Annex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005

Transcription

1 Deutsche Akkreditierungsstelle GmbH Annex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005 Period of validity: to Holder of certificate: Eurofins WEJ Contaminants GmbH Neuländer Kamp 1, Hamburg Tests in the fields: physico-chemical and chemical analysis of food, feed, tobacco and tobacco products and raw materials for cosmetic products; selected immunochemical analysis of food and grain dust; sampling of food and feed Abbreviations used: see last page Within the given testing field marked with * the testing laboratory is permitted, without being required to inform and obtain prior approval from DAkkS, the following the modification, development and refinement of testing methods. The listed testing methods are exemplary. The testing laboratory maintains a current list of all testing methods within the flexible scope of accreditation. This document is a translation. The definitive version is the original German annex to the accreditation certificate. 1/11

2 1 Analysis of food, feed, tobacco and tobacco products as well as raw materials for cosmetic products 1.1 sample preparation ASU L / ASU L / CON-PV CON-PV Foodstuffs - Determination of trace elements in food - Part 1: pressure digestion (withdrawn document) (Modification: Expansion of application to feed, addition of direct digestion) Foodstuffs - Sample preparation procedure for the provision of the official and mediation sample for the determination of mycotoxin content in food - Part 1: - Wet homogenisation process Sample preparation process for dry homogenization Non-quantitative fat extraction 1.2 Determination of residues and contaminants in food and feed by gas chromatography with flame ionisation detector* CON-PV CON-PV CON-PV Determination of mineral oil saturated hydrocarbons in vegetable oil by LC-GC/FID coupling MOSH-MOAH separation of mineral oil hydrocarbons in food by LC-GC/FID coupling (additional application to feed) Determination of water-soluble solvents in foods and food additives by headspace GC/FID (additional application to feed) Period of validity: to Translation - 2/11

3 1.3 Determination of residues and contaminants of food and feed by gas chromatography with MS-detector * DGF C-VI-18[10] 2011 US FDA/CFSAN CON-PV CON-PV CON-PV CON-PV CON-PV Fatty acid-bound 3-chloropropane-1,2-diol (3-MCPD ester) and 2,3-epoxypropan-1-ol (glycidol) Determination in fats and oils by GC-MS (difference method) (Modification: sample weight; solvent and IS-volume; expansion to 2-MCPD-Ester; MS/MS-detection) Determination of furan in foods (Modification: sample weight; solvent and IS-volume) Determination of furan in foodstuffs by gas chromatographic headspace analysis (headspace GC/MS) Determination of polycyclic aromatic hydrocarbons (PAHs) by SPE GC/MS (additional application to feed) Determination of 3-MCPD and DCP in foodstuffs by GC-MS Determination of 3-MCPD in glycerol by GC-MS Determination of residues of volatile organic solvents in foods and food additives by headspace GC/MS 1.4 Determination of polycyclic aromatic hydrocarbons (PAHs) in raw materials for cosmetic products by gas chromatography with MS-detector CON-PV Determination of polycyclic aromatic hydrocarbons (PAHs) by SPE GC/MS Period of validity: to Translation - 3/11

4 1.5 Determination of mycotoxins in food and feed by high performance liquid chromatography with Fluorescence-detector * DIN EN DIN EN DIN EN DIN EN DIN EN AOAC 84, No CON-PV Foodstuffs - Determination of aflatoxin B 1 and the sum of aflatoxin B 1, B 2, G 1 and G 2 in hazelnuts, peanuts, pistachios, figs and paprika powder - High performance liquid chromatographic method with post-column derivatisation and immunoaffinity column cleanup (Modification: Expansion of application to foodstuffs in general (in particular to nuts and nut-like products, dried fruits, cereal products, spices, tea, coffee and cocoa) and feed, adaptation of the extracting solvent and measurement conditions) Foodstuffs - Determination of ochratoxin A in barley and roasted coffee - HPLC method with immunoaffinity column clean-up (Modification: Expansion of application to cereals, coffee, cocoa, pepper, dried fruits, samples containing liquorice, feed, modification of extraction solvent, additional post-column derivatisation) Foodstuffs - Determination of ochratoxin A in wine and beer - HPLC method with immunoaffinity column clean-up (Modification: Expansion of application to beverages, additional post-column derivatisation) Foodstuffs - Determination of ochratoxin A in currants, raisins, sultanas, mixed dried fruit and dried figs - HPLC method with immunoaffinity column cleanup and fluorescence detection Foodstuffs - Determination of aflatoxin B 1 in cereal based foods for infants and young children - HPLC method with immunoaffinity column cleanup and fluorescence detection (Modification: additional determination of aflatoxin B2, G1 and G2) Determination of ochratoxin A in baby food by HPLC-FD Determination of aflatoxin M1 in milk and milk products using LC-FD Period of validity: to Translation - 4/11

5 1.6 Determination of mycotoxins in tobacco and tobacco products by high performance liquid chromatography with Fluorescence-detector * DIN EN DIN EN Foodstuffs - Determination of aflatoxin B 1 and the sum of aflatoxin B 1, B 2, G 1 and G 2 in hazelnuts, peanuts, pistachios, figs and paprika powder - High performance liquid chromatographic method with post-column derivatisation and immunoaffinity column cleanup (Modification: Expansion of application to tobacco and tobacco products) Foodstuffs - Determination of ochratoxin A in barley and roasted coffee - HPLC method with immunoaffinity column clean-up (Modification: Expansion of application to tobacco and tobacco products, change of extraction solvent, additional post column derivatisation) 1.7 Determination of aflatoxins in raw materials for cosmetic products by high performance liquid chromatography with Fluorescence-detector DIN EN Foodstuffs - Determination of aflatoxin B 1 and the sum of aflatoxin B 1, B 2, G 1 and G 2 in hazelnuts, peanuts, pistachios, figs and paprika powder - High performance liquid chromatographic method with post-column derivatisation and immunoaffinity column cleanup (Modification: Expansion of application to raw materials for cosmetic products, adaptation of extraction solvent and measurement conditions) 1.8 Determination of additives, residues and contaminants in food and feed by high performance liquid chromatography with mass selective detectors (, LC- HRMS) * ASU L (V) LC/GC Europe 17/11a, Foodstuffs - Determination of residues of macrolides and lincosamides in kidney and milk by (Modification: Expansion of application to fish, egg, egg powder, honey, water, milk powder and feed; extraction at ph 8 with acetonitrile) Multi-toxin method: Determination of Fusarium toxins in vegetal foods by Period of validity: to Translation - 5/11

6 CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV Determination of tetracyclines in meat, fish, crustaceans and eggs by Determination of dyes with a fungicide effect in fish, feeding stuffs and oleoresin by Determination of nitrofuran metabolites in animal foodstuffs by Determination of coccidiostats in eggs, egg products, feeding stuffs and poultry by Determination of sulphonamides in meat after direct extraction by Determination of patulin in apple juice and other fruit preparations by Determination of quinolones and fluoroquinolones respectively in meat by Determination of nicotine and cotinine in eggs, egg products, poultry, poultry products, mushrooms and herbs by Determination of residues of macrolides and lincosamides in muscle, kidney, fish, egg, egg powder, honey, milk, water, milk powder and feed by Determination of ergot alkaloid content in foodstuffs by HP Determination of benzimidazoles in meat, liver and milk by Determination of fumonisins in foodstuffs and feeding stuffs by Determination of gestagens in meat and protein-rich foodstuffs by Multi-toxin method: Determination of mycotoxins by Period of validity: to Translation - 6/11

7 CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV CON-PV Determination of thyrostatics in meat by LC-MS / MS Determination of amphenicols in meat, shrimp, egg and milk powder by Determination of NSAID in meat, offal and milk Determination of avermectins in meat and protein rich matrices as well as feed by Determination of estradiol in feeding stuffs by Multi method for analysis of veterinary drugs in meat and protein-rich foodstuffs by Determination of estrogens in meat and protein-rich foodstuffs, water and urine by Determination of androgens in meat and protein-rich foodstuffs, water and urine by Determination of amino glycosides in food Determination of pyrrolizidine alkaloids and their N-oxides in food by Determination of β-lactams in protein-rich matrices and feed by Determination of beta-2-agonists in protein-rich and fatty food by Multi method for high resolution analysis of veterinary drugs in meat, fish and eggs Determination of plasticizers in oil and fat by LC-ESI-MS/MS Determination of bisphenols in food by LC-ESI-MS/MS Period of validity: to Translation - 7/11

8 CON-PV CON-PV CON-PV CON-PV Determination of sedatives in meat and protein-rich matrices by Determination of banned and restricted colorants in foodstuffs using LC-ESI-MS/MS Quantitative determination of BADGE, BFDGE and NOGE as well as their derivatives in foodstuffs using LC-ESI-MS/MS Quantitative determination of acrylamide in foodstuffs using LC-ESI-MS/MS 1.9 Determination of elements in food and feed by Atomic absorption spectrometry (GF-AAS, K-AAS, HG-AAS) * ASU L / ASU L / ASU L ASU L Foodstuffs - Determination of trace elements - Determination of lead, cadmium, chromium and molybdenum by graphite furnace atomic absorption spectrometry (GF-AAS) after pressure digestion (Modification: Expansion of analytes to Co, Ni, Ag, Te, Tl, Sn, V, Sb, Be, As, Se; Expansion of application to feed) Foodstuffs - Determination of trace elements in food - Part 4: Determination of mercury by atomic absorption spectrometry (AAS) with cold vapour technique after pressure digestion (Modification: Expansion of application to feed) Foodstuffs - Determination of inorganic arsenic in algae - atomic absorption spectrometry - hydride generation (HG-ASS) after acidic extraction (Modification: Expansion of application to fish, fish oil ans fish meal) Foodstuffs - Determination of inorganic arsenic in rice - atomic absorption spectrometry - hydride generation (HG-ASS) after acidic extraction Period of validity: to Translation - 8/11

9 1.10 Determination of elements in food and feed by inductively coupled plasma with atomic emission spectrometry (ICP-OES) * DIN EN ISO (E 22) DIN EN Water quality - Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES) (Modification: Expansion of application to food and feed after pressure digestion) Animal feeding stuffs - Determination of calcium, sodium, phosphorus, magnesium, potassium, iron, zinc, copper, manganese, cobalt, molybdenum, arsenic, lead and cadmium by ICP-AES 1.11 Determination of elements in food and feed by inductively coupled plasma with mass spectrometry (ICP-MS) * DIN EN DIN EN DIN EN Foodstuffs - Determination of trace elements - Determination of iodine by ICP-MS (inductively coupled plasma mass spectrometry) (Modification: Expansion of analytes to bromine; expansion of application to feed) Foodstuffs - Determination of trace elements - Determination of arsenic, cadmium, mercury and lead in foodstuffs by inductively coupled plasma mass spectrometry (ICP-MS) after pressure digestion (Modification: including high-resolution ICP-MS, expansion of analytes to various elements of DIN EN ISO , expansion of application to feed) Foodstuffs - Determination of elements and their chemical species - Determination of inorganic arsenic in foodstuffs of marine and plant origin by anion-exchange HPLC-ICP-MS Period of validity: to Translation - 9/11

10 1.12 Determination of elements in tobacco and tobacco products by inductively coupled plasma with mass spectrometry (ICP-MS) DIN EN Foodstuffs - Determination of trace elements - Determination of arsenic, cadmium, mercury and lead in foodstuffs by inductively coupled plasma mass spectrometry (ICP-MS) after pressure digestion (Modification: Expansion of application to tobacco and tobacco products, expansion of analytes to various elements of DIN EN ISO ) 1.13 Photometric determinations in food and feed CON-PV Photometric determination of iodide via the Sandell-Kolthoff reaction after combusting according to Grote-Krekeler 1.14 Determination of radioactive nuclides in food, feed and raw materials for cosmetic products CON-PV Determination of radioactive nuclides by gamma spectrometry 2 Determination of mycotoxins by immunoassay (dip sticks) in food and grain dust Eurofins rapidust Mycotoxins PJCRF rapidust Indirect determination of mycotoxins in cereals via analysis of dust samples by lateral flow immunoassay dip 3 Sampling of food and feed samples CON-PV CON-PV Sampling of Cereals and cereal (Based on regulations VO (EG) no. 401/2006, VO (EG) no. 333/2007, guideline 2002/63/EG, VO (EG) 1883/2006, DIN EN ISO 24333, Codex Alimentarius CAC/GL , ICC 101/1, ICC 120, ICC 130, ICC 138) Sampling of food and food samples (except cereals and cereal products) Period of validity: to Translation - 10/11

11 Eurofins rapidust Mycotoxins PJCRF rapidust - Sampling of cereal lots via dust retrieval Abbreviations used: AOAC Official Methods of Analysis of AOAC International ASU Official Collection of Testing Methods according to 64 LFGB CON-PV XXXXX Methods of Eurofins WEJ Contaminants GmbH DIN German Institute for Standardization e. V. EN European Standard FDA Food and Drug Administration IEC International Electrotechnical Commission ISO International Organization for Standardization LFGB German Food and Feed Code pren European Standard Draft Period of validity: to Translation - 11/11