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1 ' : Document Control Uniqu;, ID RAPPORT D'ANALYSE DES MATIERES PREMIERES Code No.: L-130 / Spec. approuvees par!'assurance Qualite NOM DU PRODUIT: DISTRIBUTEUR: Lutein 5 TG (MFR) DSM Nutritional Products, Inc / LOTDUDISTRIBUTEUR: DATE D'EXPIRATION: / DATE DE RE-ANALYSE: NIA NO. DE RECEPTION: R-35274@ MANUFACTURIER: NO. DE LOTDU MAN.: DSM PAYS DE FABRICATION: Suisse QUANTITE RE<;UE: 30 x 5 kg / DESCRIPTION SPECIFICATION OBSERVATION COULEUR: Brun rouge Conforme ODEUR: Inodore ou legere odeur Legere odeur / FORME: Petits granules Conforme / ANALYSE METHODE SPECIFICATION RESULTAT PERTE DE POIDS (a 105 C) (thermogravimetrique) USP <891> * v ESSAI Marigold Calcul / Resultat X I 0 I 5 l / Entrer le resultat ci-dessus dans Visual Manufacturing SOLVANTS RESIDUELS USP <467> Rencontre!es nonnes Conforme ** / 1- RE _,_ VI_S E _ P _ A _ R _ : _-l- _; =..:,._--1.D A _ T _ E _ : : :)_ :..._.;_I +.:.._ -t 0 :_ REJETE 0 Produit certifie APPROU VE (.'\ Analyse par Laboval I PAR: *Se referer au certificat du manufacturier 1/ivicZI 'µ._s ** Se re1.erer " a I a J ettre de con fi rrmation Conh ole Qualite j DATE: RESUL TA TS ENTRES PAR: NES DATE: RELACHE P DATE:,)OJ-f-t()-3V a latj Os / Assurance Qualite.Jor}-{0-30
2 Certificat d'analyses Client: Date: CA: Att: Fax: Produit: Lutein 5 TG (MFR) Code: L-130 / Tests Description Couleur Forrne Odeur Teneur par UV Luteine t -Verifiepar: - Specifications Brun rouge Petits granules lnodore ou legere odeur.:5.0 Karim Koush, Ph. D. Approuve par: Resultats Conforme Conforme / Legere odeur / PO: Req: Lot: Page: page 1/1 Methodes Organoleptique Organoleptique Organoleplique 5.1./ Mari Gold CJ y\ lj l,. / \._ -. Fred Bakshi, B. Sc er 4r 46 ff MiS , 50e Avenue Lachine (Quebec) Canada H8T 2V5 Tel.: Telec.:
3 FLORAGLO LUTEIN 5 CWS/S-TG Certificate for Customer «at OosM Productcode : Lot No. : Analysis No. : CfC Number: Articlecode : Sales Name : Manufacturing Date : 07-DEC-2016 Best Use Before Date : 07-DEC-2019./ Delivery Note No. Destination : Customer Ref. No : Customer Article No: Customer Name: Canada Comment Quantity Shipped: KG Thank you for your order and continued business. DSM Nutritional Products is committed to delivering superior quality products and excellent services for our valued customers. If you have any questions, please contact our Account Service Center at Our webshop provides 24/7 access to the products and services of DSM Nutritional Products. Visit our website at: /unlimitednutrition-na.dsm.com DSM Nutritional Products, Inc. 45 Waterview Boulevard Parsippany, NJ U.S.A Date of issue: 05-0ct-2017
4 FLORAGLO LUTEIN 5 CWS/S-TG CERT/FICA TE OF ANALYSIS Productcode : Lot No. Analysis No. Test Appearance visual Colour visual Fineness (US standard sieves): - through sieve No. 20 / USP riddle screen sieving - through sieve No. 40 / USP riddle screen sieving - through sieve No. 100 / USP riddle screen sieving Result free-flowing particles red Loss on drying Halogen moisture analysis Residue on ignition 0.9 EP Dispersibility in water dispersible Dispersibility in water at 20 c Colour intensity of aqueous solution 107 A (1, 1cm) at maximum absorbance Photometer Assay total Carotenoids Photometer Assay Lutein Photometer ,/ Lutein 90.5 Zeaxanthin 7.9 Total rel. compounds (incl. Zeaxanthin) 8.8 Any other single related compound <1.0 Microbiological purity Total aerobic microbial count <10 3 Total combined yeast/moulds count <10 2 Limits/ Specifications free-flowing particles red reddish min. 100 min. 85 max. 15 max. 8 max. 2.0 dispersible min to to 6.0 min to 9.0 max < < ' < Dimension / Units (w/w) (w/w) CFU/g CFU/g DSM Nutritional Products Ltd Branch Site Sisseln Quality Management CH-4334 Sisseln I 1/2 Date of issue: 21-Dec-2016
5 FLORAGLO LUTEIN 5 CWS/S-TG OosM CERTIFICATE OF ANALYSIS Productcode : Lot No. Analysis No. Test Enterobacteria Escherichia coli Salmonella spp. Staphylococcus aureus Pseudomonas aeruginosa Result <10 negative in 25 g negative in 1 O g Limits/ Specifications <10 negative in 25 g negative in 1 O g Dimension / Units CFU/g This lot was analysed and released by our authorized Quality Control Department and was found to meet the specifications as given above. DSM Nutritional Products Ltd The Quality Assurance Manager Scherer Susanne DSM Nutritional Products Ltd Branch Site Sisseln Quality Management CH-4334 Sisseln 2/2 Date of issue: 21-Dec-2016
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7 Document Control Unique ID RAPPORT D'ANALYSE DES MATIERES PREMIERES Code No.: L-130 Spec. approuvees par )'Assurance Qualite ,/ Reevaluation NOM DU PRODUIT: Lutein 5 TG (MFR) DISTRIBUTEUR: DSM Nutritional Products, Inc LOT DU DISTRIBUTEUR: DATE D'EXPIRATION: DATE DE RE-ANALYSE: NIA... NO. DE RECEPTION: MANUFACTURIER: SM NO. DE LOT DU MAN.: PAYS DE FABRICATION: Suisse.,.- QUANTITE RE<;UE: 12 x 25 kg,,. DESCRIPTION SPECIFICATION OBSERVATION COULEUR: Brun rouge Brun rouge ODEUR: Inodore ou legere odeur Legere odeur / FORME: Petits granules Petits granules ANALYSE METHODE SPECIFICATION RESULTAT PERTE DE POIDS USP <891> (a 105 C) (thermogravimetrique) :5: ESSAI Marigold Calcul 5.0 Resultat X Entrer le resultat ci-dessus dans Visual Manufacturing SOLV ANTS RESIDUELS USP <467> Rencontre Jes normes Conforme, t REVISE PAR: h\ h. "' :--\ IDATE: lr-o;).- l REJETE D COMMENT AIRE( Analyse par Laboval t Solvants residuels analyses: - Dichloromethane (classe 2) : conforme - Hexane ( classe 2): conforme APPRO'GZl p AR: f DATE: RELACHEPAR: Controle Qualite clof&-o;:}.-d-{,j RESULT ATS ENTRES PAR: NES DATE: Assurance Qualite DATE:
8
9 Certificat d'analyses Client: Date: CA: Att: Fax: Produit: Luteln 6 TG (MFR) Code: L-130 Tests TeneurparW Luteine Solvants residuels Verifle par. Specifications 5.0 Resul tats 5:9 Dichloromethane: Rencont re les normes USP (Class II) Conforme les normes USP (Class II) Approuve par. /,/ PO: Req: Lot: Page: 1/1 Conforme / ' rf l - - \_, Fr akshi, B. Sc. Methodes Mari Gold USP <467>, Ed. courante f¼_ #:ttj(?:j-/3 jj-(;:-s , 50e Avenue Lachlne (Quebec) Canada H8T 2V5 Tel.: Telec.:
10 RAPPORT D'ANALYSE DES MATIERES PREMIERES Code No.: L-130 Spec. approuvees par!'assurance Qualite NOM DU PRODUIT: Lutein 5 TG (MFR) DISTRIBUTE UR: LOT DU DISTRIBUTEUR: DATE D'EXPIRATION: DATE DE RE-ANALYSE: NO. DE RECEPTION: - 55 d MANUFACTURIER: NO. DE LOT DU MAN.: PAYS DE FABRICATION: QUANTITE RE<;UE: (y DESCRIPTION SPECIFICATION OBSERVATION COULEUR: Brun rouge ODEUR: Inodore ou legere odeur FORME: Petits granules ANALYSE METHODE SPECIFICATION RESULTAT PERTE DE POIDS USP <891> (a 105 C) (thermogravimetrique) s; 8.0 ESSAI Marigold Calcul 25.0 Resu I tat X 1 0 Entrer le resultat ci-dessus clans Visual Manufacturing SOLVANTS RESIDUELS USP <467> Rencontre les normes REVISE PAR: COMMENT AIRE: IDATE: REJETE APPROUVE D PAR: Contrc,le Qualite DATE: RELACHE PAR: RESULTATS ENTRES PAR: DATE: DATE: Assurance Qualite
11 FLORAGLO LUTEIN 5 CWS/S-TG Certificate for Customer Productcode : Lot No. : Analysis No. : S CfC Number: Articlecode : Sales Name : Manufacturing Date : 28-SEP-2017 Best Use Before Date : 27-SEP-2020 Delivery Note No. Destination : Customer Ref. No : Customer Article No: L 130 Customer Name:.,, Comment Quantity Shipped: KG Thank you for your order and continued business. DSM Nutritional Products is committed to delivering superior quality products and excellent services for our valued customers. If you have any questions, please contact our Account Service Center at Our webshop provides 24/7 access to the products and services of DSM Nutritional Products. Visit our website at: DSM Nutritional Products, Inc. 45 Waterview Boulevard Parsippany, NJ U.S.A Date of issue: 27-Dec-2017
12 FLORAGLO LUTEIN 5 CWS/S-TG CERTIFICATE OF ANALYSIS Productcode : Lot No. Analysis No. (1) Test Appearance visual Colour visual Fineness (US standard sieves): - through sieve No. 20 / USP riddle screen sieving - through sieve No. 40 I USP riddle screen sieving - through sieve No. 100 / USP riddle screen sieving Loss on drying Halogen moisture analysis Residue on ignition EP Dispersibility in water Dispersibility in water at 20 c Result free-flowing particles reddish Colour intensity of aqueous solution 91 A (1,1cm) at maximum absorbance Photometer dispersible Assay total Carotenoids 6.1 Photometer Assay Lutein 5.5 Photometer Lutein 90.1 Zeaxanthin Total rel. compounds (incl. Zeaxanthin) 9.2 Any other single related compound <1.0 (percentage relative to total carotinoids} Microbiological purity Total aerobic microbial count <10 3 Total combined yeast/moulds count < Limits/ Specifications free-flowing particles red reddish min. 100 min. 85 max. 15 max. 8 max. 2.0 dispersible min to to 6.0 min to 9.0 max < < < Dimension / Units (w/w) (w/w) CFU/g CFU/g Date of issue : ao\6-0\ ct d-d
13 F-LORAGLO LUTEIN 5 CWS/S-TG CERT/FICA TE OF ANALYSIS Productcode : Lot No. Analysis No. Test Enterobacteria Escherichia coli Salmonella spp. Staphylococcus aureus Pseudomonas aeruginosa G) Result <10 negative in 25 g Limits/ Specifications <10 negative in 25 g Dimension / Units CFU/g This lot was analysed and released by our authorized Quality Control Department and was found to meet the specifications as given above. DSM Nutritional Products Ltd The Quality Assurance Manager Scherer Susanne./ DSM Nutritional Products Ltd 2 / 2 Date of issue : 20-0ct-2017 ra h i'.6. -i- 8. '.n_, G) 1½,()'-> \ f\)q\y '\9UQ(" J Ol'ltQ.( Qu d 0 d018- O\ O<; g? <:)t)\, () - d
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