Needle Gauge. Needle OD (mm) Needle ID (mm)

Transcription

1 s LC Manual s Beckman/Altex, Rheodyne, SSI Instruments and Valco Valves s and Borosilicate Glass Barrel Outer Diameter () Scale 5 µl and 10 µl = 6.5 mm, 25 µl to 500 µl = 8 mm, 1 ml = 8.8 mm, 2.5 ml = 10.8 mm 60 mm (5 µl and 10 µl are 54.1 mm) Fixed ped Code 6 Pack 5 µl " 0.17 LC 5F-LC µl " 0.17 LC 10FX-LC SuperfleX 10 µl " 0.17 LC 10F-LC µl " 0.17 LC 10F-LC-GT µl " 0.37 LC 25F-LC µl " 0.37 LC 50F-LC µl " 0.37 LC 100F-LC µl " 0.37 LC 250F-LC µl " 0.37 LC 500F-LC ped Removable with Repeating Adaptor Code 10 µl " 0.17 LC 10R-LC-RAX µl " 0.37 LC 25R-LC-RAX µl " 0.37 LC 50R-LC-RAX µl " 0.37 LC 100R-LC-RAX µl " 0.37 LC 250R-LC-RAX µl " 0.37 LC 500R-LC-RAX The blunt LC needle tip design and 51 mm needle length are used to avoid damage to the LC valve. LC manual s are a good choice for general liquid dispensing. 48 For more syringe tips view our video at sge.com/support/videos

2 s and ped Removable Code 5 µl " 0.17 LC 5R-LC µl " 0.17 LC 10R-LC µl " 0.17 LC 10R-GT-LC µl " 0.17 LC 10RX-LC µl " 0.37 LC 25R-LC µl " 0.37 LC 25R-GT-LC µl " 0.37 LC 50R-LC µl " 0.37 LC 50R-GT-LC µl " 0.37 LC 100R-LC µl " 0.37 LC 100R-GT-LC µl " 0.37 LC 250R-LC µl " 0.37 LC 250R-GT-LC µl " 0.37 LC 500R-LC µl " 0.37 LC 500R-GT-LC ml " 0.37 LC 1MR-LC-GT ml " 0.37 LC 2.5MDR-LC-GT injectors requiring 3/4 long needles, When using the complete loop fill technique, the syringe capacity should be greater than twice the loop volume. The loop capacity sets the injection volume. When using the partial loop technique, the injection volume should be no greater than half the loop capacity. The injection size sets the injection volume. s LC Manual s 49

3 s LC Autosampler s Hitachi Instruments s and Borosilicate Glass Barrel Outer Diameter () Scale 8 mm No scale (60 mm stroke) ped Front Thread Code 500 µl M10 x C-HITACHI PerkinElmer Instruments Borosilicate Glass Barrel Outer Diameter () Scale 50 µl to 500 µl = 8 mm, 1 ml = 9 mm, 2.5 ml = 11 mm 60 mm ped Front Thread Code 50 µl 1/4-28 UNF 50D-CX-GT µl 1/4-28 UNF 100D-CX-GT µl 1/4-28 UNF 250D-CX-GT µl 1/4-28 UNF 500D-CX-GT ml 1/4-28 UNF 1MD-C-GT ml 1/4-28 UNF 2.5MD-C-GT For SGE s HPLC column range see page This selection guide can be viewed as an electronic book at sge.com/selectionguide

4 CTC Analytics Borosilicate Glass Barrel Outer Diameter () Scale 10 µl to 250 µl = 6.5mm (except P/N and P/N = 8 mm) 500 µl = 8 mm, 1 ml = 7.6 mm, 2.5 ml = 9.7 mm, 5 ml = 14 mm 10 µl = 54.1 mm, 25 µl to 5 ml = 60 mm s and ped Fixed mm) Code 10 µl LC 10F-CTC-LC µl LC 10F-CTC-GT-LC µl LC 25F-CTC-GT-LC * 25 µl LC 25F-C/T-LC µl LC 50F-C/T-GT-LC µl LC 100F-CTC-GT-LC µl LC 100F-CTC-GT-LC (0.4) µl LC 250F-CTC-GT-LC (0.4) * 500 µl LC 500F-CTC-GT-LC (0.4) * Please note barrel is 8mm. ped Removable mm) Code 25 µl LC 25R-C/T-GT-LC µl LC 50R-C/T-GT-LC µl LC 100R-C/T-GT-LC µl LC 250R-C/T-GT-LC ml LC 1MR-CTC-GT-LC(0.4) ml LC 2.5MR-CTC-GT-LC(0.4) ml LC 5MR-CTC-GT-LC(0.4) CTC PAL-XT and XCHANGE For more information on XCHANGE on CTC PAL- XT contact CTC Analytics. For alternative needle options, see pages XCHANGE CTC PAL-XT LC Autosampler s ped Removable 10 µl " 0.17 LC µl " 0.17 LC µl " 0.17 LC µl " 0.17 LC µl " LC µl " LC ml " LC ml " LC ml " LC s LC Autosampler s 51

5 s LC Autosampler s Spark Holland Instruments s and Borosilicate Glass Barrel Outer Diameter () Scale 250 µl = 8 mm, 1 ml = 9 mm 60 mm ped Front Thread Code 250 µl 1/4-28 UNF 250D-SPARK-GT ml 1/4-28 UNF 1MD-SPARK-GT Thermo Scientific Instruments Borosilicate Glass Barrel Outer Diameter () Scale 250 µl = 8 mm No scale (60mm stroke) ped AS100/300 and AS1000/3000/3500 Front Thread Code 250 µl 1/4-28 UNF 250C-THERMOSPEC Waters Instruments Borosilicate Glass Barrel Outer Diameter () Scale 8 mm No scale (60 mm stroke) ped Front Thread Code 25 µl 1/4-28 UNF 25D-WISP µl 1/4-28 UNF 250D-WISP WISP Dipper Description Side Hole Cone N-121/1.59(0.5)SH s LC Autosampler s

6 s LC Pump High Capacity s LC Pump High Capacity s High capacity Luer Lock syringes are ideal for loop fill injection techniques when used in conjunction with an LC tipped Luer Lock needle. They are also perfect for flushing sample loops after injection, and priming the LC pump. s and Borosilicate Glass Barrel Outer Diameter () Scale 1 ml = 9 mm, 2.5 ml = 11 mm, 5 ml = 14 mm, 10 ml = 18 mm, 25 ml = 27 mm 60 mm ped Termination Code 1 ml Fixed Luer Lock 1MDF-LL-GT ml Fixed Luer Lock 2.5MDF-LL-GT ml Fixed Luer Lock 5MDF-LL-GT ml Fixed Luer Lock 10MDF-LL-GT ml Fixed Luer Lock 25MDF-LL-GT Description Pack Size For complete loop fill, the syringe capacity should be greater than twice the loop volume. The loop capacity sets the injection volume. For partial loop fill, the injection volume should be no greater than half the loop capacity. The injection size sets the injection volume. s LC Pump High Capacity s 53

7 s General Purpose Manual s µl Nano With the ability to inject down to 50 nl with high precision and accuracy, SGE injection as well as making accurate standards that require small volumes. The sample is only drawn into the needle, not the syringe barrel. When the plunger is depressed, the sample is completely extends to the tip of the needle. Displacing the full sample during injection results in virtually zero dead volume and carry over between Reduced Diameter injections. The plungers and needles are matched sets and must be replaced as a set. Refer to page 65 for a list of replacement plunger and needle kits. Sample NOZZLE TIP SHOWN IN DIAGRAM. s and Borosilicate Glass Barrel Outer Diameter () 6.5 mm and 8 mm Scale 0.5 µl (6.5 mm barrel) = mm, 0.5 µl (8 mm barrel) = 63.7 mm, 1 µl = 54.1 mm, 63.7 mm, 5 µl = 48.7 mm 6.5 mm Outer Diameter () Barrel Code and 0.5 µl Cone 0.5BNR µl Bevel µl Cone 0.5BNR-5/ mm Outer Diameter () Barrel 0.5 µl Cone 0.5BR µl Bevel µl Cone 1BR µl Bevel µl Cone 1BR µl Bevel µl Cone 1BR µl Cone 1BR-7/ µl Cone 5BR µl Bevel µl Cone 5BR µl Bevel µl Cone 5BR µl Nozzle 5BR-7N When replacing the plunger and needle follow the instructions included in the kit the front cover nut must be loosened before removing the plunger. s Fitted with Repeating Adaptor See page 63 for more details about the RAX repeating adaptor. 6.5 mm Outer Diameter () Barrel Code and 0.5 µl Cone 0.5BNR-5-RAX µl Cone 0.5BNR-5/0.47-RAX mm Outer Diameter () Barrel 0.5 µl Cone 0.5BR-7-RAX µl Cone 1BR-5-RAX µl Cone 1BR-7-RAX s General Purpose Manual s 35

8 s General Purpose Manual s 5-10 µl Metal s and Borosilicate Glass Barrel Outer Diameter () Scale 6.5 mm (guided plunger syringes 8 mm) 54.1 mm Standard Protection s Fixed Code 6 Pack Part No. 10 Pack Part No. 25 Pack Part No. 5 µl Bevel 5F µl Bevel 5F µl Cone 5F- 4.2/0.63C µl Bevel 10F µl Bevel 10F µl cone 10F-5C µl Bevel 10F µl Cone 10F- 4.2/0.63C Removable µl Bevel 5R µl Bevel 10R µl Bevel 10R SuperFlex s protection helps prevent plunger bending during injection. Fixed Code 6 Pack Part No 5 µl Bevel 5FX µl Cone 5FX-5C µl Bevel 10FX µl Bevel 10FX µl Cone 10FX-5C µl Cone 10FX-5/0.63C Removable 5 µl Bevel 5RX µl Bevel 10RX The virtually indestructible Titanium Nickel alloy plunger of the SuperFlex s is ideal for student use. 36 This selection guide can be viewed as an electronic book at sge.com/selectionguide

9 s and Guided s Guided plunger syringes are the most rugged syringe available, making them perfect for industrial environments. Fixed Code 6 Pack Part No 5 µl Bevel 5F-GP µl Bevel 10F-GP Removable 5 µl Bevel 5R-GP µl Bevel 5R-GP µl Bevel 5R-GPS * 10 µl Bevel 10R-GP * Short half scale syringe (scale length 27 mm). s Fitted with Repeating Adaptor See page 63 for more details about the RAX repeating adaptor. Fixed Code 6 Pack Part No 10 µl Bevel 10F-RAX Removable 5 µl Bevel 5R-RAX µl Bevel 10R-RAX Removable - Guided 5 µl Bevel 5R-GP-RAX µl Bevel 10R-GP-RAX µl Bevel 10R-GP-7-RAX The RAX repeating adaptor improves precision and reproducibility when repeatedly injecting the same volume manually. s General Purpose Manual s 37

10 s General Purpose Manual s µl Metal s and Borosilicate Glass Barrel Outer Diameter () Scale 8 mm 60 mm Fixed Code 25 µl Bevel 25F µl Bevel 50F µl Bevel 100F µl Bevel 250F µl Bevel 500F Removable 25 µl Bevel 25R µl Bevel 50R µl Bevel 100R µl Bevel 100R µl Bevel 250R µl Bevel 500R s Fitted with Repeating Adaptor See page 63 for more details about the RAX repeating adaptor. Removable Code 25 µl Bevel 25R-RAX µl Bevel 50R-RAX µl Bevel 100R-RAX µl Bevel 250R-RAX µl Bevel 500R-RAX To eliminate carryover between samples, flush the syringe with solvent 5-20 times, remembering to discard the first 2-3 washes. 38 For more syringe tips view our video at sge.com/support/videos

11 µl ped Borosilicate Glass Barrel Outer Diameter () Scale 10 µl = 6.5 mm, µl = 8 mm 10 µl = 54.1 mm, µl = 60 mm s and Fixed ped Code 6 Pack Part No. Part No. 10 µl Bevel 10F-GT µl Bevel 10F-GT µl Bevel 25F-GT µl Bevel 50F-GT µl Bevel 100F-GT µl Bevel 250F-GT µl Bevel 500F-GT Removable 10 µl Bevel 10R-GT µl Bevel 25R-GT µl Bevel 50R-GT µl Bevel 100R-GT µl Bevel 250R-GT µl Bevel 500R-GT Guided 10 µl Bevel 10R-GP-GT On-Column 10 µl On- Column Fixed Luer 10R-GT-OC- CE µl F-LT-GT µl F-LT-GT µl F-LT-GT µl F-LT-GT Fixed Luer Lock 50 µl F-LL-GT µl F-LL-GT µl F-LL-GT µl F-LL-GT For details of Luer Lock needles and alternative needle options see pages s General Purpose Manual s 39

12 s General Purpose Manual s ml ped Also Suitable for Pumps and Dispensers s and Borosilicate Glass Barrel Outer Diameter () Scale Thread in Button 1 ml = 9 mm, 2.5 ml = 11 mm, 5 ml = 14 mm, 10 ml = 18 mm, 25 ml = 27 mm, 50 ml = 32.8 mm, 100 ml = 40.8 mm 1 25 ml = 60 mm, 50 ml = 84.2 mm, 100 ml = 104 mm 6-32 UNC Fixed ped Code 1 ml Bevel 1MDF-GT ml Bevel 2.5MDF-GT Removable 1 ml Bevel 1MR-GT * 2.5 ml Bevel 2.5MDR-GT ml Bevel 5MDR-GT ml Bevel 10MDR-GT Fixed Luer 1.0 ml Luer 1MF-LT-GT * 2.5 ml Luer 2.5MDF-LT-GT Fixed Luer Lock 1.0 ml Luer Lock 1MDF-LL-GT ml Luer Lock 2.5MDF-LL-GT ml Luer Lock 5MDF-LL-GT ml Luer Lock 10MDF-LL-GT ml Luer Lock 25MDF-LL-GT Removable Luer Lock 5 ml Luer Lock 5MDR-LL-GT ml Luer Lock 10MDR-LL-GT ml Luer Lock 25MR-LL-GT ml Luer Lock 50MR-LL-GT * 100 ml Luer Lock 100MR-LL-GT * * No thread in plunger stem of syringe part numbers , , and s Valves valves are ideal for sample storage and transportation or to pressurize sample prior to injection. SGE offers three basic types of manually operated syringe valves; push-pull for smaller volumes (25 µl 2.5 ml), septum and pushbutton for larger volumes (5 ml 2 L). SGE Luer, Luer Lock and removable needle syringes can be fitted with valves. The valve allows fluid to be stored in the syringe without contamination. 40 For more syringe tips view our video at sge.com/support/videos

13 Push-pull Valves Septum Valve Push-button Valves CLOSE OPEN OPEN CLOSE (Turn to close) OPEN s and and Push-pull valves suit removable needle 25 µl ml syringes The septum cap (P/N ) allows sample access without loss or contamination. It can be removed and Luer Lock needles or devices fitted Suits 5 ml - 2 L syringes with removable Luer Lock or removable needle Suitable for any Luer Lock and Luer syringes or other Luer devices. With the valve in the closed position it is possible to move the plunger to pre-pressurize the sample. Description Valve Code Valve 25 µl ml * 25 µl ml ˆ 25 µl ml ml - 2 L ml - 2 L µl - 2 L * 50 mm, 0.63 mm cone tip needle. ˆ 50 mm, 0.47 mm cone tip needle. s Pre-fitted with Valves ped Code Pre-fitted with Removable Push-pull Valve Valve 50 µl µl µl µl ml ml Pre-fitted with Luer Lock Valve 1 ml ml ml ml ml ml ml Valve s For use with P/N and Pack Size Valve Cone Side Hole/Dome Cone See page 67 for the complete range of Luer Lock needles suitable for use on Luer Lock valves. s 41

14 s valves SealTight s and SealTight low pressure valves are designed for improved valve seal life. SGE valves have overcome the problem of leakage by reducing perpendicular rotor force, and optimizing the rotor face union, thereby improving plug integrity. The end result is a longer life seal. The SealTight Other valves, including custom OEM configurations, are available. Flow Path 1.5 mm (0.059") Threaded Ports 1/4 28 UNF Pressure Rating 120 psi Temperature Rating C Standard Weight 58 g Bulkhead Weight 65 g Breakaway Torque 0.15 Nm Lifetime Testing 8,000 cycles ADVANTAGES Extended life resulting from face rotor seal technology, making valves cost effective and reliable. Inert and Kel-F flow path compatible with a variety of solvents and sample matrices. Easily reassembled by hand: no need to torque it up like other valves. Screw thread for connection onto 5 ml 2 L syringes using syringe-valve connector ( ). APPLICATIONS Description Mounting Code Port Valves I flow 2 port Standard I flow 2 port T flow 3 port Standard L flow 3 port Standard T flow 3 port L flow 3 port SealTight Valve Fittings and Connectors Description Code Kel-F Female Luer Metal Thread Male Luer Lock - Flow Path Ferrules for 1/16" Tubing PF Ferrules for 1/8" Tubing PF SealTight valves offer the versatility to be utilized in a variety of industries and applications: Dispensers. Diluters. Flow path variation. Biocompatible, suitable for use in pathology equipment. 42 s