RAPPORT D'ANALYSE DES MATIERES PREMIERES. DSM DSM Nutritional Products, Inc. ;l\1.anuf ACTURIER: QUANTITE RE<;UE: SPECIFICATION.

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1 RAPPORT D'ANALYSE DES MATIERES PREMIERES Code No.: V-014 Spec. approuvees par l'assurance Qualite NOM DU PRODUIT: DISTRIBUTE UR: LOT DU DISTRIBUTEUR: DATE D'EXPIRATION: DATE DE RE-ANALYSE: Vitamin E Acetate 500 IUg NO. DE RECEPTION: R-35314@ (50%) * ;l\1.anuf ACTURIER: DSM DSM Nutritional Products, Inc. NO. DE LOT DU MAN.: NIA PAYS DU MANUFACTURIER: USA QUANTITE RE<;UE: 70 x 50 kg * DL Alpha Tocophe,yl Acetate 500 U1g DESCRIPTION SPECIFICATION OBSERVATION COULEUR: Blanc a blanc beige Conforme FORME: Poudre Iegere Conforme ANALYSE METHODE SPECIFICATION RESULTAT IDENTIFICATION: SOP.MP.068 Conforme Conforme ESSAI: (Acetate de dl-tocopheryle) SOP.MP U1g 530 U1g t Calcul Resultat X Entrer le resultat ci-dessus dans Visual Manufacturing PERTE DE POIDS: (105 C) USP <891> :;6,0% 2%t I SOLVANTS RESIDUELS:. USP <467> Rencontre Jes normes Conforme f, REVISE PAR: IIAJ1111 l( J, IDATE: COMMENTAIRE:l@Produit certifie -; Analyse par Laboval t Se refere au certificat du manufacturier f Se referer a la lettre de conf i rmation J-ol::f REJETE D Os- APPROUVE [kl {AtJ PAR: Controle Qualite DATE: oj.01-1-l O RELACIIEPAR Qr RESULTATSENTRESPAR: NES DATE: DATE: J Assurance Qualite

2 Certificat d'analyses Client: Date; CA: Att: Fax: PO: Produit: Vrtamine E Acetate 500 IUg (50%) Req: Code: V-014 Lot: Page: 11 Tests Specifications Resultats Methodes Description Couleur Blanc a blanc beige Conforme. Organoleptique Fonne Poudre legere Conforme Organoleptique Identification DL-cx-tocopheryl acetate (Vilamine E) Conforme Conforme MP Verifie par. Approuve par: {)ec # lt?i) 3 At--S2017-1' , 50e Avenue Lachine (Quebec} Canada H8T 2VS Tel.: Telec.:

3 DRY VITAMIN E ACETATE 50% TYPE SD Certifjcate for Customer Productcode : Lot No. : Analysis No. : CfC Number: Articlecode : Sales Name: Manufacturing Date: 13-JUN-2017 Best Use Before Date: 12-JUN-2020 Delivery Note No. Destination : Canada Customer Ref. No : Customer Article No: V014 Customer Name: Comment Quantity Shipped: KG Thank you for your order and continued business. DSM Nutritional Products is committed to delivering superior quality products and excellent services for our valued customers. If you have any questions, please contact our Account Service Center at Our webshop provides 247 access to the products and services of DSM Nutritional Products. Visit our website at: http: unlimitednutrition-na.dsm.com DSM Nutritional Products, Inc. 45 Waterview Boulevard Parsippany, NJ U.S.A Date of issue: 16-0ct-2017

4 DRY VITAMIN E ACETATE 50 o TYPE SD CERTFICA TE OF ANALYSIS Productcode : Lot No. Analysis No. Test Result Limits Specifications APPEARANCE Visual free flowing powder free flowing powder COLOR Visual LOSS ON DRYING Oven SODIUM BENZOATE TLC SORBIC ACID TLC ASSAY: DL-ALPHA TOCOPHERYL ACETATE LC MICROBIOLOGICAL PURITY (USP) Total Aerobic Bacteria Yeasts and Molds Enterobacteria Escherichia coli Salmonella sp Staphylococcus aureus Pseudomonas aeruginosa ') checked at regular intenals white to off-white 2 corresponds' corresponds* 53 <10 <10 less than 10 white to off-white max. 6 % present present min. 50 % Dimension Units max cfug max. 100 cfug less than 10 cfug 10g g 10g This lot was analysed and released by our authorized Quality Control Department and was found to meet the specifications as given above. The product meets all requirements of the following valid compendia when tested accordingly: USP and Ph.Eur. The Quality Assurance Manager Joan Ji DSM Nutritional Products 253 Macks Island Drive Belvidere New Jersey U.S.A 1 I 1 Date of Issue: 05-Jul-2017

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6 Document Control Unique ID RAPPORT D'ANALYSE DES MATIERES PREMIERES Code No.: V-014 Spec. approuvees par l'assurance Qualite NOM DU PRODUIT: Vitamin E Acetate 500 IUg NO. DE MCEPTION: (50%) *..;MANlJACTURIER: DISTRIBUTE UR: DSM Nutritional Products, Inc. LOT DU DISTRIBUTEUR: NO. DE LOT DU MAN.: DATE D'EXPIRATION: DSM PAYS DU MANUFACTURIER: USA DATE DEM-ANALYSE: NIA QUANTITE RE<;UE: 35 x 50 kg.1 * DL Alpha Tocophetyl Acetate 500 UIg DESCRIPTION SPECIFICATION OBSERVATION COULEUR: Blanc a blanc beige Blanc beige,, FORME: Poudre legere Poudre legere ANALYSE METHODE SPECIFICATION MSULTAT IDENTIFICATION: SOP.MP.068 Conforme Conforme ESSAI: SOP.MP UIg 530 UIg t "' (Acetate de dl-tocopheryle) Calcul Resultat X Entrer le resultat ci-dessus dans Visual Manufacturing PERTE DE POIDS: (105 C) USP <891> :,;; 6.0% 2%t SOLVANTS MSIDUELS: USP <467> Rencontre!es normes Conforme f. I- R _E_ V IS _ E P AR _ : _ -J.:.J...:..t!::w...,_-=.:. --,J...;_ D A _ TE _ : ;_ 2...;_ 0_ 17_-_ 1_' =- 1...;_ 5_--IREJETE COMMENT Produit certifie,, APPROUVE [LI. {j, Analyse par Laboval PAR ; II J'n,, l't I J '({,aj: VW'I t Se refere au certificat du manufacturier U-MtU4't:',r f Se referer a la lettre de confirmation _,, Controle Qualite DATE: D J i J RE LA CHE P j ;ta,_;,, c},,nj9f! RESUL TAT S ENTRES PAR: NES DATE: I DATE: Assurance Qualite,,.. '""'""-,,..,,... LUii - c I J

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8 DRY VITAMIN E ACETATE 50% TYPE SD Certificate for Customer Productcode : Lot No. : Analysis No. : ,IJ L..' CfC Number : Articlecode : Sales Name : Manufacturing Date : 15-JUN-2017 Best Use Before Date : 14-JUN :,, Delivery Note No. Destination : Canada Customer Ref. No : Customer Article No: V014,1 Customer Name: Comment Quantity Shipped: KG Thank you for your order and continued business. DSM Nutritional Products is committed to delivering superior quality products and excellent services for our valued customers. If you have any questions, please contact our Account Service Center at Our webshop provides 247 access to the products and services of DSM Nutritional Products. Visit our website at: http: unlimitednutrition-na.dsm.com DSM Nutritional Products, Inc. 45 Waterview Boulevard Parsippany, NJ U.S.A Date of issue: 07-Nov-2017

9 DRY VITAMIN E ACETATE 50% TYPE SD CERTIFICATE OF ANALYSIS Productcode : Lot No. Analysis No. Test Result Limits Specifications APPEARANCE Visual free flowing powder free flowing powder COLOR Visual LOSS ON DRYING Oven SODIUM BENZOATE TLC SORBIC ACID TLC ASSAY: DL-ALPHA TOCOPHERYL ACETATE LC MICROBIOLOGICAL PURITY (USP) Total Aerobic Bacteria Yeasts and Molds Enterobacteria Escherichia coli Salmonella sp Staphylococcus aureus Pseudomonas aeruginosa *) checked at regular intervals white to off-white 2 corresponds* corresponds* 53 <10 <10 less than 10 white to off-white max.6 % present present min. 50 % Dimension. Units max cfug max. 100 cfug less than 10 cfug 10g 25g 10g 10g This lot was analysed and released by our authorized Quality Control Department and was found to meet the specifications as given above. The product meets all requirements of the following valid compendia when tested accordingly: USP and Ph.Eur. The Quality Assurance Manager Joan Ji DSM Nutritional Products 253 Macks Island Drive Belvidere New Jersey U.S.A 1 1 Date of issue: 10-Jul-2017

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