Analytical Results SC Laboratories Oregon LLC ORELAP# 4133/OLCC# D SW 74th Ave Suite 110, Tigard, OR

Transcription

1 Sample Name: Tested for: Durban Poison SoFresh Farms Compliance - Usable Laboratory ID: 18D Matrix: Useable Marijuana Sample Metrc ID: 1A E Lot # GH R DP Batch RFID: 1A E Batch Size: (g) Date Extracted: 04/04/18 Date Analyzed: 04/04/18 Strain: Durban Poison Date Sampled: 04/03/18 10:04 Date Accepted: 04/03/18 s Valid Until: 04/03/19 Potency Analysis Analysis Method/SOP: Potency * - ORELAP certified analyte Cannabinoids % weight mg/g Cannabinoids Profile Total THC ((THCA*0.877)+d9) Total CBD ((CBDA*0.877)+CBD) 3.41 d9-thc (d9-tetrahydrocannabinol)* 34.1 d8-thc (d8-tetrahydrocannabinol)* THCA (d9-tetrahydrocannabinolic Acid)* CBD (Cannabidiol)* CBDA (Cannabidiolic Acid)* CBN (Cannabinol)* CBG (Cannabigerol)* 0.68 CBGA (Cannabigerolic Acid) 6.8 CBDV (Cannabidivarin)* CBDVA (Cannabidivarinic Acid) CBC (Cannabichromene)* THCV (Tetrahydrocannabivarin) Total Cannabinoids Water Activity and Moisture THC 3.41 THCA CBGA 0.68 Total: Analyte Units LOQ Analyzed Method Water Activity AW /04/2018 Water Activity Percent Moisture % /04/2018 Moisture Cannabinoids reported as dry weight (moisture corrected) s above the action level are highlighted in red #. <LOQ - s below the of Quantitation - Compound not detected Page 1 of 16 04/06/ :40

2 Sample Name: Tested for: Durban Poison SoFresh Farms Compliance - Usable Date Sampled: 04/03/18 10:04 Date Accepted: 04/03/18 s Valid Until: 04/03/19 Laboratory ID: 18D Matrix: Useable Marijuana Lot # GH R DP Strain: Durban Poison Sample Metrc ID: 1A E Batch RFID: 1A E Batch Size: (g) Terpene Analysis Date Extracted: 04/04/18 Date Analyzed: 04/04/18 Analysis Method/SOP: Potency Analyte (%) LOQ Analyte LOQ alpha Pinene Myrcene alpha Phellandrene Carene alpha Terpinene Limonene Terpinolene Linalool Fenchol Borneol Terpineol Geraniol alpha Humulene beta Caryophyllene Caryophyllene Oxide alpha Bisabolol Camphene beta Pinene Ocimene Sabinene Camphor Isoborneol Menthol alpha Cedrene Nerolidol R-(+)-Pulegone Eucalyptol p-cymene (-)-Isopulegol Geranyl Acetate Guaiol Valencene Phytol Citronellol gamma-terpinene <LOQ - s below the of Quantitation - Compound not detected Terpene Analysis is not ORELAP Accredited. Total Terpenes % Page 2 of 16 04/06/ :40

3 Sample Name: Tested for: Durban Poison SoFresh Farms Compliance - Usable Laboratory ID: 18D Matrix: Useable Marijuana Terpene Profile Date Sampled: 04/03/18 10:04 Date Accepted: 04/03/18 11:20 s Valid Until: 04/03/19 Client/Metrc ID: 1A E alpha Pinene Myrcene alpha Phellandrene 3-Carene alpha Terpinene Limonene Terpinolene Linalool Fenchol Borneol Terpineol Geraniol alpha Humulene beta Caryophyllene Caryophyllene Oxide alpha Bisabolol Camphene beta Pinene Ocimene Sabinene Camphor Isoborneol Menthol alpha Cedrene Nerolidol R-(+)-Pulegone Eucalyptol p-cymene (-)-Isopulegol Geranyl Acetate Guaiol Valencene Phytol Citronellol gamma-terpinene % Page 3 of 16 04/06/ :40

4 Sample Name: Tested for: Durban Poison SoFresh Farms Compliance - Usable Date Sampled: 04/03/18 10:04 Date Accepted: 04/03/18 s Valid Until: 04/03/19 Laboratory ID: 18D Matrix: Useable Marijuana Lot # GH R DP Date Analyzed: Strain: Durban Poison Pesticide Analysis in ppm Sample Metrc ID: 1A E Batch RFID: 1A E Batch Size: (g) Date Extracted: 04/04/18 Analysis Method/SOP: Pesticides Analyte 04/04/18 s above the action levels are highlighed in red #. Action LOQ Analyte Action LOQ Abamectin Acephate Acequinocyl Acetamiprid Aldicarb Azoxystrobin Bifenazate Bifenthrin Boscalid Carbaryl Carbofuran Chlorantraniliprole Chlorfenapyr Chlorpyrifos Clofentezine Cyfluthrin Cypermethrin Daminozide DDVP (Dichlorvos) Diazinon Dimethoate Ethoprophos Etofenprox Etoxazole Fenoxycarb Fenpyroximate Fipronil Flonicamid Fludioxonil Hexythiazox Imazalil Imidacloprid Kresoxim-methyl Malathion Metalaxyl Methiocarb Methomyl Methyl parathion MGK Myclobutanil Naled Oxamyl Paclobutrazol Permethrins (total) Phosmet Piperonyl butoxide Prallethrin Propiconazole Propoxur Pyrethrins (total) Pyridaben Spinosad Spiromesifen Spirotetramat Spiroxamine Tebuconazole Thiacloprid Thiamethoxam Trifloxystrobin <LOQ - s below the of Quantitation - Compound not detected Page 4 of 16 04/06/ :40

5 Case Narrative Terpenes- Alpha Humulene and Phytol exceeded normally accepted QC criteria in the sample duplicate. Due to relatively large variations in very small values calculated high. Batch: B Potency/Terpenes Potency Blank(B BLK1) Extracted - 04/04/18 9:24 Analyzed - 04/04/18 17:33 d9-thc (d9-tetrahydrocannabinol) % d8-thc (d8-tetrahydrocannabinol) % THCA (d9-tetrahydrocannabinolic Acid) % CBD (Cannabidiol) % CBDA (Cannabidiolic Acid) % CBN (Cannabinol) % CBG (Cannabigerol) % CBGA (Cannabigerolic Acid) % CBDV (Cannabidivarin) % CBDVA (Cannabidivarinic Acid) % CBC (Cannabichromene) % THCV (Tetrahydrocannabivarin) % Duplicate(B DUP1) Extracted - 04/04/18 9:24 Analyzed - 04/04/18 17:50 d9-thc (d9-tetrahydrocannabinol) 3.19 % d8-thc (d8-tetrahydrocannabinol) % 20 THCA (d9-tetrahydrocannabinolic Acid) % CBD (Cannabidiol) % 20 CBDA (Cannabidiolic Acid) 0.04 % CBN (Cannabinol) % 20 CBG (Cannabigerol) 0.05 % CBGA (Cannabigerolic Acid) 0.64 % CBDV (Cannabidivarin) % 20 CBDVA (Cannabidivarinic Acid) 0.05 % CBC (Cannabichromene) % 20 THCV (Tetrahydrocannabivarin) 0.11 % LCS(B BS1) Extracted - 04/04/18 9:24 Analyzed - 04/05/18 10:00 Page 5 of 16 04/06/ :40

6 Potency (Continued) Batch: B Potency/Terpenes (Continued) LCS(B BS1) Extracted - 04/04/18 9:24 Analyzed - 04/05/18 10:00 d9-thc (d9-tetrahydrocannabinol) 0.05 % CBD (Cannabidiol) 0.04 % CBDA (Cannabidiolic Acid) 0.04 % CBN (Cannabinol) 0.04 % Page 6 of 16 04/06/ :40

7 Pesticide Analysis Batch: B Pesticide Prep Blank(B BLK1) Extracted - 04/04/18 9:20 Analyzed - 04/04/18 15:48 Abamectin ppm Acephate ppm Acequinocyl ppm Acetamiprid ppm Aldicarb ppm Azoxystrobin ppm Bifenazate ppm Bifenthrin ppm Boscalid ppm Carbaryl ppm Carbofuran ppm Chlorantraniliprole ppm Chlorfenapyr ppm Chlorpyrifos ppm Clofentezine ppm Cyfluthrin ppm Cypermethrin ppm Daminozide ppm DDVP (Dichlorvos) ppm Diazinon ppm Dimethoate ppm Ethoprophos ppm Etofenprox ppm Etoxazole ppm Fenoxycarb ppm Fenpyroximate ppm Fipronil ppm Flonicamid ppm Fludioxonil ppm Hexythiazox ppm Imazalil ppm Imidacloprid ppm Kresoxim-methyl ppm Malathion ppm Metalaxyl ppm Page 7 of 16 04/06/ :40

8 Pesticide Analysis (Continued) Batch: B Pesticide Prep (Continued) Blank(B BLK1) Extracted - 04/04/18 9:20 Analyzed - 04/04/18 15:48 Methiocarb ppm Methomyl ppm Methyl parathion ppm MGK-264 ppm Myclobutanil ppm Naled ppm Oxamyl ppm Paclobutrazol ppm Permethrins (total) ppm Phosmet ppm Piperonyl butoxide ppm Prallethrin ppm Propiconazole ppm Propoxur ppm Pyrethrins (total) ppm Pyridaben ppm Spinosad ppm Spiromesifen ppm Spirotetramat ppm Spiroxamine ppm Tebuconazole ppm Thiacloprid ppm Thiamethoxam ppm Trifloxystrobin ppm LCS(B BS1) Extracted - 04/04/18 9:20 Analyzed - 04/05/18 10:02 Acephate 0.95 ppm Acetamiprid 0.92 ppm Aldicarb 0.82 ppm Bifenazate 0.93 ppm Boscalid 0.82 ppm Chlorantraniliprole 0.91 ppm Chlorpyrifos 0.88 ppm Cyfluthrin 1.07 ppm Page 8 of 16 04/06/ :40

9 Pesticide Analysis (Continued) Batch: B Pesticide Prep (Continued) LCS(B BS1) Extracted - 04/04/18 9:20 Analyzed - 04/05/18 10:02 DDVP (Dichlorvos) 1.24 ppm Ethoprophos 0.91 ppm Etoxazole 0.76 ppm Fenoxycarb 0.85 ppm Flonicamid 0.99 ppm Imazalil 1.04 ppm Imidacloprid 1.03 ppm Methiocarb 0.91 ppm Myclobutanil 0.94 ppm Oxamyl 0.95 ppm Paclobutrazol 0.93 ppm Piperonyl butoxide 0.80 ppm Prallethrin 0.91 ppm Propoxur 0.87 ppm Spiromesifen 0.81 ppm Spiroxamine 0.49 ppm Thiacloprid 0.87 ppm Thiamethoxam 0.86 ppm Trifloxystrobin 0.87 ppm Matrix (B MS1) Extracted - 04/04/18 9:20 Analyzed - 04/04/18 16:20 Acephate 1.31 ppm Acetamiprid 1.58 ppm Aldicarb 1.46 ppm Bifenazate 1.70 ppm Boscalid 1.90 ppm Chlorantraniliprole 1.68 ppm Chlorpyrifos 1.62 ppm Cyfluthrin 2.09 ppm DDVP (Dichlorvos) 1.60 ppm Ethoprophos 1.58 ppm Etoxazole 1.55 ppm Fenoxycarb 1.49 ppm Flonicamid 1.51 ppm Page 9 of 16 04/06/ :40

10 Pesticide Analysis (Continued) Batch: B Pesticide Prep (Continued) Matrix (B MS1) Extracted - 04/04/18 9:20 Analyzed - 04/04/18 16:20 Imazalil 1.83 ppm Imidacloprid 1.87 ppm Methiocarb 1.49 ppm Myclobutanil 1.64 ppm Oxamyl 1.32 ppm Paclobutrazol 1.51 ppm Piperonyl butoxide 1.50 ppm Prallethrin 1.57 ppm Propoxur 1.39 ppm Spiromesifen 1.43 ppm Spiroxamine 0.82 ppm Thiacloprid 1.51 ppm Thiamethoxam 1.40 ppm Trifloxystrobin 1.66 ppm Matrix Dup(B MSD1) Extracted - 04/04/18 9:20 Analyzed - 04/04/18 Acephate 1.31 ppm Acetamiprid 1.70 ppm Aldicarb 1.55 ppm Bifenazate 1.65 ppm Boscalid 1.76 ppm Chlorantraniliprole 1.50 ppm Chlorpyrifos 1.57 ppm Cyfluthrin 2.32 ppm DDVP (Dichlorvos) 1.68 ppm Ethoprophos 1.56 ppm Etoxazole 1.50 ppm Fenoxycarb 1.40 ppm Flonicamid 1.53 ppm Imazalil 1.76 ppm Imidacloprid 2.03 ppm Methiocarb 1.46 ppm Myclobutanil 1.61 ppm Oxamyl 1.31 ppm Page 10 of 16 04/06/ :40

11 Pesticide Analysis (Continued) Batch: B Pesticide Prep (Continued) Matrix Dup(B MSD1) Extracted - 04/04/18 9:20 Analyzed - 04/04/18 Paclobutrazol 1.48 ppm Piperonyl butoxide 1.46 ppm Prallethrin 1.56 ppm Propoxur 1.50 ppm Spiromesifen 1.45 ppm Spiroxamine 0.86 ppm Thiacloprid 1.65 ppm Thiamethoxam 1.43 ppm Trifloxystrobin 1.54 ppm Page 11 of 16 04/06/ :40

12 Moisture Content Batch: B Gravimetric Duplicate(B DUP1) Extracted - 04/04/18 11:23 Analyzed - 04/04/18 11:23 Percent Moisture 12.5 % Batch: B Water Activity Duplicate(B DUP1) Extracted - 04/04/18 12:54 Analyzed - 04/04/18 12:54 Water Activity AW Batch: B Potency/Terpenes Blank(B BLK1) Extracted - 04/04/18 9:27 Analyzed - 04/04/18 18:18 alpha Pinene % Myrcene % alpha Phellandrene % 3-Carene % alpha Terpinene % Limonene % Terpinolene % Linalool % Fenchol % Borneol % Terpineol % Geraniol % alpha Humulene % beta Caryophyllene % Caryophyllene Oxide % alpha Bisabolol % Camphene % beta Pinene % Ocimene % Sabinene % Camphor % Isoborneol % Menthol % alpha Cedrene % Page 12 of 16 04/06/ :40

13 Terpene Analysis (Continued) Batch: B Potency/Terpenes (Continued) Blank(B BLK1) Extracted - 04/04/18 9:27 Analyzed - 04/04/18 18:18 Nerolidol % R-(+)-Pulegone % Eucalyptol % p-cymene % (-)-Isopulegol % Geranyl Acetate % Guaiol % Valencene % Phytol % Citronellol % gamma-terpinene % Duplicate(B DUP1) Extracted - 04/04/18 9:27 Analyzed - 04/04/18 18:18 alpha Ocimene % 20 alpha Terpineol % beta Ocimene % beta Terpineol % 20 cis-nerolidol % 20 Phytol 1 % 20 Phytol % trans-nerolidol % 20 alpha Pinene % Myrcene % alpha Phellandrene % Carene % alpha Terpinene % Limonene % Terpinolene % Linalool % 20 Fenchol % 20 Borneol % 20 Terpineol % Geraniol % alpha Humulene % Page 13 of 16 04/06/ :40

14 Terpene Analysis (Continued) Batch: B Potency/Terpenes (Continued) Duplicate(B DUP1) Extracted - 04/04/18 9:27 Analyzed - 04/04/18 18:18 beta Caryophyllene % Caryophyllene Oxide % 20 alpha Bisabolol % 20 Camphene % 20 beta Pinene % Ocimene % 20 Sabinene % 20 Camphor % 20 Isoborneol % 20 Menthol % 20 alpha Cedrene % 20 Nerolidol % 20 R-(+)-Pulegone % Eucalyptol % 20 p-cymene % 20 (-)-Isopulegol % Geranyl Acetate % Guaiol % Valencene % Phytol % Citronellol % 20 gamma-terpinene % Page 14 of 16 04/06/ :40

15 . Client: Sofresh Farms Client License: D6B6 Date: 4/3/2018 Thermometer ID: T014 Location: S Gribble Rd, Canby, OR Requestor: Andrew Montgomery Event ID: 18D005 Balance ID: SAMP_BAL_02 Sampling SOP: SC-OR-SAMP-003 Sampler: Scott Forster Transporter: Scott Forster Hygrometer ID: Anemometer_02 Lab ORELAP ID: 4133 Weight used (g) Weight Set ID Acceptance Criteria Initial Measured Initial P/F Final Measured Final P/F Lab OLCC ID: D 0.5 SAMP_CAL_02 ±2.5% P 200 ±2.5% Container Type METRC Harvest/Processing Lot ID #: Product Type Client Sample Name Product Date Batch Size (g) P Rubber Bin GH R1 PNC 3/20/2018 Usable Marijuana Peaches n Cream 3/20/ METRC Batch ID Product Temp ( C) Humidity (%) # of Containers Sample Media # Zones # of Inc. 1 Sample Size (g) Sample Name 1A E Mylar Bag Peaches n Cream Primary Lab Sample ID Container ID Increment Zone Sampling Media Wt. (g) Wt. Inc+Media (g) Increment Weight (g) Sample METRC ID# 18D Peaches n Cream-1 A A E D Peaches n Cream-1 A A E D Peaches n Cream-1 A A E D Peaches n Cream-1 A A E D Peaches n Cream-1 A A E D Peaches n Cream-1 A A E D Peaches n Cream-1 A A E D Peaches n Cream-1 A A E D Peaches n Cream-1 A A E Minimum Sample Size = 27.3g (Usable Marijuana Only) Total Sample Mass = 27.7 Observations and Abnormalities: Batch # Marks/Labels Cont. Types/Sizes Uniform Plant Colors Shape and Size Sampling Plan Container Type METRC Harvest/Processing Lot ID #: Product Type Client Sample Name Product Date Batch Size (g) Rubber Bin GH R DP Usable Marijuana Durban Poison 11/27/ METRC Batch ID Product Temp ( C) Humidity (%) # of Containers Sample Media # Zones # of Inc. 1 Sample Size (g) Sample Name 1A E Mylar Bag Durban Poison Primary Lab Sample ID Container ID Increment Zone Sampling Media Wt. (g) Wt. Inc+Media (g) Increment Weight (g) Sample METRC ID# 18D Durban Poison-1 A A E D Durban Poison-1 A A E D Durban Poison-1 A A E D Durban Poison-1 A A E D Durban Poison-1 A A E D Durban Poison-1 A A E D Durban Poison-1 A A E

16 . Minimum Sample Size = 9.1g (Usable Marijuana Only) Total Sample Mass = Batch # Marks/Labels Cont. Types/Sizes Uniform Plant Colors Shape and Size Sampling Plan Observations and Abnormalities:

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