SCOPE OF ACCREDITATION TO ISO/IEC 17025:2017
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1 SCOPE OF ACCREDITATION TO ISO/IEC 17025:2017 R. J. REYNOLDS TOBACCO COMPANY 1 Product Services Analytical Testing Laboratories 950 Reynolds Blvd. Winston Salem, NC Jannell Rowe Phone: CHEMICAL Valid To: June 30, 2020 Certificate Number: In recognition of the successful completion of the A2LA evaluation process, accreditation is granted to this laboratory to perform the following types of tests on cigarettes, cigarette smoke, and related processes and materials: Test(s) Test Procedure(s) Test Method(s) I. Cigarette Smoke Parameters Carbon Monoxide 45 FR 46483; ISO 8454 Nicotine 32 FR 11178, 45 FR 46483; ISO RJRT-WI RJRT-WI TNCO in Mainstream Smoke by Cambridge Filter Pad Method TNCO in Mainstream Smoke by ISO Methods 4387 and FR 11178, 45 FR 46483; ISO 4387; TIOJ Method RJRT-WI , RJRT-WI Water 32 CFR 11178, 45 CFR 46483; ISO RJRT-WI II. Ignition Properties Eclipse (Non Burn-Down) Testing Procedure for NYS Free Air Extinction RJRT-WI Ignition Strength of Cigarettes ASTM E Appendix A to Part 429 of Title 19 NYCRR Regulation RJRT-WI (A2LA Cert. No ) Revised 10/09/2018 Page 1 of 7
2 III. Spectroscopy Chemiluminescence Nitrogen Oxides in Smoke RJRT-WI Nitrite in Tobacco Products RJRT-WI Continuous Flow Analyzers Alkaloids, Total and Reducing Sugars in Tobacco RJRT-WI Nitrate in Tobacco RJRT-WI Ammonia in Tobacco RJRT-WI Hydrogen Cyanide in Smoke RJRT-WI ICP/Mass Spectroscopy Elemental Content RJRT-WI Smoke and E-Cigarette Aerosol Metals Analysis RJRT-WI Inductively Coupled Plasma Optical Emission Spectroscopy Analysis of Tobacco and Paper after Digestion RJRT-WI Non-Dispersive Infrared Carbon Monoxide in Smoke RJRT-WI IV. Chromatography Gas Chromatography Nicotine in Tobacco Products- CDC Nicotine RJRT-WI Nicotine and Water in Smoke RJRT-WI Nicotine, Water, Menthol, Glycerin and Propylene Glycol in Smoke RJRT-WI Menthol in Smoke RJRT-WI Menthol in Tobacco, Cigarettes and Cigarette Components RJRT-WI Plasticizer(s) in Filter/Filter Rods RJRT-WI Propylene Glycol and Glycerin in Tobacco RJRT-WI Specific Alkaloids in Tobacco RJRT-WI (A2LA Cert. No ) Revised 10/09/2018 Page 2 of 7
3 Gas Chromatography (Cont.) Water, Acetone, and Nicotine in Cigarette for Dermal Studies RJRT-WI Water in Tobacco RJRT-WI Combustion/Gas Chromatography Carbon, Hydrogen and Nitrogen Elemental Analysis RJRT-WI Ion Chromatography Ammonia in Smoke RJRT-WI Liquid Chromatography B[a]P in Tobacco Materials and Cigarette Smoke Condensate RJRT-WI Carbonyls in Cigarette Smoke and Aerosol RJRT-WI Carbonyls in Tobacco RJRT-WI Citric Acid in Cigarette Paper RJRT-WI Hydroxybenzenes in Aerosol from Electronic Cigarettes RJRT-WI Licorice in Tobacco and Glycyrrhizic Acid in Licorice RJRT-WI Organic Acids in Tobacco and Tobacco Products RJRT-WI Phenols in Smoke and Smoke Condensate RJRT-WI Sucralose in Tobacco and Tobacco Products RJRT-WI Sucrose, Glucose and Fructose in Tobacco and Raw Materials RJRT-WI Analysis of BaP in Smoke and Tobacco Materials RJRT-WI Liquid Chromatography/Mass Spectrometry/Mass Spectrometry Aflatoxin B1 in Tobacco Materials RJRT-WI Analysis of Trace TSNAs in Vapor RJRT-WI Carbonyls in Electronic Cigarette Aerosol and E-Liquid RJRT-WI Extraction of Acrylamide from Tobacco and Alternative Tobacco Products RJRT-WI Extraction of TSNA from Smoke and Aerosol RJRT-WI Extraction of TSNA from Tobacco Materials RJRT-WI (A2LA Cert. No ) Revised 10/09/2018 Page 3 of 7
4 Liquid Chromatography/Mass Spectrometry/Mass Spectrometry (Cont.) Free Amino Acids in Tobacco Materials by UPLC/MS/MS RJRT-WI Limit Test for Benzo(a)Pyrene in E-Liquid and E-Cigarette Aerosol Samples RJRT-WI Quantitative Determination of Acrylamide by UPLC RJRT-WI Quantitative Determination of Tobacco Specific Nitrosamines RJRT-WI Trace Level Ammonia Analysis of E-Liquid and Aerosol Samples RJRT-WI Gas Chromatography/Mass Spectrometry 1,3-Butadiene, Ethylene Oxide, Vinyl Chloride and Propylene Oxide in MVP Cigarette Smoke RJRT-WI Anabasine in E-cigarette Liquid and Aerosol by GC/MS/MS RJRT-WI Diacetyl and Acetylpropionyl in E-Liquids and Aerosols RJRT-WI Evaluation of Primary Aromatic Amines in E-Cigarette Aerosol and E-Liquid by GC/MS Extraction of PAH from MSPP of Burn-Down Products, HNB Products, Aerosols from E-Cigs and from Tobacco Material Extraction of Volatile Nitrosamines from Smokeless Tobacco Products RJRT-WI RJRT-WI RJRT-WI Level of Flavors Applied to Snus Products RJRT-WI Level of Mint Flavor Applied to Camel Snus Product RJRT-WI Limit Test for Selected Volatile Organics in E-Cigarettes Liquid and Aerosol RJRT-WI Menthol, Methyl Salicylate and Ethyl Salicylate in Snuff Products RJRT-WI Percent Purity of Methyl Salicylate and Ethyl Salicylate (Raw Flavors) Polycyclic Aromatic Hydrocarbons in MSPP from Burn-Down Products RJRT-WI RJRT-WI Primary Aromatic Amines RJRT-WI Pyridine, Quinoline, and Acrylamide RJRT-WI Qualitative Profiling of Raw Flavors RJRT-WI (A2LA Cert. No ) Revised 10/09/2018 Page 4 of 7
5 Gas Chromatography/Mass Spectrometry (Cont.) Quantitation of SVO in MSPP and Aerosol by Impingement and GCMS Trace Level Ethylene Glycol and Diethylene Glycol Analysis of E- Liquid and E-Liquid Vapor Samples RJRT-WI RJRT-WI Volatile Nitrosamines RJRT-WI Quantitation of SVO in ETHP, E-Cig Liquid and Aerosol by GC/ RJRT-WI V. Gravimetric and Electrode Analysis Gravimetric Charcoal in Cellulose Acetate Filters RJRT-WI Hot Water Solubles in Tobacco RJRT-WI Moisture in Tobacco 74 FR 712 RJRT-WI Moisture in Tobacco by Microwave RJRT-WI Percent Solids by CEM SMART System RJRT-WI Resin in Cellulose Acetate Filters RJRT-WI Sand in Tobacco RJRT-WI Tobacco Ash RJRT-WI Total Solids in Tobacco Extract RJRT-WI Electrode Analysis ph of Aerosol RJRT-WI Puff by Puff ph in Tobacco Smoke utilizing the Mass/Texas Smoke Regime RJRT-WI Titration Tobacco ph 74 FR 712 RJRT-WI Chloride in Tobacco RJRT-WI Potassium Carbonate and DAP Content using Sulfuric Acid and an Automatic Titrator RJRT-WI Water Analysis by Karl Fisher RJRT-WI (A2LA Cert. No ) Revised 10/09/2018 Page 5 of 7
6 Sensory Evaluation Raw Materials and Products Acceptability by Sensory Evaluation RJRT-WI Density Smoke Condensate and Dosing Solution Density RJRT-WI BIOLOGICAL In recognition of the successful completion of the A2LA evaluation process, accreditation is also granted to this laboratory to perform the following types of tests on cigarettes, cigarette smoke and related processes and materials: Test Test Procedure Test Method Microbial Enumeration RJRT-WI Thermophile and Anaerobe Enumeration RJRT-WI Water Activity RJRT-WI This accreditation covers testing performed at the main laboratory as well as the satellite laboratory listed below. R. J. REYNOLDS TOBACCO COMPANY Ingredient Mixing and Storage Laboratory 7855 King Road Tobaccoville, NC CHEMICAL Test Test Procedure Test Method Density using Gardner Cup RJRT-WI Melting Ranges using a Buchi M RJRT-WI Percent Solids by CEM SMART System RJRT-WI ph by ph Meter RJRT-WI Propylene Glycol and Menthol in Top Dressings using Gas Chromatography RJRT-WI Raw Materials and Products Acceptability by Sensory Evaluation RJRT-WI Specific Gravity and Refractive Index RJRT-WI (A2LA Cert. No ) Revised 10/09/2018 Page 6 of 7
7 Test Test Procedure Test Method Specific Gravity and Refractive Index by Anton/Paar DMA 4500 and Rudolph Research Analytical J RJRT-WI Verification of Raw Material Identity by Infrared Spectrometer RJRT-WI Viscosity RJRT-WI (A2LA Cert. No ) Revised 10/09/2018 Page 7 of 7
8 Accredited Laboratory A2LA has accredited R. J. REYNOLDS TOBACCO COMPANY Winston Salem, NC for technical competence in the field of Chemical Testing This laboratory is accredited in accordance with the recognized International Standard ISO/IEC 17025:2017 General requirements for the competence of testing and calibration laboratories. This accreditation demonstrates technical competence for a defined scope and the operation of a laboratory quality management system (refer to joint ISO-ILAC-IAF Communiqué dated April 2017). Presented this 6 th day of June President and CEO For the Accreditation Council Certificate Number Valid to June 30, 2020 For the tests to which this accreditation applies, please refer to the laboratory s Chemical Scope of Accreditation.
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