CERTIFICATE OF ANALYSIS - GC PROFILING
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1 Date : May 22, 2018 CERTIFICATE OF ANALYSIS - GC PROFILING SAMPLE IDENTIFICATION Internal code : 18E08-NAD3-1-CC Customer identification : Grapefruit Oil Pink - R Type : Essential oil Source : Citrus x paradisi cv. Pink Customer : TruIQ Global, LLC ANALYSIS Method: PC-PA J19 - Analysis of the composition of an essential oil, or other volatile liquid, by FAST GC-FID (in French); identifications validated by GC-MS. Analyst : Benoit Roger, Ph. D. Analysis date : May 15, 2018 Checked and approved by : Sylvain Mercier, M. Sc., chimiste This report is digitally signed, it is only considered valid if the digital signature is intact. Page 1/9
2 PHYSICOCHEMICAL DATA Physical aspect: Bright orange liquid Refractive index: ± (20 C) CONCLUSION No adulterant, contaminant or diluent has been detected using this method. Page 2/9
3 ANALYSIS SUMMARY Identification DB-5 (%) DB-WAX (%) Classe Toluene tr tr* Simple phenolic Heptanal tr tr Aliphatic aldehyde α-thujene tr [tr]* Monoterpene α-pinene Monoterpene Camphene tr tr Monoterpene β-pinene 0.39* 0.06 Monoterpene Sabinene [0.39]* 0.33 Monoterpene Heptanol tr tr* Aliphatic alcohol Myrcene Monoterpene Octanal 0.33* 0.31 Aliphatic aldehyde α-phellandrene [0.33]* 0.03 Monoterpene Δ3-Carene 0.01 Monoterpene Limonene 94.32* Monoterpene 1,8-Cineole [94.32]* 0.21* Monoterpenic ether β-phellandrene [94.32]* [0.21]* Monoterpene para-cymene [94.32]* 0.06 Monoterpene (Z)-β-Ocimene Monoterpene (E)-β-Ocimene Monoterpene γ-terpinene Monoterpene cis-sabinene hydrate Monoterpenic alcohol Octanol Aliphatic alcohol Terpinolene Monoterpene 6,7-Epoxymyrcene tr tr Monoterpenic ether Linalool Monoterpenic alcohol Nonanal Aliphatic aldehyde trans-para-mentha-2,8-dien-1-ol Monoterpenic alcohol cis-limonene oxide Monoterpenic ether cis-para-mentha-2,8-dien-1-ol * Monoterpenic alcohol (Z)-Myroxide 0.01* [tr]* Monoterpenic ether trans-limonene oxide [0.01]* 0.01 Monoterpenic ether (E)-Myroxide tr 0.04* Monoterpenic ether Citronellal Monoterpenic aldehyde Terpinen-4-ol 0.01 tr Monoterpenic alcohol Cryptone tr tr Normonoterpenic ketone α-terpineol * Monoterpenic alcohol trans-isopiperitenol tr tr Monoterpenic alcohol Decanal Aliphatic aldehyde Octyl acetate 0.04 [0.04]* Aliphatic ester trans-carveol tr 0.01 Monoterpenic alcohol Neral 0.08 [0.08]* Monoterpenic aldehyde Geranial Monoterpenic aldehyde Undecanal 0.01 tr Aliphatic aldehyde α-terpinyl acetate Monoterpenic ester Limonene hydroperoxide IV tr Monoterpenic peroxide Neryl acetate tr 0.01 Monoterpenic ester α-copaene Sesquiterpene Geranyl acetate 0.09* 0.06 Monoterpenic ester β-cubebene [0.09]* 0.04 Sesquiterpene Page 3/9
4 β-elemene * Sesquiterpene Dodecanal Aliphatic aldehyde β-caryophyllene 0.28 [0.28]* Sesquiterpene α-humulene Sesquiterpene (E)-β-Farnesene Sesquiterpene Germacrene D 0.04 [0.11]* Sesquiterpene Bicyclogermacrene * Sesquiterpene α-muurolene 0.01 [0.02]* Sesquiterpene Cubebol tr tr Sesquiterpenic alcohol δ-cadinene Sesquiterpene α-elemol Sesquiterpenic alcohol (E)-Nerolidol tr tr Sesquiterpenic alcohol Germacrene D-4-ol Sesquiterpenic alcohol Caryophyllene oxide Sesquiterpenic ether β-sinensal Sesquiterpenic aldehyde Myristic acid Aliphatic acid Nootkatone Sesquiterpenic ketone Palmitic acid Aliphatic acid Bergapten tr Furanocoumarin Osthole 0.01 Coumarin Linoleic acid Aliphatic acid Oleic acid Aliphatic acid Stearic acid Aliphatic acid 7-Methoxy-8-(2-formyl-2- methylpropyl)coumarin tr Coumarin Isoauraptene 0.02 Coumarin Meranzin 0.04 Coumarin Auraptenol 0.01 Coumarin Auraptene 0.10 Coumarin Epoxyaurapten 0.04 Coumarin Tangeretin 0.01 Flavonoid Total identified 99.39% 99.37% *: Two or more compounds are coeluting on this column [xx]: Duplicate percentage due to coelutions, not taken account in the identified total tr: The compound has been detected below 0.005% of total signal. Note: no correction factor was applied Page 4/9
5 This page was intentionally left blank. The following pages present the complete data of the analysis. Page 5/9
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8 FULL ANALYSIS DATA Identification Column DB-5 Column DB-WAX R.T R.I % R.T R.I % Toluene tr 1.43* 1001 tr Heptanal tr tr α-thujene tr 1.43* 1001 [tr] α-pinene Camphene tr tr β-pinene 3.58* Sabinene 3.58* 967 [0.39] Heptanol tr 6.86* 1426 tr Myrcene Octanal 4.08* α-phellandrene 4.08* 1000 [0.33] Δ3-Carene Limonene 4.63* ,8-Cineole 4.63* 1036 [94.32] 3.41* β-phellandrene 4.63* 1036 [94.32] 3.41* 1176 [0.21] para-cymene 4.63* 1036 [94.32] (Z)-β-Ocimene (E)-β-Ocimene γ-terpinene cis-sabinene hydrate Octanol Terpinolene ,7-Epoxymyrcene tr tr Linalool Nonanal trans-para-mentha-2,8- dien-1-ol cis-limonene oxide cis-para-mentha-2,8- dien-1-ol * (Z)-Myroxide 6.13* * 1426 [tr] trans-limonene oxide 6.13* 1131 [0.01] (E)-Myroxide tr 7.08* Citronellal Terpinen-4-ol tr Cryptone tr tr α-terpineol * trans-isopiperitenol tr tr Decanal Octyl acetate * 1442 [0.04] trans-carveol tr Neral * 1626 [0.08] Geranial Undecanal tr α-terpinyl acetate Limonene hydroperoxide IV tr Neryl acetate tr Page 8/9
9 α-copaene Geranyl acetate 9.85* β-cubebene 9.85* 1382 [0.09] β-elemene * Dodecanal β-caryophyllene * 1542 [0.28] α-humulene (E)-β-Farnesene Germacrene D * 1650 [0.11] Bicyclogermacrene * α-muurolene * 1672 [0.02] Cubebol tr tr δ-cadinene α-elemol (E)-Nerolidol tr tr Germacrene D-4-ol Caryophyllene oxide β-sinensal Myristic acid Nootkatone Palmitic acid Bergapten tr Osthole Linoleic acid Oleic acid Stearic acid Methoxy-8-(2-formyl tr methylpropyl)coumarin Isoauraptene Meranzin Auraptenol Auraptene Epoxyaurapten Tangeretin Total identified 99.39% 99.37% Total reported 99.39% 99.37% *: Two or more compounds are coeluting on this column [xx]: Duplicate percentage due to coelutions, not taken account in the identified total tr: The compound has been detected below 0.005% of total signal. Note: no correction factor was applied R.T.: Retention time (minutes) R.I.: Retention index Page 9/9
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