleged Byproduct Precursor in Iodixanol Preparation Marianne Bore Haarr, Emil Lindbäck, Torfinn Håland, * and Magne O. Sydnes * Department of Mathematics and Natural
General Assembly 2014 Vienna Austria 27 April 02 May 2014
Irena Grgić 1, Zoran Kitanovski 2, Ana Kroflič 1 and Alen Čusak 3 1 Analytical Chemistry Laboratory, 2 Laboratory for Food Chemistry, National Institute of Chemistry, Ljubljana, Slovenia 3 EN-FIST Center