Thickeners for Aircraft Anti-icing Fluids
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1 Thickeners for Aircraft Anti-icing Fluids Relationship to Performance Properties
2 AAF Requirements Provide a thick fluid film on stationary aircraft Absorb precipitation (snow, freezing rain) Prevent absorbed precipitation from re-freezing Absorb residual Type I (deicing) fluid Flow off the wings at takeoff Completely eliminate from the wing s leading edge Substantially complete elimination from trailing edge No re-freeze in aerodynamic quiet areas at altitude
3 Viscosity (Pa s) at -20 C ~1000x Viscosity Drop Viscosity Profiles of Type IV AAFs -20 C Shear Stress (Pa)
4 Picture of Conventional Thickening Thickening by entanglement of polymer strands
5 Conventional Thickening: Shear Stress Applied Polymer strands untangle and align with flow
6 - OOC Thickener Structure COO - - OOC - OOC - OOC COO - - OOC Typically long polymers having carboxylate salts ( ) salt on a string Some of the salts dissociate Resulting net negative charges on the polymer repel each other This repulsion uncoils the polymer The polymer thickens the mixture by entanglement of the polymer strands COO -
7 Effect of Salts COO - CH 3 COO - CH 3 COO - CH 3 COO - - OOC CH 3 COO - COO - - OOC - OOC - OOC - OOC COO - CH 3 COO - CH CH 3 COO - 3 COO -
8 Polymer Chain Geometry as a Function of Salt Content No Salt Low Salt High Salt Thickener wads up as salt increases
9 Polymer Chain Geometry as a Function of Water Content water = ion dissociation = chain unfolding More Water Less Water Least Water Thickener wads up as water decreases
10 1 st Performance Obstacle: Dilution & Salt Sensitivity Thickener efficiency is greatly affected by how much the polymer backbone is coiled up A tightly coiled polymer does not entangle well with other polymer molecules Salt content and water content can greatly affect the polymer coiling. X
11 Thickener Architecture Unbranched Comb type Branched or Network
12 Thickener Composition The polymer strands are made up of many monomer units. Monomers are like beads on a string Monomers can be: Water soluble or insoluble Ionic or non-ionic Stiff or flexible
13 Thickener Crosslinking Unbranched Comb type Branched or Network
14 Polymer Mixtures
15 Targets & Controls Performance Controls Polymer Architecture Branching Cross-linking Monomer makeup Water solubiltiy Stiffness Ionic/non-ionic Polymer Blends Performance Targets Shear-thinning viscosity Insensitivity to salts Insensitivity to dilution
16 2 nd Performance Obstacle: Shear Degradation Problem:Polymer strands may break with applied shear stress
17 Schematic of an Associative Thickener Water-soluble Polymer Backbone Water-soluble side chains Water-insoluble caps (hydrophobes)
18 Associative Thickener Network at Rest Hydrophobic Cluster
19 Associative Thickeners & Surfactants Non-ionic Surfactant: Water-insoluble head Water-soluble tail 3-D cluster of surfactant molecules = micelle Hydrophobic Cluster
20 Associative Thickeners & Surfactants Hydrophobic Cluster = Surfactant micelle with embedded polymer hydrophobes
21 Associative Thickener Shear Applied Hydrophobes separate and thickener molecules align with flow
22 Conventional vs. Associative Thickeners Conventional Higher m.w. Branched or cross-linked Thicken by polymer chain entanglement Lose viscosity by untangling chains Associative Lower m.w. Comb-type Thicken by association of hydrophobe clusters + some entanglement Lose viscosity by pulling hydrophobes out of clusters (micelles)
23 Conventional vs. Associative Thickeners Conventional PROS Simpler formulation Lower aquatic toxicity CONS More degradation by mechanical shear More dryout residue Associative PROS Less degradation by mechanical shear Less dryout residue CONS More complex formulation Higher aquatic tox
24 End of Thickener Presentation Questions?
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