1,2,3,6--Tetramethyltricyclo[ (3,9)]undec-3- ene. 16.alpha.-Acetyloxy-3.beta.,22.alpha.-dihydroxyolean- 12-en-28-al

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1 ,2,3,6--Tetramethyltricyclo[ (3,9)]undec-3- ene H-Purin-6-amine, [(2-fluorophenyl)methyl] alpha.-Acetyloxy-3.beta.,22.alpha.-dihydroxyolean- 12-en-28-al Ethyl 3,7,11,15-tetramethyl-2-hexadecenoate cis-vaccenic acid Sodium 1H,1H,2H,2H-Perfluorooctane Sulfonate (6:2) Sodium 1H,1H,2H,2H-Perfluorodecane Sulfonate (8:2) Sodium 1H,1H,2H,2H-Perfluorohexane Sulfonate (4:2) Perfluoro(2-Propoxypropanoic) Acid Hexene Methyl Abietate (1-Methylethylidene)-Bicyclo[4.1.0]Heptane ,3,3-Trimethylbicyclo[2.2.1]Heptan-2-One Methoxypropane Di(P-Nitrophenyl) Sulfide (E)-4-Octene Isopropylpodocarpen-12-Ol-20-Al ,5-Dichlorothiophene (3.Beta.,22E)-Ergosta-5,22-Dien-3-Ol Dimethyltetrasulfide ,3,5-Tribromo-2-Methoxybenzene Methyl-2-Furancarboxaldehyde ,3'4,4'-Tetrachlorodiphenylsulfide ,6-Dioxacyclododecane-7,12-dione Clothianidin beta.-Methoxyolean-12-ene H-Cyclopenta[a]pyrene H-Benz[de]anthracen-6-one (7A-Isopropenyl-4,5-Dimethyl-Octahydroinden-4- Yl)-3-Methyl Hexaethylene Glycol Monododecyl Ether Heptaethylene Glycol Monododecyl Ether Crown-5 M2-4:2FTS Sodium 1H,1H,2H,2H-perfluoro-1-[1,2-13C2]-hexane sulfonate (4:2) M2-6:2FTS Sodium 1H,1H,2H,2H-perfluoro-1-[1,2-13C2]-octane sulfonate (6:2) M2-8:2FTS Sodium 1H,1H,2H,2H-perfluoro-1-[1,2-13C2]-decane sulfonate (8:2) H-Carbazole, 9-phenyl Benzene, (1-methyl-3-butenyl) (3H)-Furanone, dihydro-5-pentyl ,2,3-Propanetriol, diacetate

2 H-2,3-Benzodiazepine, 1-methyl p-menthan-8-ol (3H)-Furanone, 5-hexyldihydro Oxalic acid, hexadecyl propyl ester Hemiketal fo 9,10-Dihydroxy derivative Dodecanoic acid, 2-hydroxy-1-(hydroxymethyl)ethyl ester H-Pyrrolo[2,3-b]pyridine, 4-methyl-2-phenyl Phenol, o-[(.alpha.-methylbenzyl)sulfonyl] Cyclohexane, 1,4-dimethyl-2-(2-methylpropyl)-, (1α,2β,4α) Glycerol, 1-hexadecanoate, diacetate Octadecanoic acid, 2-(acetyloxy)-1- [(acetyloxy)methyl]ethyl ester Eicosanoic acid, 2,3-bis(acetyloxy)propyl ester Azatetracyclo[ ,7.04,11]trideca-2,12-dien-5- one D-Allose SMPREMARK Sample Remark ,4,5,5-Tetramethyl-2-Cyclopenten-1-One CITRONELLA Piperidine Benzylidenecamphor Cyclooctane, butyl Azetidine, 2-methyl LONGIFOLENALDEHYDE Oxazole, 4,5-dimethyl Beta.-Acetoxyfriedo-Olean-7-Ene Undecyne Pyrazoline, 1-isopropyl-5-methyl Bicyclo[4.1.0]heptane Naphthalene, 1,2,3,4-tetrahydro-1-pheny Ethyl-3-methylnaphthalene Octyne, 7-methyl Benzo[c]phenanthrene, 1,12-dimethyl Cyclopropane, 1-butyl-1-methyl-2-propyl Bicyclo[4.1.0]heptane, 7-pentyl Bicyclo[4.1.0]heptane, 3-methyl ,10-Phenanthroline, 2,9-dimethyl Benzenemethanol, 4-(1-methylethyl) Pentanol, 4-methyl-2-propyl Pentenal, 2,2-dimethyl Cholestan-4-One Phenyl-1-Deuteroxy-2-Propene Cyclopentene, 5-hexyl-3,3-dimethyl Longiborn-8-Ene Benzonitrile, 4,4'-(1,2-ethenediyl)bis-

3 Dodecenol ,4,4-Trimethyl-2-pentenal Cyclohexane, 2-ethyl-1,3-dimethyl Cyclopentane, 1-butyl-2-ethyl Undecene, 4-methyl ,3,9-Trimethoxy-8-keto-10-hydroxy-syn Cyclooctene ,5-Dihydrobenzo[E]Pyrene ,4-Dihydro-3,6-dimethylphenanthrene Ethyl-3-propylquinoxaline-1,4-dioxide Bicyclo[2.2.1]heptane-7-methanol, 2-hydroxy-1, dimethyl Strictalamine Lycopodan-5-one, 12-hydroxy-15-methyl-, D1-2,4-Dimethyl-1-Pentene R-Methyl-2T-Phenylcyclopropane (+)-2-Endo,3-Endo-Dimethylbornane Cyclopropane, 1-butyl-2-pentyl-, cis (5-Chloro-8-Quinolinato-O,N)Borane (Z)-6,6-Dimethylcyclooct-4-en-1-one Tricyclo[ (2,5)]dec-8-ene, 1,2,3,3,4,4,5, octafluoro Bicyclo[2.2.1]hept-2-ylethanone H-9-Silafluorene, 9-methyl H-Pyrazole, 4,5-dihydro-3-methyl-1-propyl Tricyclo[ (3,7)]decane, 2-bromo ,5-Dimethylhexa-1,3-Diene Propenal, 3-(2,6,6-trimethylcyclohexen-1-yl) ,3-Diselenolane-2-thione ,2-Benzenedicarboxylic acid, dicyclohexyl ester ,5-Dicyano-2-isopropylimidazole Estra-1,3,5(10)-triene-4,17-diol, 3-methoxy-, (17.beta.) Spiro[benzofuran-2(3H),2'-oxiran]-3-one, 6-methoxy- 3'-phenyl Propen-1-One, 1-(2-Hydroxyphenyl)-3-(4- Hydroxyphenyl) Estra-1,3,5(10)-trien-17-one, 16.beta.-fluoro-3- methoxy Chlorobenzenemethanol Benzoyl-(rel)-benzoic acid N,N-diethyl-1,4-Benzenediamine PCBTOTCONG Total PCB Congeners PCBTRI_PLUS Sum of Tri+ PCB Concentrations Cyclohexyl-3-Deuteroprop-1-Ene (1 -Isopropyl-2,2 -dimethylcyclopentyl)-1-propanol

4 (4-Methoxyphenyl)-N,N,2-trimethyl-1-pyrrolamine exo-Hydroxy-10- oxatetracyclo[ (3,11).0(4,9)]tridecan-2-one [4aS- (4a.alpha.,4b.beta.,7.alpha.,8.alpha.,8a.alpha.,10a.b eta.)]-tetradecahydro-1,1,4a,7,8a-pentamethyl-8- butylphenanthrene (2S*,1'S*)-2-(2'-(Benzyloxy)-1'-methylethyl)-2,3- dihydro-4h-pyran-4-one (Z)-4-2,6,6 -Trimethyl-2 -cyclohexen-1 -yl)-3-penten- 2-one Morpholinesulfenamide, N,N-bis(trimethylsilyl) Ethylidene-7-alpha-methyl-cis-1H-Indene ,2,3,4,5,6-Hexachloro-cyclohexane Benzo[b]selenophene-3-carboxylic acid, 2-methyl-, methyl ester Benzenemethanol, ar, ar,.alpha.-trimethyl VINYLINDENE (R)-3-Methylcyclohexanone ,4-Dioxane, 2,5-dimethyl- 1,2,3,4,4A,7-Hexahydro-1,6-Dimethyl-4-( Methylnaphthalene Methyl-4-Indanol ,3,4,5,6,7-Hexahydro-1H-Inden-1-One (4-Methylphenyl)-4-Phenylbuta-1,3-Diene Trans-4,4'-Dimethoxychalcone Cyclobutene, 2-propenylidene Docosane, 7-butyl Octyldocosane 2,2-Dimethyl-3-(3,7,12,16,20-Pentamethyl-3,7,11,15, Oxirane (4-Acetylphenyl)Phenylmethane Methyl-1-Buten-3-Yne trans-(2-octenyl)succinic anhydride Methyl-1,5-Hexadien-3-Yne Ethyl Acetate - C13 1,2-Benzenedicarboxylic acid, butyl 2-ethylhexyl ester Docosyl pentafluoropropionate Methyl-1,4-heptadiene α-citronellal T-Butyl-4-Methylimidazole Octacosanol acetate ,5-Cyclohexadiene-1,4-Dione, 2-(Phenylthio) Ethanone, 1-(2,5-dimethylphenyl) H-Indene, 1-methylene-

5 ,7,7-Trimethylcyclohepta-1,3,5-triene ,1,3,3,3-Pentafluoro-2-(Trifluoromethyl)-1-Propene Thiophosgene (2H-Benzotriazol-2-Yl)-5-Methylphenol Sabina ketone ,2-Dimethyl-3,5-decadiene Dodecyl pentafluoropropionate Bromotridecane Cyclohexyl methyl ketone L 13C8-Perfluorooctane sulfonamide Perfluoropentanesulfonic Acid (Pfpes) Perfluorononanesulfonic Acid (Pfns) E-11-Hexadecenal (+)-.alpha.-terpineol (p-menth-1-en-8-ol) Sulfurous Acid, Butyl Dodecyl Ester Oxalic Acid, 2-Ethylhexyl Tetradecyl Ester Dotriacontyl Trifluoroacetate Tetratriacontyl Pentafluoropropionate Tetratriacontyl Heptafluorobutyrate Dotriacontyl Heptafluorobutyrate Octatriacontyl Trifluoroacetate ,4-Dimethylcumene Isobutyl Tetradecyl Ether Cis-1,3-Dimethyl-Cyclohexanol Pyridine-3-Carboxamide, Oxime, N-(2- Trifluoromethylphenyl) ,2,4A,6A,8A,9,12B,14A-Octamethyl- 1,2,3,4,4A,5,6,6A,6B,7,8,8 13C2PFHXSA 1H,1H,2H,2H-Perfluoro[1,2-13C2]Hexanesulfonic Acid (M2-4:2Fts) 6H13C2PFHXSA 1H,1H,2H,2H-Perfluoro[1,2-13C2]Hexanesulfonic Acid (M2-4:2Fts) 6H13C2PFOSA 1H,1H,2H,2H-Perfluoro[1,2-13C2]Octanesulfonic Acid (M2-6:2Fts) 6H13CPFDSA 1H,1H,2H,2H-Perfluoro[1,2-13C2]Decanesulfonic Acid (M2-8:2Fts) 6HPFHXSA 1H,1H,2H,2H-Perfluorohexanesulfonic Acid (4:2Fts) M3PFBS Perfluoro[2,3,4-13C3]Butanesulfonic Acid (M3Pfbs) M8PFOS Perfluoro[13C8]Octanesulfonic Acid (M8Pfos) Cis-9-Hexadecenoic Acid Revised cis-propenylbenzene Revised Tetracosanol Revised ,2-Dimethylindene, 2,3-dihydro- Revised Oxalic Acid, Decyl 2-Ethylhexyl Ester Revised

6 RT_ANALYTIC_METHOD Change Log 10/5/2017-2/20/2018 #ANALYTIC_METHOD PREFERRED_NAME Action SOM02 VOLATILE ORGANIC COMPOUNDS SW9010C Total and Amenable Cyanide USDA 26 Soil Moisture Content E1694 Pharmaceuticals and Personal Care Products in Water, Soil, Sediment, and Biosolids by HPLC/MS/MS (December 2007) ISM02.4 METALS SOM02.4 VOLATILE ORGANIC COMPOUNDS

7 RT_COMPANY Change Log 10/5/2017-2/20/2018 #COMPANY CODE COMPANY TYPE COMPANY NAME CONTACT NAME Action HURLEYWALSH SURVEYOR Hurley and Welsh Land Surveying & Engineering, PLLC Alexandra Hurley C2G-NP CONSULTANT C2G Environmental Consultants, LLC Cara Gentry MCI SUBCONTRACTOR Mark Cerrone Inc. Nathan Clifton USAENVIRON CONSULTANT USA Environment, LP Robert H. Frank II SOVEREIGNNY CONSULTANT Sovereign Consultants, Inc. Albert Tonn ARCADISNY CONSULTANT ARCADISNY Edward Mason Revised

8 RT_QUALIFIER Change Log 10/5/2017-2/20/2018 #QUALIFIER DESC (Organic, Inorganic) Action BH BL INDICATES THE ANALYTE WAS ALSO DETECTED IN THE ASSOCIATED BLANK AT A LEVEL MORE THAN 10 TIMES THAT FOUND IN THE SAMPLE INDICATES THE ANALYTE WAS ALSO DETECTED IN THE ASSOCIATED BLANK AT A LEVEL LESS THAN 10 TIMES THAT FOUND IN THE SAMPLE

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