GC/MS BATCH NUMBER: C90110
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1 GC/MS BATCH NUMBER: C90110 ESSENTIAL OIL: CHAMOMILE ROMAN BOTANICAL NAME: CHAMAEMELUM NOBILE ORIGIN: UNITED KINGDOM KEY CONSTITUENTS PRESENT IN THIS BATCH OF CHAMOMILE ROMAN OIL % 3-METHYLAMYL ANGELATE 16.6 METHALLYL ANGELATE 13.3 ISOBUTYL ANGELATE METHYLBUTYL ANGELATE 7.4 trans-pinocarveol 7.2 ISOAMYL ANGELATE METHYLAMYL ISOBUTYRATE + β-thujone 4.4 α-pinene 4.1 PINOCARVONE METHYLAMYL METHACRYLATE METHYLBUTYL ISOBUTYRATE 1.7 ISOBUTYL ISOBUTYRATE 1.2 Comments from Robert Tisserand: Delightful fine, powdery floral odor profile. Constituents are in expected amounts for English Chamomile. No red flags nd St S. Twin Falls, ID * * planttherapy.com facebook.com/planttherapy * planttherapy.com/blog
2 Date : April 10, 2017 SAMPLE IDENTIFICATION Internal code : 17D03-PTH1-1-DM Customer identification : Roman Chamomile - United Kingdom - C R Type : Essential oil Source : Chamaemelum nobile Customer : Plant Therapy ANALYSIS Method : PC-PA E06, "Analysis of the composition of a liquid essential oil by GC-FID" (in French). Analyst : Sylvain Mercier, M. Sc., chimiste Analysis date : Checked and approved by : Alexis St-Gelais, M. Sc., chimiste Note: This report may not be published, including online, without the written consent from Laboratoire PhytoChemia. This report is digitally signed, it is only considered valid if the digital signature is intact. Page 1 of 6
3 IDENTIFIED COMPOUNDS Identification Column: BP5 Column: WAX R.T. R.I. % % R.I. R.T. Molecular Class Ethanol Aliphatic alcohol 2-Methylbutyral Aliphatic aldehyde Isoamyl alcohol * Aliphatic alcohol 2-Methylbutyl alcohol [0.51] * Aliphatic alcohol (E)-2-Penten-1-ol Aliphatic alcohol Ethyl isobutyrate Aliphatic ester Methyl 2-methylbutyrate 1.41* Aliphatic ester Isobutyl acetate 1.41* 771 [0.13] Aliphatic ester Butyric acid 1.41* 771 [0.13] Aliphatic acid Hexanal Aliphatic aldehyde Methyl angelate Aliphatic ester Ethyl 2-methylbutyrate Aliphatic ester 3-Methylpentanol Aliphatic alcohol Propyl isobutyrate Aliphatic ester cis-hex-3-en-1-ol Aliphatic alcohol Isoamyl acetate Aliphatic ester Hexanol * Aliphatic alcohol 2-Methylbutyl acetate Aliphatic ester Ethyl angelate? Aliphatic ester Isobutyl isobutyrate 3.22* Aliphatic ester Tricyclene 3.22* 917 [1.31] Monoterpene α-pinene 3.41* Monoterpene Prenyl acetate 3.41* 928 [4.34] Aliphatic ester C. nobile biomarker [0.51] * Aliphatic ester Isobutyl methacrylate Aliphatic ester Camphene Monoterpene Propyl 2-methylbutyrate Aliphatic ester Thuja-2,4(10)-diene * Monoterpene Methallyl methacrylate Aliphatic ester Sabinene [0.12] * Monoterpene β-pinene Monoterpene Isoamyl propionate Aliphatic ester Dehydro-1,8-cineole 4.41* Monoterp. ether Methallyl isobutyrate 4.41* 988 [0.47] Aliphatic ester Myrcene 4.41* 988 [0.47] Monoterpene Propyl angelate Aliphatic ester Isobutyl 2-methylbutyrate * Aliphatic ester Isobutyl isovalerate [0.51] * Aliphatic ester Isoamyl isobutyrate [2.67] * Aliphatic ester 2-Methylbutyl isobutyrate [2.67] * Aliphatic ester meta-cymene Monoterpene Page 2 of 6
4 para-cymene Monoterpene Limonene Monoterpene β-phellandrene Monoterpene 1,8-Cineole [2.67] * Monoterp. ether Isoamyl methacrylate * Aliphatic ester 2-Methylbutyl [1.83] * Aliphatic ester methacrylate Isobutyl angelate * Aliphatic ester γ-terpinene Monoterpene Prenyl isobutyrate Aliphatic ester Methallyl angelate Aliphatic ester 3-Methylamyl propionate? * Aliphatic ester Terpinolene [1.83] * Monoterpene Unknown (m/z = 69, 41 (59), 67 (32), 68 (27), 53 (12) (5)) Aliphatic ester Butyl angelate Aliphatic ester Isobutyl tiglate [0.08] * Aliphatic ester Isoamyl 2-methylbutyrate [9.10] * Aliphatic ester 2-Methylbutyl 2- methylbutyrate 6.59* [9.10] * Aliphatic ester Linalool 6.59* 1105 [0.48] Monoterp. alcohol α-thujone Monoterp. ketone Methallyl tiglate? * Aliphatic ester 3-Methylamyl isobutyrate 6.90* [4.64] * Aliphatic ester β-thujone 6.90* 1117 [4.43] Monoterp. ketone α-campholenal Monoterp. aldehyde trans-pinocarveol Monoterp. alcohol 3-Methylamyl methacrylate Aliphatic ester Isoamyl angelate Aliphatic ester 2-Methylbutyl angelate Aliphatic ester Camphene hydrate Monoterp. alcohol C. nobile biomarker [0.65] * Aliphatic ester Pinocarvone Monoterp. ketone Isoborneol Monoterp. alcohol Isopinocamphone Monoterp. alcohol Borneol * Monoterp. alcohol Terpinen-4-ol Monoterp. alcohol Isobutyl 3-hydroxy-2- methylenebutyrate * Aliphatic ester Prenyl angelate Aliphatic ester Myrtenal Monoterp. aldehyde Isoamyl tiglate 9.24* [0.65] * Aliphatic ester Myrtenol 9.24* 1201 [0.64] [0.49] * Monoterp. alcohol Page 3 of 6
5 3-Methylamyl valerate 9.42* Aliphatic ester α-terpineol 9.42* 1205 [0.97] Monoterp. alcohol Verbenone Monoterp. ketone 2-Hydroxy-2-methylbut * Aliphatic ester enyl 2-methyl-(2Z)- butenoate + 3-Methylamyl angelate 3-Methylamyl angelate [16.88] * Aliphatic ester Bornyl acetate Monoterp. ester Isoamyl 3-hydroxy Aliphatic ester methylenebutyrate 3-Methylamyl tiglate * Aliphatic ester α-copaene Sesquiterpene C. nobile biomarker Aliphatic ester β-caryophyllene [0.31] * Sesquiterpene trans-β-farnesene [0.55] * Sesquiterpene Germacrene D [0.55] * Sesquiterpene β-selinene Sesquiterpene Bicyclogermacrene Sesquiterpene α-muurolene Sesquiterpene (E,E)-α-Farnesene * Sesquiterpene δ-cadinene Sesquiterpene trans-cadina-1,4-diene [0.36] * Sesquiterpene (E,E)-Matricaria ester? Polyyne Spathulenol Sesquiterp. alcohol Copaborneol Sesquiterp. alcohol Chamazulene Azulene Total identified 97.54% 96.49% *: Two or more compounds are coeluting on this column [xx]: Duplicate percentage due to coelutions, not taken account in the identified total Note: no correction factor was applied OTHER DATA Physical aspect : Faintly blue liquid Refractive index : ± (20 C) CONCLUSION No adulterant, contaminant or diluent were detected using this method. Page 4 of 6
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