Agilent 7700x ICP-MS

Transcription

1 Agilent 7700x ICP-MS Metals analysis Mid ppt to low ppb detection range Option to detect in four different gas modes to gain optimum detection of multiple metals or interferences in a sample Autosampler can hold 21, 50 ml falcon tubes and 180, 15 ml falcon tubes

2 Shimadzu 8040 LC-Triple Quadrupole MS with PDA and Fluorescence Detection Nexera X2 LC-30AD UHPLC system with a binary solvent system ESI triple quadrupole mass spectrometer SPD-M30A diode array detector RF-20A XS fluorescence detector Quantitative analysis or structural elucidation of small molecules Mid ppt to low ppb detection limits Mass Range: Da Temperature controlled autosampler holds 324, 2 ml RAM vials Column oven Acquired through Shimadzu Grant.

3 Thermo Scientific Altis LC-Triple Quadrupole MS UltiMate 3000 UHPLC System with a binary solvent system which allows 4 different mobile phases, but only 2 at a time. TSQ Altis ESI triple quadrupole mass spectrometer Online concentration capabilities Online concentration detection range in low ppt Standard detection range mid ppt to low ppb Mass Range: Da Temperature controlled autosampler holds 162, 2 ml RAM vials, and 30, 10 ml vials and column oven Run by laboratory staff only and primarily used for large projects

4 Thermo Scientific LTQ Orbitrap XL with Nano LC and HPLC capabilities High resolution mass spectrometer. o Resolution 60,000 at m/z 400 at a scan rate of 1 Hz o Up to 100,000 resolution o External calibration and lock mass for 1 ppm error. Easy nano LC 1200 Waters Alliance HT 2795 HPLC with temperature controlled autosampler which holds 144, 2 ml RAM vials and column oven. o Quaternary pump up to 4,500 psi. Mass Range o Linear Ion trap: m/z o Orbi-Trap: m/z Sensitivity sub-femtomol range for peptides

5 Bruker UltrafleXtreme MALDI-TOF/TOF kda mass range with linear mode kda mass range with reflection mode and LIFT fragmentation. CID or LID to analyze structure of proteins, RNA/DNA, and polymers. FlexImaging for MALDI Imaging Mass Spectrometry. BioTools for protein identification on Mascott database. BioTyper for bacteria culture Identification. SCiLs software package for 3D imaging and statistical analysis.

6 Waters 2695/ZQ Waters 2695 HPLC with temperature controlled autosampler which holds 120, 2 ml RAM vials and column oven psi maximum pressure quaternary pump. ESI source with quadrupole analyzer from Da. Source fragmentation by adjustable cone voltage. Nominal mass accuracy for direct injection or chromatographic analysis. 20 ng/ml to 10 μg/ml; Acetonitrile, Methanol, Water, or Isopropanol.

7 Agilent 6890/ Semivolatiles Automatic Liquid Sampler holds 100, 2 ml RAM vials. EI source and quadrupole analyzer from Da Rxi-5ms column for walk up analysis of organic reactions and quantitative analysis of semivolatiles. Chemstation software and NIST database searching of fragmentation patterns. Optional CDS8000 Thermal Desorption, Purge and Trap, and Pyrolyzer.

8 Agilent 6890/5973 Volatiles EI source and quadrupole analyzer from Da or FID. Restek RTX-Volatiles column Chemstation software and NIST database searching of fragmentation patterns. Optional CDS8000 Thermal Desorption, Purge and Trap, and Pyrolyzer. Optional Solatek 72 Purge and Trap autosampler with Velocity XPT Concentrator. Optional manual SPME analysis.

9 CDS8000 Concentrator Manual Purge and Trap. Manual thermal desorption tube sampling from active air sampling unit. Bulk headspace analysis options: 10 x 9.5 cm Large BDHS 13 x 3 cm (a silanized steel tray is available that sits in the center of the tube long ways, for height of 1.5 cm) 15 x 1.5 cm testube sampler Cryofocusing available.

10 Solatek 72 Purge and Trap with Velocity XPT Concentrator 72 vial autosampler for 40 ml purge and trap vials. In vial purge with heated sampler and stirring for soils and sludges. Add 0-20 ml of water before sampling vapor. 10 ml purge and trap liquid sampling sparging vessel. 3 Optional internal standard or calibrant addition vials online.

11 Perkin Elmer Clarus 580/Turbomatrix 40 Headspace GC-FID-ECD 40 vial autosampler for headspace analysis. Preheats samples during GC run to save time. Flame Ionization Detector and Electron Capture Detectors available. Minimum sample temperature of 35 C

12 Waters 2695/996 PDA Waters 2695 HPLC with 120 sample autosampler with column oven psi maximum pressure quaternary pump. UV detector with Empower software package for quantitative analysis.