Standard Operating Procedures Listing for TestAmerica Irvine
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1 Standard Operating Procedures Listing for TestAmerica Irvine Department Document Number Revision Active Date SOP Title EXTRACTIONS IR-EXT-SIGEL-PAH 2 4/11/2014 SILICA GEL CLEAN-UP FOR PAHs EXTRACTIONS IR-EXT-3520C 2 8/1/2014 EPA METHOD 3520C AND EPA METHOD 625 (CONTINUOUS LIQUID-LIQUID EXTRACTION) EXTRACTIONS IR-EXT /17/2014 EPA METHOD 3546 MICROWAVE EXTRACTION OF SOLIDS EXTRACTIONS IR-EXT /7/2014 SEPARATORY FUNNEL EXTRACTION AND CLEAN-UP PROCEDURES FOR DIESEL-RANGE ORGANICS, ORGANOCHLORINE PESTICIDES, PCBS, AND NITROSAMINES IN WATER (EPA 3510C) EXTRACTIONS IR-EXT-3580A 3 11/21/2014 EPA METHOD 3580A Waste Dilution EXTRACTIONS IR-EXT-1664_SPE 5 6/29/2015 EXTRACTIONS IR-EXT /24/2015 EXTRACTIONS IR-EXT /25/2015 EXTRACTIONS IR-EXT /23/2015 EXTRACTIONS IR-EXT-IGNITE 3 9/24/2015 IGNITABILITY IN SOIL GC_GCMS_SEMI_DW IR-GCS /14/2014 GC_GCMS_SEMI_DW IR-MSS-525_2 4 11/14/2014 GC_GCMS_SEMI_DW IR-MSS-548_1 5 11/14/2014 GC_GCMS_SEMI_DW IR-GCS-552_2 5 4/3/2015 GC_GCMS_SEMI_DW IR-GCV /3/2015 GC_GCMS_SEMI_DW IR-GCS /6/2015 GC-BTEX IR-GCA /3/2015 GC-BTEX IR-GCV /4/2015 GRAVIMETRIC DETERMINATION OF N-HEXANE EXTRACTABLE MATERIAL AND SILICA GEL TREATED N- HEXANE EXTRACTABLE MATERIAL IN WATER BY SOLID PHASE EXTRACTION (SPE) EPA METHOD 1010 (PENSKY-MARTENS CLOSED-CUP METHOD FOR DETERMINING IGNITABILITY) GRAVIMETRIC DETERMINATION OF N-HEXANE EXTRACTABLE MATERIAL AND SILICA GEL TREATED N- HEXANE EXTRACTABLE MATERIAL IN WATER HEM and STG-HEM IN SOLID SAMPLES, EPA 9071B MOD/EPA 3550C MOD EPA 505 (DETERMINATION OF ORGANOHALIDE PESTICIDES AND POLYCHLORINATED BIPHENYL (PCBs) EPA METHOD (ORGANIC COMPOUNDS BY LIQUID- SOLID EXTRACTION AND GAS CHROMATOGRAPGY/MASS SPECTROMETRY) EPA METHOD 548.1( DETERMINATION OF ENDOTALL IN DRINKING WATER BY ION EXCHANGE EXTRACTION, ACIDIC METHANOL METHYLATION AND GCMS) EPA METHOD (DETERMINATION OF HALOACETIC ACIDS IN DW BY LIQUID-LIQUID EXTRACTION, DERIVATIZATIONS BY GC) EPA METHOD (EDB, DBCP, AND 123TCP IN WATER BY MICROEXTRACTION AND GAS CHROMATOGRAPHY) EPA METHOD (DETERMINATION OF CHLORINATED ACIDS IN DW BY 515.4) DETERMINATION OF TOTAL GASEOUS NON-METHANE ORGANIC COMPOUNDS AS CARBON USING GAS CHROMATOGRAPHY SAMPLE PREPARATION and the DETERMINATION OF DISSOLVED GASES in WATER using GAS CHROMATOGRAPHY HEADSPACE EQUILIBRATION TECHNIQUE (RSK-175) GC-BTEX IR-GCV /6/2015 GASOLINE RANGE ORGANICS (GRO) / BTEX GCMS-SEMI IR-MSS-8270C_ /31/2013 EPA METHOD 8270C (SEMI-VOLATILE ORGANIC COMPOUNDS)/EPA METHOD 625 (BASE/NEUTRALS AND ACIDS) Revised /6
2 GCMS-SEMI IR-MSS-14DIOX 2 9/12/2014 1,4-DIOXANE BY 8270C MODIFIED SCAN MODE GCMS-SEMI IR-MSS-TEL 2 10/17/2014 TETRAETHYLLEAD BY GCMS EPA 8270C MOD GCMS-SEMI IR-MSS-NITROSA 4 6/3/2015 NITROSAMINES BY GC/MS USING CHEMICAL IONIZATION (EPA 1625C MODIFIED) GCMS-SEMI IR-MSS-PAHSIM 3 9/22/2015 PAHs COMPOUNDS BY EPA 8270C SELECTIVE ION MONITORING (SIM) MODE GCMS-VOL IR-MSV-123TCP 5 11/14/2014 1,2,3-Trichloropropane by GCMS SIM MODE, EPA GCMS-VOL IR-MSV /14/2014 EPA METHOD (PURGEABLE ORGANIC COMPOUNDS) GCMS-VOL IR-MSV-PREP 3 10/17/2014 VOLATILE ORGANIC PREPARATION (EPA 5030B, 5030C & 5035) GCMS-VOL IR-MSV-8260_ /2/2015 EPA METHOD 8260B/624/TPH BY GCMS (VOLATILE ORGANIC COMPOUNDS) GCMS-VOL IR-MSV-SIM 3 8/3/2015 Volatile Organic Compounds by GCMS-SIM, EPA 8260B ORGANOCHLORINE PESTICIDES BY GC (EPA METHODS GC-SEMI IR-GCS-PEST 2 3/7/ & 8081A) GC-SEMI IR-GCS-8015_D 3 11/14/2014 GC-SEMI IR-GCV-ALC 3 1/23/2015 GC-SEMI IR-GCS-PCBs 3 6/15/2015 HPLC_DW IR-HP /7/2014 HPLC_DW IR-HP /9/2015 EPA METHOD 8015B AND MODIFIED FOR DHS LUFT (TOTAL PETROLOLEUM HYDROCARBONS AS DIESEL ) EPA METHOD 8015B ( METHANOL AND ETHANOL BY GC) EPA METHOD 8082/608 (POLYCHLORINATED BIPHENYLS (PCBS) BY GC) EPA (Measurement of Carbamates in Water by Direct Aqueous Injection HPLC with Post Column Derivatization) EPA 547 (DETERMINATION OF GLYPHOSATE IN DW DIRECT-AQUEOUS INJECTION HPLC W/POST COLUMN DERIVATIZATION & FLUORESCENCE DETECTION) HPLC_DW IR-HP /16/2014 HPLC_DW IR-HP-549_2 5 10/19/2015 Inorganic Prep IR-WET-TURB 6 11/14/2014 INORGANIC PREP IR-WET-PH 6 11/21/2014 Determination of Carbonyl Compounds by Derivatization and HPLC-UV Detection (EPA Method 8315A) EPA (DETERMINATION OF DIQUAT & PARAQUAT IN DW BY LIQUID-SOLID EXTRACTION AND HPLC-UV DETECTION) TURBIDITY, NEPHELOMETRIC (EPA METHOD AND STANDARD METHOD 2130B) EPA METHOD 150.1/ 9040B/9040C/ 9041A/9045C/SM4500- H+B (ELECTROMETRIC ph) INORGANIC PREP IR-WET-ODOR 7 11/28/2014 THRESHOLD ODOR (SM 2150B) INORGANIC PREP IR-PREP /5/2014 ACID DIGESTION OF SOLIDS FOR TOTAL METALS BY ICP and ICPMS (EPA METHOD 3050B) INORGANIC PREP IR-PREP-ORP 2 3/7/2014 STANDARD METHOD 2580B (OXIDATION REDUCTION POTENTIAL) INORGANIC PREP IR-MET-CEC 3 4/25/2014 EPA METHOD 9081A CATION-EXCHANGE CAPACITY OF SOILS (SODIUM ACETATE) INORGANIC PREP IR-MET-TCLP_SPLP_VOL 1 6/30/2014 INORGANIC PREP IR-MET-STLC 1 9/5/2014 INORGANIC PREP IR-WET-COLOR 6 10/9/2015 INORGANIC PREP IR-MET-PREP_W 4 10/30/2015 TOXICITY CHARACTERISTIC LEACHING PROCEDURE (TCLP), SYNTHETIC PRECIPITATION LEACHING PROCEDURE (SPLP) FOR VOLATILES EPA METHODS 1311 and 1312 For Metals and Non-volatile Organics STLC/ WET EXTRACTION (TITLE 22, SECTION , APPENDIX III) SM 2120B (COLOR, COLORIMETRIC-PLATINUM-COBALT) ACID DIGESTION OF WATER FOR TOTAL RECOVERABLE OR DISSOLVED METALS BY ICP AND ICP/MS (EPA METHODS 200.2, 3005A AND 3010A) INORGANIC PREP IR-WET-FE2 6 10/30/2015 FERROUS IRON BY SM 3500Fe-B & D MODIFIED INORGANIC PREP IR-WET-SETT 4 8/3/2015 SETTLEABLE MATTER (SM2540F) Revised /6
3 INORGANIC PREP IR-MET-TCLP_SPLP_NV 2 11/6/2015 INORGANIC PREP IR-PREP-WASH 6 11/6/2015 GLASSWARE WASHING TOXICITY CHARACTERISTIC LEACHING PROCEDURE (TCLP), SYNTHETIC PRECIPITATION LEACHING PROCEDURE (SPLP) FOR NON-VOLATILES EPA METHODS 1311 and 1312 For Metals and Non-volatile Organics METALS IR-MET-ICPMS 4 10/7/2014 METALS BY ICP/MS (EPA METHOD & EPA 6020) METALS IR-MET-ICP 5 3/2/2015 ICP METALS ANALYSES (EPA METHOD 6010B, EPA METHOD 200.7) METALS IR-MET-HG 5 10/5/2015 MERCURY, COLD-VAPOR ATOMIC ABSORPTION SPECTROMETRY (EPA METHODs 245.1/7470A/7471) MICRO IR-MICRO-HPC-POUR 4 9/12/2014 HETEROTROPHIC PLATE COUNT (HPC) POUR PLATE BY SM 9215B MICRO IR-MICRO-9230D-ENTERO 4 9/19/2014 MICRO IR-MICRO-QC_EQUIP-ENVI 2 10/1/2013 MICRO IR-MICRO-9223B 5 10/17/2014 MICRO IR-MICRO-9221-WW 2 2/4/2014 MICRO IR-MICRO-AUTOCLAVE 2 3/7/2014 MICRO IR-MICRO-Pure Culture 2 4/25/2014 MICRO IR-MICRO-MRQS 2 7/18/2014 MICRO IR-MICRO-HPC-SIM 5 10/30/2015 MICRO IR-MICRO-9221-DW & SW 5 11/6/2015 FECAL ENTEROCOCCUS GROUP IN UNTREATED WATERS BY MULTIPLE TUBE FERMENTATION SM 9230D MICROBIOLOGICAL QUALITY CONTROL CHECKS FOR LABORATORY EQUIPMENTS AND LABORATORY ENVIRONMENT TOTAL COLIFORM AND E. COLI PRESENCE/ABSENCE OR (Quanti-Tray) MPN BY COLILERT, COLILERT 18, COLISURE OR COLITAG SM 9223B TOTAL COLIFORMS, FECAL COLIFORMS, AND E. COLI IN NON-POTABLE WATERS, BIOSOLIDS, SOIL AND SLUDGE BY MULTIPLE TUBE FERMENTATION (MTF) / MOST PROBABLE NUMBER (MPN) STANDARD METHODS 9221 B, C, E, AND F MICROBIOLOGICAL STERILIZATION EQUIPMENT - AUTOCLAVE AND HOT AIR OVEN MICROBIOLOGICAL - PURE CULTURE PREPARATION AND MAINTENANCE MICROBIOLOGICAL MEDIA, REAGENTS AND QUANTITATION SUPPLIES RECEIVING, PREPARATION AND QUALITY CONTROL CHECK HETEROTROPHIC PLATE COUNT (HPC SIM) BY IDEXX SIM PLATE TOTAL COLIFORMS, FECAL COLIFORMS, AND E. COLI IN DRINKING WATER AND SOURCE OF DW BY MULTIPLE TUBE FERMENTATION (MTF) / MOST PROBABLE NUMBER (MPN) STANDARD METHODS 9221 B, C, E, AND F MICRO IR-MICRO-WASH 3 9/30/2015 MICROBIOLOGY - GLASSWARE WASHING MICRO IR-MICRO-RGW 3 11/2/2015 MICROBIOLOGY - REAGENT GRADE WATER PROJECT MANAGEMENT--Initial Quote/Project Setup and PM IR-PM-SOP 0 2/27/2013 Deliverable Generation QA IR-QA-MDL 3 11/3/2014 DETERMINATION OF METHOD DETECTION LIMITS QA IR-QA-LOTTEST 4 11/14/2014 CONTAINER AND REAGENT VERIFICATION BY LOT TESTING QA IR-QA-CNTRLLIM 4 11/21/2014 CONTROL CHARTS AND STATISTICAL PROCESS CONTROL QA IR-QA-DOC 4 12/19/2014 DOCUMENT CONTROL QA IR-QA-LOGBOOK 4 12/19/2014 QA IR-QA-STDCNTRL 3 12/19/2014 QA IR-QA-SUBSAMP 3 12/20/2013 SUBSAMPLING QA IR-QA-SIGFIG 4 1/5/2015 SIGNIFICANT FIGURES QA IR-QA-THERMA 4 1/5/2015 LOGBOOKS, DOCUMENTATION, AND LABORATORY COMMUNICATION REAGENT AND STANDARD CONTROL AND DOCUMENTATION THERMOMETER CALIBRATION, TEMPERATURE MONITORING, AND DOCUMENTATION QA IR-IT-COMPUSEC 4 8/1/2014 COMPUTER SECURITY AND SOFTWARE MAINTENANCE Revised /6
4 QA IR-QA-WATER 4 10/19/2015 LABORATORY WATER QUALITY BALANCE CALIBRATION VERIFICATION AND QA IR-QA-BAL 3 9/12/2014 DOCUMENTATION QA IR-QA-PIPET 4 9/30/2015 PIPET, SYRINGE, AND DISPENSER CALIBRATION QA IR-QA-REFRBLANK 3 11/3/2014 REFRIGERATOR STORAGE BLANKS QA IR-QA-TRAIN 3 5/13/2015 TRAINING AND DOCUMENTATION Sample Control IR-SC-BOTTLESHIP_r0 0 11/21/2014 PREPARING BOTTLES AND COOLERS for SHIPMENT Sample Control IR-SC-FIELD 3 1/30/2015 FIELD SAMPLING Sample Control IR-SC-LOGIN 4 9/19/2014 SAMPLE LOGIN WETCHEM IR-WET /3/2014 WETCHEM IR-WET /6/2014 WETCHEM IR-WET-CRIC 4 10/6/2014 WETCHEM IR-WET-ICMS 5 10/6/2014 WETCHEM IR-WET /7/2014 WETCHEM IR-WET-5310C 5 11/7/2014 EPA METHOD and EPA SW9056 (THE DETERMINATION OF INORGANIC ANIONS BY ION CHROMATOGRAPHY) EPA METHOD 7196A/STANDARD METHODS 3500-CR D (HEXAVALENT CHROMIUM, COLORIMETRIC + ALKALINE DIGEST (EPA 3060A) Determination of Hexavalent Chromium by Ion Chromatography--EPA Methods 7199 and Determination of Perchlorate by Ion Chromatography/Mass Spectrometry, EPA & 6860 Determination of Perchlorate by Ion Chromatography--EPA TOTAL AND DISSOLVED ORGANIC CARBON (STANDARD METHOD 5310C) WETCHEM IR-WET-5710B 4 11/7/2014 TRIHALOMETHANE FORMATION POTENTIAL SM5710B WETCHEM IR-WET /21/2014 Hexavalent Chromium by EPA SM 5540C (ANION SURFACTANTS AS METHYLENE BLUE WETCHEM IR-WET-MBAS 6 3/2/2015 ACTIVE SUBSTANCES) WETCHEM IR-WET-MERCAP 3 3/26/2014 MERCAPTANS, TOTALS (LACSD 258) WETCHEM IR-WET-HARD 6 4/1/2015 HARDNESS BY TITRATION SM2340C PAINT FILTER LIQUIDS TEST, EPA 9095A AND EPA WETCHEM IR-WET-PAINT 3 4/21/ B WETCHEM IR-WET-THIO 3 4/25/2014 THIOSULFATE BY TITRATION (LACSD 253B) WETCHEM IR-WET-COD 3 4/30/2014 EPA METHOD 410.4/SM 5520D (CHEMICAL OXYGEN DEMAND) WETCHEM IR-WET /1/2015 EPA METHOD (THE DETERMINATION OF INORGANIC ANIONS BY ION CHROMATOGRAPHY) WETCHEM IR-WET-ACID 3 5/2/2014 ACIDITY, TITRIMETRIC (SM 2310B) SPECIFIC ELECTRICAL CONDUCTANCE (EPA METHOD WETCHEM IR-WET-COND 6 6/3/ / STANDARD METHOD 2510B ) WETCHEM IR-WET-ALK 7 6/12/2015 ALKALINITY BY SM2320B WETCHEM IR-WET-420_4 0 6/30/2014 WETCHEM IR-WET-NH3ISE 4 6/30/2014 WETCHEM IR-WET-KELADA /2/2015 WETCHEM IR-WET /3/2015 WETCHEM IR-WET-TS 7 8/13/2015 WETCHEM IR-WET-CO2 7 11/6/2015 IN-LINE DISTILLATION AND DETERMINATION OF VOLATILE PHENOLICS BY FLOW INJECTION ANALYSIS COLORIMETRY - EPA Method AMMONIA POTENTIOMETRIC, ION SELECTIVE ELECTRODE (SM4500-NH3 D) DETERMINATION OF TOTAL CYANIDE BY IN-LINE DIGESTION, DISTILLATION, AND FLOW INJECTION ANALYSIS KELADA-01 AMMONIA DETERMINATION OF AMMONIA BY FLOW INJECTION ANALYSIS UTILIZING IN-LINE DISTILLATION (Lachat) EPA AND SM4500 NH3-G SM2540B AND SM2540G (TOTAL SOLIDS / PERCENT SOLIDS / PERCENT MOISTURE, GRAVIMETRIC, DRIED AT C) STANDARD METHOD 4500-CO2 (TITRIMETRIC METHOD FOR FREE CARBON DIOXIDE) WETCHEM IR-WET-OXY 6 11/6/2015 WETCHEM IR-WET-TDS 7 11/6/2015 STANDARD METHOD 4500-O-G (DISSOLVED OXYGEN) TOTAL DISSOLVED SOLIDS, FILTERABLE RESIDUE (SM2540C) Revised /6
5 WETCHEM IR-WET-TRC 7 11/6/2015 SM 4500-Cl G ( CHLORINE AND CHLORAMINES) WETCHEM IR-WET-FLUOR_ISE 5 9/23/2015 WETCHEM IR-WET-2540G 3 10/3/2014 WETCHEM IR-WET-PERM 3 10/3/2014 WETCHEM IR-WET-TOTALCN 5 10/5/2015 WETCHEM IR-WET-CN_WAD 3 10/6/2014 WETCHEM IR-WET-TSS 6 10/19/2015 WETCHEM IR-WET-SULFIDE_SPEC 3 10/31/2014 WETCHEM IR-WET-3060A 2 11/7/2014 WETCHEM IR-WET-BOD 3 12/2/2014 EPA METHOD 9214/SM 4500F (FLUORIDE BY POTENTIOMETRIC, ION SELECTIVE ELECTRODE) STANDARD METHOD 2540G (TOTAL FIXED AND VOLATILE SOLIDS IN SOLIDS AND SEMISOLIDS) STANDARD METHOD 4500-KMnO4 (POTASSIUM PERMANGANATE) EPA 9010B, 9014 & SM 4500-CN~ -B,C,E (CYANIDES, TOTAL) STANDARD METHODS 4500-CN, I - WEAK ACID DISSOCIABLE CYANIDE SM 2540D TOTAL SUSPENDED SOLIDS ( NON- FILTERABLE RESIDUE) SULFIDE, COLORIMETRIC, METHYLENE BLUE (STANDARD METHOD 4500 S2-B, C, D & H) ALKALINE DIGESTION PROCEDURE FOR HEXAVALENT CHROMIUM EPA 3060A (FOR METHOD EPA 7196 & EPA 7199) BIOCHEMICAL OXYGEN DEMAND / CARBONACEOUS BIOLOGICAL OXYGEN DEMAND (SM 5210B) WETCHEM IR-WET-351_2 2 3/2/2015 TOTAL KJELDAHL NITROGEN ( EPA METHOD 351.2) WETCHEM IR-WET-NH3_KONE 2 8/3/2015 AMMONIA DETERMINATION BY AUTOMATED PHENATE METHOD (Konelab) EPA AND SM4500 NH3-G WETCHEM IR-WET-TVS 4 8/3/2015 EPA METHOD 160.4/SM2540E (FIXED AND VOLATILES RESIDUE IN WATERS) WETCHEM IR-WET-TOC 4 8/13/2015 SM 5310B / EPA METHOD SW 9060A (TOTAL ORGANIC CARBON) WETCHEM IR-WET-SPECGRAV 3 9/25/2015 SPECIFIC GRAVITY BY MASS RATIO (SM2710F) EPA METHOD 9030B/9031/ ACID SOLUBLE WETCHEM IR-WET-SULFIDE_TITR 3 9/25/2015 SULFIDES WETCHEM IR-WET-PHOSP 3 10/5/2015 EPA METHOD (PHOSPHORUS, ALL FORMS) Revised /6
6 Revised /6
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