60 8 weeks = 25 2 year weeks = 25 2 year
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1 Formula Book
2 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED. 2 Formula stability Check 2 Year Shelf Life at Room Temperature should be examined...but it s too long! Something faster test methods needed Acceleration Test at Higher Temp 60 8 weeks = 25 2 year weeks = 25 2 year
3 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED. 3 How to judge whether formula is stable or not? SUNJIN suggests 5 criteria for the stability of Fabric Softener formulation 1. Phase separation 2. Sedimentation 3. White Scum(=Halo effect) 4. Severe change of viscosity of formula 5. Severe change of color of formula If you see any of these, the formula is no good
4 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED. 4 How to judge whether formula is stable or not? SUNJIN suggests 5 criteria for the stability of Fabric Softener formulation 1. Phase separation 2. Sedimentation 3. White Scum(=Halo effect) 4. Severe change of viscosity of formula 5. Severe change of color of formula <Example> Phase separation noticed : No Good
5 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED. 5 How to judge whether formula is stable or not? SUNJIN suggests 5 criteria for the stability of Fabric Softener formulation 1. Phase separation 2. Sedimentation 3. White Scum(=Halo effect) 4. Severe change of viscosity of formula 5. Severe change of color of formula <Example> Sedimentation at the bottom noticed : No Good
6 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED. 6 How to judge whether formula is stable or not? SUNJIN suggests 5 criteria for the stability of Fabric Softener formulation 1. Phase separation 2. Sedimentation White Scum 3. White Scum(=Halo effect) 4. Severe change of viscosity of formula 5. Severe change of color of formula <Example> White scum on the surface noticed : No Good
7 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED. 7 How to judge whether formula is stable or not? SUNJIN suggests 5 criteria for the stability of Fabric Softener formulation 1. Phase separation 2. Sedimentation 3. White Scum(=Halo effect) 4. Severe change of viscosity of formula 5. Severe change of color of formula <Example> Viscosity increased significantly noticed : No Good
8 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED. 8 How to judge whether formula is stable or not? SUNJIN suggests 5 criteria for the stability of Fabric Softener formulation 1. Phase separation 2. Sedimentation 3. White Scum(=Halo effect) 4. Severe change of viscosity of formula 5. Severe change of color of formula Before After <Example> Color paled significantly noticed : No Good
9 Regular Type Fabric Softener Formula
10 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED. 10 Thickeners Used: ACUSOL882 : Nonionic Thickener A hydrophobically modified, nonionic polyol (HEURs) thickener and stabilizer used in detergent formulations for household and industrial applications, providing outstanding rheology and excellent chemical compatibility. Flosoft 222 : Polymer Thickener Cationic acrylamide-based polymer used as a thickening agent for acidic aqueous compositions, and particularly in domestic detergents and laundry softeners. White creamy water-in-oil emulsion typically used ar a concentration range between 0.1% and 5.0% in fabric softener compositions.
11 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED cps Regular 100cps ver1.0 Step Trade Name REMARK TE90 TEQ90 CEQ90 CTN90 PEQ90HV D.I-Water Aqua Dye Dye SUNQAT Ester Quat FS-222 Thickener Fragrance Fragrance Kathone CG Preservative weeks@45, 7 weeks@60 stability tests passed
12 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED cps Regular 300cps ver1.0 Step Trade Name REMARK TE90 TEQ90 CEQ90 CTN90 PEQ90HV D.I-Water Aqua Dye Dye SUNQAT Ester Quat FS-222 Thickener Fragrance Fragrance Kathone CG Preservative weeks@45, 7 weeks@60 stability tests passed
13 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED cps Regular 500cps ver1.0 Step Trade Name REMARK TE90 TEQ90 CEQ90 CTN90 PEQ90HV D.I-Water Aqua Dye Dye SUNQAT Ester Quat FS-222 Thickener Fragrance Fragrance Kathone CG Preservative weeks@45, 7 weeks@60 stability tests passed
14 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED cps Regular 1000cps ver1.0 Step Trade Name REMARK TE90 TEQ90 CEQ90 CTN90 PEQ90HV D.I-Water Aqua Dye Dye SUNQAT Ester Quat FS-222 Thickener Fragrance Fragrance Kathone CG Preservative weeks@45, 7 weeks@60 stability tests passed
15 Concentrated Type Formula
16 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED. 16 Viscosity control agent: CaCl2 Calcium Chloride : Reduction of surface tension \ The presence of calcium chloride reduce the surface activity to a greater extent above the critical micelle concentration region of cationic surfactant. Ageing effects due to the salts affected the surface tension, probably by reason of the tendency of a solution to take in water by osmosis.
17 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED cps Concentrated 200cps ver1.0 Step Trade Name REMARK TE90 TEQ90 CEQ90 CTN90 1 D.I-Water Aqua Dye Dye DB-110A Anti foam LA-9N Emulsifier SUNQAT Ester Quat CaCl2 Viscosity Fragrance Fragrance Kathone CG Preservative weeks@45, 4 weeks@60 stability tests passed
18 Copyright 2013 by SUNJIN Chemical Co. LTD ALL RIGHTS RESERVED cps Concentrated 3500cps ver1.0 Step Trade Name REMARK TE90 TEQ90 CEQ90 CTN90 1 D.I-Water Aqua Dye Dye DB-110A Anti foam LA-9N Emulsifier SUNQAT Ester Quat CaCl2 Viscosity Fragrance Fragrance Kathone CG Preservative weeks@45, 4 weeks@60 stability tests passed
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