Choose for Your Instrument. GC Supplies - Shimadzu Instrument Quick Pick Guide

Transcription

1 Choose for Your Instrument GC Supplies - Shimadzu Instrument Quick Pick Guide Syringes Septa Inlet Liners O-rings and Sealing Rings SilTite FingerTite Ferrules Ferrules Replacement Parts

2 Your chromatography analysis does not end with the selection of the GC column. The combination of components selected for your instrument also make an important contribution to successful separations. SGE brings technology and chromatography expertise to improve your chromatography. SGE Supplies for Sample Preparation, Sample Introduction, and Separation SAMPLE INTRODUCTION - Syringes Our involvement in all areas of chromatography provides us with a unique understanding of your requirements enabling us to optimize syringe design for sample introduction. All our syringes, both manual and autosampler, incorporate SGE s Diamond Syringe Technology offering significantly improved levels of durability, clarity and accuracy. SGE has a comprehensive range of syringe options including plunger protection, removable or fixed needles, a range of needle gauge and length options as well as needle-tip style alternatives. SAMPLE INTRODUCTION - Septa The role of septa for GC analysis is key as many chromatographic problems are caused as a result of inappropriate septa material or inappropriate handling of the septa. Desired septa attributes: Reliably seal against the carrier gas pressure in the inlet. Capable of being pierced and resealed time after time. Capable of being pierced by the syringe needle without pieces of the septa being deposited in the GC inlet system. Must not contaminate or bleed material into the chromatographic system. SAMPLE INTRODUCTION GC Inlet Liners The GC Inlet liner is where the sample is introduced and vaporized into the gaseous phase. The design of the liner is crucial, as is liner deactivation, to ensure reproducible and accurate chromatography. SEPARATION - GC Connections (ferrules and fittings) SGE manufactures an array of connection types for GC use. Poorly defined or selected connections can lead to an increase in dead volume, leaks from cycled temperatures and mismatched tubing sizes.

3 Instrument Quick Pick for Shimadzu Autosampler Syringes All needles are 42 mm long with a cone point style. Shimadzu AOC14, AOC17 and AOC20 Volume Needle Gauge (OD mm) Syringe Code Syringe Pack Size Spare Needle Pack Size Spare Plunger Fixed Needle 5 µl 26 (0.47) 5F-S-0.47C µl 23 (0.63) 5F-S-0.63C Removable Needle 0.5 µl 26 (0.47) 0.5BR-S-0.47C * 0.5 µl 23 (0.63) 0.5BR-S-0.63C * 10 µl 26 (0.47) 10R-S-0.47C µl 23 (0.63) 10R-S-0.63C µl Gas Tight 23 (0.63) 10R-S-GT-0.63C *Denotes spare Needle and Plunger kit. Pack Size Septa SGE has a number of different septa materials: Enduro Blue = For non-demanding routine applications. EC = Combines significantly longer injection life, low bleed and low injection port adhesion. HT = Bleed and temperature optimized, combined with outstanding mechanical properties. Type Material Durability Resealing Solvent Resistance Enduro Blue Tear Resistance Maximum Temperature High Temperature Silicone Excellent Excellent Excellent Excellent 350 C EC High Temperature Silicone Excellent Excellent Excellent Excellent 400 C HT BTO Silicone Excellent Excellent Excellent Excellent 400 C Septum Type Pack Size For Shimadzu 9A, 14, 15A, 16, 17A, 2010 & 2014 Enduro Blue EC HT Inlet Liners Length Description and Geometry Sketch OD (mm) ID (mm) Pack Size (mm) For GC-2010 (SPL-2010 Injector), GC-2014 (SPL-2014 Injector) and GC-17A (SPL-17 Injector) Split / Splitless FocusLiner * Split / Splitless Tapered FocusLiner * Split / Splitless FocusLiner Split / Splitless Tapered FocusLiner

4 Inlet Liners Continued Description and Geometry Sketch OD (mm) ID (mm) Length (mm) Pack Size ConnecTite Liner Standard ConnecTite Liner Top Hole ConnecTite Liner Bottom Hole Split, straight-through liner Splitless straight-through liner Split / Splitless with Single Taper Split / Splitless with middle gooseneck Split / Splitless with recessed gooseneck and quartz wool Split / Splitless with middle gooseneck ConnecTite (0.53 mm ID columns) SPME Liner For GC-14(SPL-14 Injector) Split / Splitless FocusLiner Split / Splitless Tapered FocusLiner Split / Splitless with 2.0 mm middle gooseneck Split / Splitless with single taper Splitless, Direct, wide bore liner for Shimadzu 9A/16A GC * When using a standard 42 mm needle for autosamplers, the sample will be injected on top of the wool for this liner. O-rings and Sealing Rings Description Usage Pack Size Viton O-ring Can be used at temperatures up to 300 C. For 2010 & 2014 (SPL-2010 Injector & SPL Injector). Graphite Sealing Ring Can be used at temperatures up to 450 C. For 14, 15A & 16 (SPL-14 injector) Graphite Sealing Ring Can be used at temperatures up to 450 C. For 17A (SPL-17 injector)

5 SilTite FingerTite Ferrules Description Pack Size SilTite Fingertite Shimadzu 2010 INJ / FID Starter Kit * SilTite Fingertite Shimadzu 2010 INJ / MS Starter Kit * SilTite Fingertite Ferrule 0.4 mm Replacement Items SilTite Fingertite Ferrule 0.5 mm Replacement Items SilTite Fingertite Blanking Ferrule Replacement Items SilTite Fingertite Female Nut Replacement Items * Each starter kit includes all the parts necessary to convert one GC system (one injector and one detector) to the SilTite FingerTite system suitable for installing mm ID capillary columns. In addition there are five SilTite FingerTite nuts, one packet (ten ferrules) of 0.4 mm ID SilTite FingerTite ferrules and a ferrule install tool which allows you to seat the ferrule in the correct position on the capillary column. Ferrules Column ID Description Pack Size GC14A, GC17A, GC2010 and GC2014 Detector / Injectors (Not for MS interfaces or QP2010 Injector) mm ID columns 100% Graphite mm ID columns 100% Graphite mm OD packed columns 100% Graphite mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules n/a SilTite Metal Nuts - Slotted QP5000/5050 Standard MS Interface QP5000-I mm ID columns 15% Graphite/ 85% Vespel Ferrules QP5000-I 0.32 mm ID columns 15% Graphite/ 85% Vespel Ferrules QP5000-II & QP mm ID columns 15% Graphite/ 85% Vespel Ferrules QP5000-II & QP mm ID columns 15% Graphite/ 85% Vespel Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules n/a SilTite Metal Nuts-QP5000/5050 Standard MS interface QP5000/5050 Wide Bore MS Interface, QP2010 Injector and QP2010 Standard MS Interface mm ID columns 15% Graphite/ 85% Vespel Ferrules mm ID columns 15% Graphite/ 85% Vespel Ferrules mm ID columns 15% Graphite/ 85% Vespel Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules n/a SilTite Metal Nuts * Includes ten ferrules, two SilTite nuts. Replacement Parts Material Pack Size Replacement SilTite Nuts For 2010 GC-MS System For 2010 GC-MS System with QP5000 series MS For 2010/2014 GC Injectors and atmospheric detectors QP5000 Jet Separator MS Interface QP5000 Direct MS Interface For All Injectors Jet Separator (Starter Kit), except 2010/

6 SGE's involvement in gas chromatography includes the support we give to our customers. Technical Support Contact us at for technical support information. Our Website is a detailed source for information on chromatography, applications and SGE products. It also profiles the latest posters and materials developed by our technical experts based around the world. SGE Product Selection Guide Our product selection guide can be accessed at BR-0373-C_RevE SGE Analytical Science Pty Ltd 07/2013 AUSTRALIA AND PACIFIC REGION SGE Analytical Science Pty Ltd Toll Free: Tel: +61 (0) Fax: +61 (0) support@sge.com JAPAN SGE Japan Inc Tel: +81 (0) Fax: +81 (0) japan@sge.com EUROPE SGE Europe Ltd Tel: +44 (0) Fax: +44 (0) Tel France: +33 (0) Tel Germany: +49 (0) 6155 / europe@sge.com UNITED STATES OF AMERICA SGE Inc Toll Free: Tel: Fax: usa@sge.com