Magruder Check Sample: 2016 Year End Summary
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1 Magruder Check Sample: 2016 Year End Summary
2 14 Samples in 2016 Sample Sample Name # Tests Micro Mix Grade Grade Liquid Thio S Urea Micros WS Micros Liquid Organic MAP MOP ZnSO Grade MAP plus S
3 Z-Cut Homogeneity Screening Sample Number Homogeneity Decision Pass Z Cut < 3%RSD Number of Pairs in Z Cut % Nitrogen Low n 13.0% PASS 1.0% Low *PASS Nitrogen 2.6% Low n 109.1% PASS 0.3% Low n 3.5% FAIL 10.3% PASS 0.0% Low *PASS Nitrogen 4.5% PASS 2.5% Low n 39.6% Low n 0.0% PASS 0.7% PASS 0.0%
4 2016 Z-Score Compliance ,612 Tests Action -3 > Z > 3 Warning Compliant -2 < Z < 2 Analyte 6.6% 4.4% 89.0% (419) (281) (5,689) Method 4.0% 2.7% 93.3% (217) (150) (5,123) Standard Normal 0.27% 4.28% 95.45%
5 2016 Labs Separated by Group International Private Public Number Labs Listed Number Participating Number of Individual Analytes Number of Individual Methods Z-Score Compliance Action -3 > Z > 3 7.0% 7.9% 5.0% Warning 4.8% 5.0% 3.5% Compliant -2 < Z < % 87.1% 91.5%
6 2016 Z-Score Compliance in Lab Groups N P K International Action 10.6% 4.5% 5.4% Private Public Warning 7.8% 4.1% 2.5% Compliant 81.6% 91.4% 92.1% Action 4.3% 9.1% 9.0% Warning 4.8% 3.8% 6.6% Compliant 90.9% 87.0% 84.3% Action 3.0% 7.9% 4.6% Warning 3.4% 3.9% 4.6% Compliant 93.7% 88.2% 90.9%
7 2016 N, P, K Participation by Lab Groups (# Tests) Code Analyte International Private Public 010 Total Nitrogen (%) Total Phosphorus as P2O5 (%) Direct Available Phosphorus as P2O5 050 Soluble Potassium as K2O (%)
8 # Tests Ammoniacal Nitrogen (%) Nitrate Nitrogen (%) Water Insoluble Nitrogen (%) 2016 Analyte: N, P, K Urea Nitrogen (%) Biuret Nitrogen (%) Urea (%) Biuret (%) Number of Tests Ammoniacal Plus Nitrate Nitrogen (%) Total Nitrogen (%) Total Phosphorus as P2O5 (%) Citrate Insoluble Phosphorus as P2O5 (%) Indirect Available Phosphorus as P2O5 (%) Direct Available Phosphorus as P2O5 (%) Water Soluble Orthophosphate as P2O5 (%) Water Soluble Phosphorus as P2O5 (%) Soluble Potassium as K2O (%)
9 # Tests Ammoniacal Nitrogen (%) 2016 Analyte: N, P, K by Group Nitrate Nitrogen (%) Water Insoluble Nitrogen (%) Urea Nitrogen (%) Biuret Nitrogen (%) Urea (%) Biuret (%) International Private Public Ammoniacal Plus Nitrate Nitrogen (%) Total Nitrogen (24%) Total Phosphorus as P2O5 (%) Citrate Insoluble Phosphorus as P2O5 (%) Indirect Available Phosphorus as P2O5 (5%) Direct Available Phosphorus as P2O5 (25%) Water Soluble Orthophosphate as P2O5 (%) Water Soluble Phosphorus as P2O5 (%) Soluble Potassium as K2O (4%)
10 # Tests Analyte: Other Elements Water (Free) (%) Acid Soluble Calcium (%) Acid Soluble Magnesium (%) Water Soluble Magnesium (%) Elemental Sulfur (%) Sulfate Sulfur, HCl soluble (%) Total Sulfur in Liquid (%) Total Sulfur in Urea/Formulations (%) Total Sulfur (%) Sulfur - HNO3 soluble (%) Acid Soluble Arsenic (ppm) Acid Soluble Boron (%) Water Soluble Boron (%) Acid Soluble Cadmium (ppm) Water Soluble Chlorine (%) Acid Soluble Chromium (ppm) Acid Soluble Cobalt (ppm) Acid Soluble Copper (%) Acid Soluble Iron (%) Acid Soluble Lead (ppm) Acid Soluble Manganese (%) Water Soluble Manganese (%) Acid Soluble Mercury (ppm) Acid Soluble Molybdenum (ppm) Acid Soluble Nickel (ppm) Acid Soluble Selenium (ppm) Sodium (%) Acid Soluble Zinc (%) Water Soluble Zinc (%) Number of Tests
11 # Tests Analyte: Other Elements by Group Water (Free) (%) Acid Soluble Calcium (%) Acid Soluble Magnesium (%) Water Soluble Magnesium (%) Elemental Sulfur (%) Sulfate Sulfur, HCl soluble (%) Total Sulfur in Liquid (%) Total Sulfur in Urea/Formulations (%) Total Sulfur (%) Sulfur - HNO3 soluble (%) Acid Soluble Arsenic (ppm) Acid Soluble Boron (%) Water Soluble Boron (%) Acid Soluble Cadmium (ppm) Water Soluble Chlorine (%) Acid Soluble Chromium (ppm) Acid Soluble Cobalt (ppm) Acid Soluble Copper (%) Acid Soluble Iron (%) Acid Soluble Lead (ppm) Acid Soluble Manganese (%) Water Soluble Manganese (%) Acid Soluble Mercury (ppm) Acid Soluble Molybdenum (ppm) Acid Soluble Nickel (ppm) Acid Soluble Selenium (ppm) Sodium (%) Acid Soluble Zinc (%) Water Soluble Zinc (%) International Private Public 184
12 2016 Methods: Nitrogen # Tests Ammoniacal Nitrogen, Magnesium Oxide Method (%) Ammoniacal Nitrogen, Other (%) Nitrate Nitrogen, Robertson (%) Nitrate Nitrogen, Jones Modified (%) Nitrate Nitrogen, Other (%) Water Insoluble Nitrogen, Method I (%) Water Insoluble Nitrogen, Other (%) Urea Nitrogen, Urease (as N) (%) Urea Nitrogen, Other (%) Biuret Nitrogen, Spectrophotometric (as N) (%) Biuret Nitrogen, Other (%) Urea, Urease (as Urea) (%) Urea, Other (%) Biuret, Spectrophotometric (as Biuret) (%) Biuret, Other (%) Ammoniacal Plus Nitrate Nitrogen, Devarda (%) Ammoniacal Plus Nitrate Nitrogen, Other (%) Total Nitrogen, Modified Comprehensive (%) Total Nitrogen, Salicylic (%) Total Nitrogen, Raney (%) Total Nitrogen, Comprehensive (%) Total Nitrogen, Combustion (%) Total Nitrogen, Other (%) Number of Tests 521
13 2016 Methods by Group: Nitrogen Ammoniacal Nitrogen, Magnesium Oxide Method Ammoniacal Nitrogen, Other Nitrate Nitrogen, Robertson Nitrate Nitrogen, Jones Modified Nitrate Nitrogen, Other Water Insoluble Nitrogen, Method I Water Insoluble Nitrogen, Other Urea Nitrogen, Urease (as N) Urea Nitrogen, Other Biuret Nitrogen, Spectrophotometric (as N) Biuret Nitrogen, Other Urea, Urease (as Urea) Urea, Other Biuret, Spectrophotometric (as Biuret) Biuret, Other Ammoniacal Plus Nitrate Nitrogen, Devarda Ammoniacal Plus Nitrate Nitrogen, Other Total Nitrogen, Modified Comprehensive Total Nitrogen, Salicylic Total Nitrogen, Raney Total Nitrogen, Comprehensive Total Nitrogen, Combustion Total Nitrogen, Other International Private Public Note 58 Indecisions on Method to Use
14 2016 Methods: Phosphorus # Tests Total Phosphorus as P2O5, Gravimetric Quinoli... (%) Total Phosphorus as P2O5, Spectrophotometric... (%) Total Phosphorus as P2O5, Alkalimetric Quinol... (%) Total Phosphorus as P2O5, Automated (%) Total Phosphorus as P2O5, ICP (%) Total Phosphorus as P2O5, Other (%) Citrate Insoluble Phosphorus as P2O5, Spectro... (%) Citrate Insoluble Phosphorus as P2O5, Automat... (%) Citrate Insoluble Phosphorus as P2O5, Other (%) Indirect Available Phosphorus as P2O5, Spectr... (%) Indirect Available Phosphorus as P2O5, Automa... (%) Indirect Available Phosphorus as P2O5, ICP (%) Indirect Available Phosphorus as P2O5, Other (%) Direct Available Phosphorus as P2O5, Gravimet... (%) Direct Available Phosphorus as P2O5, Gravimet... (%) Direct Available Phosphorus as P2O5, Spectrop... (%) Direct Available Phosphorus as P2O5, Spectrop... (%) Direct Available Phosphorus as P2O5, Automate... (%) Direct Available Phosphorus as P2O5, ICP (%) Direct Available Phosphorus as P2O5, ICP, Cit... (%) Direct Available Phosphorus as P2O5, Citrate-... (%) Direct Available Phosphorus as P2O5, Other (%) Water Soluble Orthophosphate as P2O5, Other (%) Water Soluble Phosphorus as P2O5, Gravimetric... (%) Water Soluble Phosphorus as P2O5, Spectrophot... (%) Water Soluble Phosphorus as P2O5, Automated (%) Water Soluble Phosphorus as P2O5, ICP (%) Water Soluble Phosphorus as P2O5, Other (%) Number of Tests
15 2016 Methods by Group: Phosphorus # Tests Total Phosphorus as P2O5, Gravimetric Quinolinium MolybdoP Total Phosphorus as P2O5, Spectrophotometric MolybdovanadoP Total Phosphorus as P2O5, Alkalimetric Quinolinium MolybdoP Total Phosphorus as P2O5, Automated Note: International vs Private Total Phosphorus as P2O5, ICP Total Phosphorus as P2O5, Other Citrate Insoluble Phosphorus as P2O5, Spectrophotometric MolybdovanadoP Citrate Insoluble Phosphorus as P2O5, Automated, test portion A-B International Private Public Citrate Insoluble Phosphorus as P2O5, Other Indirect Available Phosphorus as P2O5, Spectrophotometric Indirect Available Phosphorus as P2O5, Automated Note general lack of Interest! Indirect Available Phosphorus as P2O5, ICP Indirect Available Phosphorus as P2O5, Other
16 2016 Methods by Group: Phosphorus # Tests Direct Available Phosphorus as P2O5, Gravimetric Quinolinium Direct Available Phosphorus as P2O5, Gravimetric Quinolinium, Citrate- EDTA Ext. Direct Available Phosphorus as P2O5, Spectrophotometric Direct Available Phosphorus as P2O5, Spectrophotometric, Citrate-EDTA Ext. International Private Public Direct Available Phosphorus as P2O5, Automated Direct Available Phosphorus as P2O5, ICP Direct Available Phosphorus as P2O5, ICP, Citrate-EDTA Ext. Note lack of International Interest! Direct Available Phosphorus as P2O5, Citrate-EDTA Ext. Direct Available Phosphorus as P2O5, Other Water Soluble Orthophosphate as P2O5, Other Water Soluble Phosphorus as P2O5, Gravimetric Quinolinium Water Soluble Phosphorus as P2O5, Spectrophotometric Water Soluble Phosphorus as P2O5, Automated Note lack of Public Lab Interest! Water Soluble Phosphorus as P2O5, ICP Water Soluble Phosphorus as P2O5, Other
17 2016 Methods: Potassium # Tests Soluble Potassium as K2O, STPB Oxalate (%) Soluble Potassium as K2O, AA (Oxalate) (%) Soluble Potassium as K2O, AA (Citrate) (%) Number of Tests Soluble Potassium as K2O, AA (Citrate-EDTA) (%) Soluble Potassium as K2O, ICP (Oxalate) (%) Soluble Potassium as K2O, ICP (Citrate) (%) Soluble Potassium as K2O, ICP (Citrate-EDTA) (%) Soluble Potassium as K2O, Flame Photometric (... (%) This is a red flag Soluble Potassium as K2O, Flame Photometric (... (%) Soluble Potassium as K2O, Flame Photometric (... (%) Soluble Potassium as K2O, Other (%)
18 2016 Methods by Group: Potassium Soluble Potassium as K2O, STPB Oxalate Soluble Potassium as K2O, AA (Oxalate) Soluble Potassium as K2O, AA (Citrate) International Private Public Soluble Potassium as K2O, AA (Citrate-EDTA) Soluble Potassium as K2O, ICP (Oxalate) Soluble Potassium as K2O, ICP (Citrate) Soluble Potassium as K2O, ICP (Citrate-EDTA) Soluble Potassium as K2O, Flame Photometric (Oxalate) Soluble Potassium as K2O, Flame Photometric (Citrate) Not sure of Methods To Use Soluble Potassium as K2O, Flame Photometric (Citrate- EDTA) Soluble Potassium as K2O, Other
19 Elemental Sulfur, Gravimetric Sulfur - carbon disulfide soluble sulfur 2016 Methods by Group: Sulfur Elemental Sulfur, Other Sulfate Sulfur, HCl soluble, Gravimetric Sulfur - sulfate form Sulfate Sulfur, HCl soluble, Other International Private Public Total Sulfur in Liquid, Gravimetric - sulfate, sulfite, thiosulfate, and elemental Total Sulfur in Liquid, Other Total Sulfur in Urea/Formulations, Other (Identify) Total Sulfur, Combustion Total Sulfur, Gravimetric - sulfate and elemental Total Sulfur, ICP, w/br digestion Total Sulfur, ICP, test portion as in modified w/9:3 HNO3:HCl Total Sulfur, Other Note a lot of interest in OTHER! Sulfur - HNO3 soluble, ICP
20 2016 Methods by Group: Calcium # Tests Acid Soluble Calcium, AA, inorganic Acid Soluble Calcium, AA, , test portion A-C w/dual acid International Private Public Acid Soluble Calcium, ICP, test portion inorganic Acid Soluble Calcium, ICP, test portion A-C Acid Soluble Calcium, ICP, test portion A-C, w/dual acid Acid Soluble Calcium, Other
21 2016 Methods by Group: Magnesium Acid Soluble Magnesium, AA, inorganic Acid Soluble Magnesium, AA, , test portion A-C w/dual acid International Private Public Acid Soluble Magnesium, ICP, test portion inorganic Acid Soluble Magnesium, ICP, test portion A- C Acid Soluble Magnesium, ICP, test portion A- C, w/dual acid Acid Soluble Magnesium, Other Water Soluble Magnesium, AA Water Soluble Magnesium, ICP
22 2016 Methods by Group: Zinc Acid Soluble Zinc, AA, inorganic Acid Soluble Zinc, AA, organic Acid Soluble Zinc, AA, , test portion A-C w/dual acid International Private Public Acid Soluble Zinc, ICP, test portion inorganic Acid Soluble Zinc, ICP, test portion A-C Acid Soluble Zinc, ICP, test portion A-C, w/dual acid Acid Soluble Zinc, Other Water Soluble Zinc, AA Water Soluble Zinc, ICP Water Soluble Zinc, Other
23 Performance Against Guarantee Sample Code Analyte Guarantee Measured Micro Mix Boron 1.50% Copper 3% Iron 18% Manganese 7.50% Molybdenum 200 ppm Zinc 7% Grade Nitrogen 24% DA Phosphate 25% Potassium 4% Grade Nitrogen 5% DA Phosphate 2% Potassium 0% Liquid Thio S Potassium 25% 25.10% Total Sulfur 17% Urea Nitrogen 46% Micros Total Sulfur 9% Boron 1% Copper 1% Manganese 4% Zinc 20% 20.04
24 Performance Against Guarantee Sample Code Analyte Guarantee Measured WS Nitrogen 25.00% DA Phosphate 5% Potassium 15% Magnesium 0.10% Total Sulfur 0.13% Boron 0.025% Copper % Iron 0.125% Manganese 0.063% Molybdenum 125 ppm Zinc 0.063% Micros Nitrogen 12% DA Phosphate 12% Potassium 12% Total Sulfur 9% Boron 0.1% Copper 0.1% Iron 0.5% Manganese 0.4% Molybdenum 250 ppm Zinc 2% 2.013
25 Performance Against Guarantee Sample Code Analyte Guarantee Measured Liquid Organic Nitrogen 5% DA Phosphate 20% Potassium 4% Magnesium 0.05% Boron 0.02% Iron 0.05% 0.16 Manganese 0.2% Molybdenum 30 ppm Zinc 0.03% MAP Nitrogen 11% DA Phosphate 52% MOP Potassium 61% Chlorine 47% ZnSO Total Sulfur 17% Zinc 35% Grade Nitrogen 32% DA Phosphate 0% Potassium 10% Iron 2% MAP plus S Nitrogen 12% DA Phosphate 40% 41.4 Total Sulfur 10% Only 9 Labs participated
26 What Would You Like to See? Questions?
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