Customer : Comments and Conclusions : Daniel Dantin - Laboratory director
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1 - Page 1/5 - Customer : ANN HARMAN Circle H Institute 5951 RIVERBEND BAY FRUITLAND, WA USA Sample Nature : ESSENTIAL OIL Botanical name : THYMUS CITRIODORA Common name : THYMUS CITRODORUS Batch number : 1262 Origin : - Plant part : PLANT FLOWERED Our reference : N930 Recept : 5/10/2017 Analysis date : 10/18/2017 Packaging : Amber flask of 2 ml Requested analysis : Classic GC + classification Sample storage : 1 year - - room temperature Comments and Conclusions : Report validated by : Daniel Dantin - Laboratory director
2 - Page 2/5 - GAS CHROMATOGRAPHY (according to the norm NF ISO 11024) Analysis conditions :. GC 6890 / MS 5973 Column : VF WAX (polar) 60 m * 0.25 mm * 0.5 µm. GC 6890 FID Column : VF WAX (polar) 60 m * 0.25 mm * 0.5 µm. Temperature program : 60 C (6 min) 2 C/min 250 C (20min). Carrier gas : He (23 psis/ms 30 psis/fid). Sample injection / split : 1 µl of 10 % solution in hexane. Mass range : 30 to Oil compounds are identified by a combination of retention times (our own database) and mass spectra library NKS records. Percentages are calculated from GC/FID peaks areas without using corrections factors Chromatographic profile : Norm. 500 FID1 A, (U:\CIRCLEH\1262N930.D) min
3 - Page 3/5 - % Norm ETHANOL ACETONE TRICYCLENE alpha-pinene alpha-thuyene CAMPHENE beta-pinene SABINENE PINADIENE delta3-carene HEPTANONE beta-myrcene alpha-phellandrene alpha-terpinene LIMONENE CINEOLE Cis-beta-OCIMENE gamma-terpinene Trans-beta-OCIMENE OCTANONE p-cymene TERPINOLENE CYMENE ISOMER METHYL-5-HEPTEN-2-ONE ALIPHATIC ESTER ROSE cis-oxide NONANONE TERPENIC ESTER OCTANOL PHOTOCITRAL ISOMER PERILLENE COMPOUND Mw= OCTEN-3-OL Trans-THUYANOL NERYL OXIDE COMPOUND Mw= ISOGERANIAL NONANOL ISONERAL CAMPHOR beta-bourbonene PHOTOCITRAL A LINALOOL NONEN-3-OL PHOTOCITRAL B 0.51
4 - Page 4/5 - % Norm epsilon-cadinene BORNYL ACETATE alpha-trans-bergamotene METHYL THYMOL ETHER beta-caryophyllene TERPINENE-4-OL METHYL CARVACROL ETHER Cis-DIHYDROCARVONE ALLO-AROMADENDRENE FARNESENE ISOMER FARNESENE ISOMER alpha-humulene E-beta-FARNESENE SESQUITERPENE LAVANDULOL NERAL Z-beta-FARNESENE GERANYL FORMATE BORNEOL GERMACRENE D ALIPHATIC ALCOHOL CARVONE beta-bisabolene GERANIAL alpha-farnesene delta-cadinene GERANYL ACETATE CITRONELLOL beta-sesquiphellandrene alpha-bisabolene NERYL PROPIONATE NERYL ISOBUTYRATE NEROL Cis-ISOGERANIOL Trans-ISOGERANIOL NERYL BUTYRATE GERANYL PROPIONATE GERANIOL GERANYL ISOBUTYRATE GERANYL BUTYRATE NERYL METHYLBUTYRATE alpha-phellandrene ISOMER ISOCARYOPHYLLENE EPOXIDE ALIPHATIC ESTER CARYOPHYLLENE EPOXIDE 0.34
5 - Page 5/5 - % Norm GERANYL COMPOUND GERMACRA-1,5-DIEN-4-OL ALIPHATIC ESTER SPATHULENOL T-CADINOL THYMOL SESQUITERPENOL CARVACROL alpha-bisabolol alpha-cadinol NEOCEMBRENE NERIC ACID CARYOPHYLLA-3,7-DIEN-6-OL GERANIC ACID MENTHADIENOL ISOMER DITERPENE Mw= AROMATIC COMPOUND SESQUITERPENOL AROMATIC COMPOUND Mw= CEMBRENE INCENSOL PALMITIC ACID 0.03 TOTAL
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