ANALYTICAL REPORT. Job Number: Job Description: Tim Miller Associates, Inc.

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1 ANALYTICAL REPORT Job Number: Job Description: Tim Miller Associates, Inc. For: Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Attention: Ms. Maureen Fisher Debra Bayer Customer Service Manager 12/09/2009 The test results in this report meet all NELAP requirements unless specified within the case narrative. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory. EnviroTest Laboratories Inc. certifies that the analytical results contained herein apply only to the samples tested as received by our laboratory. All questions regarding this report should be directed to the EnviroTest Customer Service Representative. EnviroTest Laboratories, Inc. Certifications and Approvals: NELAP Accredited, NYSDOH 10142, NJDEP NY015, CTDOPH PH-0554, EPA NY Envirotest Laboratories, Inc. 315 Fullerton Avenue, Newburgh, NY Tel (845) Fax (845) Page 1 of 22 12/09/2009

2 Job Narrative 420-J Comments No additional comments. Receipt All samples were received in good condition within temperature requirements. GC VOA No analytical or quality issues were noted. Metals Method Rev 4.4: One or more compounds (Ag) in the continuing calibration verification (CCV) for batch recovered above the upper control limit. These compounds are flagged with carrots (^) on the sample result sheet. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported with high confidence of no false negatives. Method Rev 4.4: One or more compounds (Ag) in the continuing calibration verification (CCV) for batch recovered above the upper control limit. These compounds are flagged with carrots (^) on the sample result sheet. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported with high confidence of no false negatives. Method Rev 4.4: One or more compounds (Ag) in the continuing calibration verification (CCV) for batch recovered above the upper control limit. These compounds are flagged with carrots (^) on the sample result sheet. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported with high confidence of no false negatives. No other analytical or quality issues were noted. General Chemistry No analytical or quality issues were noted. Biology No analytical or quality issues were noted. Page 2 of 22 12/09/2009

3 METHOD SUMMARY Client: Tim Miller Associates, Inc. Description Matrix Water ICP Metals by Series Drinking Water Prep Determination Step Lab Location EnvTest EnvTest Job Number: Method Preparation Method EPA Rev 4.4 EPA 200 ICPMS Metals by Series Drinking Water Prep Determination Step EnvTest EnvTest EPA EPA 200 Apparent Color EnvTest SM B Mercury in Water by CVAA Digestion for CVAA Mercury in Waters EnvTest EnvTest EPA EPA Anions by Ion Chromatography EnvTest MCAWW Anions by Ion Chromatography EnvTest MCAWW Volatile Organic Compounds by Purge and Trap (Preserved) EnvTest EPA Turbidity Odor, Threshold Test Cyanide, Total: Colorimetric Method Cyanide: Distillation Membrane Filter Technique - Fecal Coliform Procedure Total Coliform and Escherichia coli by Colilert - Quantity Tray General Sub Contract Method Lab References: = EnvTest = EnviroTest EnvTest EnvTest EnvTest EnvTest EnvTest EnvTest SM20 SM 2130B SM20 SM 2150B SM18 SM 4500 CN E SM18 SM 4500 CN C SM18 SM 9222D SMWW SM 9223 Subcontract Method References: EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/ , March 1983 And Subsequent Revisions. SM18 = "Standard Methods For The Examination Of Water And Wastewater", 18th Edition, SM20 = "Standard Methods For The Examination Of Water And Wastewater", 20th Edition." SM21 = SMWW = "Standard Methods for the Examination of Water and Wastewater" EnviroTest Laboratories, Inc. Page 3 of 22 12/09/2009

4 SAMPLE SUMMARY Client: Tim Miller Associates, Inc. Job Number: Lab Sample ID Client Sample ID Client Matrix Date/Time Sampled Date/Time Received Well-O Lost Lake Resort Drinking Water Well-P Lost Lake Resort Drinking Water Well-DD Lost Lake Resort Drinking Water 11/12/ /12/ /12/ /12/ /12/ /12/ EnviroTest Laboratories, Inc. Page 4 of 22 12/09/2009

5 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-O Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /12/ Drinking Water Analyte Result/Qualifier Unit NONE NONE Dilution Method: 2120B Date Analyzed: 11/12/ Apparent Color 5.0 Color Units 1.0 Page 5 of 22 12/09/2009

6 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-O Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /12/ Drinking Water Analyte Result/Qualifier Unit RL RL Dilution Method: Date Analyzed: 11/20/ Trichlorofluoromethane 0.50 U ug/l Trichloroethene 0.50 U ug/l trans-1,3-dichloropropene 0.50 U ug/l trans-1,2-dichloroethene 0.50 U ug/l Toluene 0.50 U ug/l Tetrachloroethene 0.50 U ug/l tert-butylbenzene 0.50 U ug/l Styrene 0.50 U ug/l sec-butylbenzene 0.50 U ug/l o-xylene 0.50 U ug/l N-Propylbenzene 0.50 U ug/l n-butylbenzene 0.50 U ug/l Methylene Chloride 1.0 U ug/l MTBE 1.0 U ug/l m-xylene & p-xylene 0.50 U ug/l Isopropylbenzene 0.50 U ug/l Hexachlorobutadiene 0.50 U ug/l Ethylbenzene 0.50 U ug/l Dichlorodifluoromethane 0.50 U ug/l Dibromomethane 0.50 U ug/l cis-1,3-dichloropropene 0.50 U ug/l cis-1,2-dichloroethene 0.50 U ug/l Chloromethane 0.50 U ug/l Chloroethane 0.50 U ug/l Bromochloromethane 0.50 U ug/l Chlorobenzene 0.50 U ug/l Carbon tetrachloride 0.50 U ug/l Bromomethane 0.50 U ug/l Bromobenzene 0.50 U ug/l Benzene 0.50 U ug/l p-isopropyltoluene 0.50 U ug/l Chlorotoluene 0.50 U ug/l Chlorotoluene 0.50 U ug/l ,2-Dichloropropane 0.50 U ug/l ,4-Dichlorobenzene 0.50 U ug/l ,3-Dichloropropane 0.50 U ug/l ,3-Dichlorobenzene 0.50 U ug/l ,3,5-Trimethylbenzene 0.50 U ug/l ,2-Dichloropropane 0.50 U ug/l ,2-Dichloroethane 0.50 U ug/l Page 6 of 22 12/09/2009

7 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-O Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /12/ Drinking Water Analyte Result/Qualifier Unit RL RL Dilution 1,2-Dichlorobenzene 0.50 U ug/l ,2,4-Trimethylbenzene 0.50 U ug/l ,2,4-Trichlorobenzene 0.50 U ug/l ,2,3-Trichloropropane 0.50 U ug/l ,2,3-Trichlorobenzene 0.50 U ug/l ,1-Dichloropropene 0.50 U ug/l ,1-Dichloroethene 0.50 U ug/l ,1-Dichloroethane 0.50 U ug/l ,1,2-Trichloroethane 0.50 U ug/l ,1,2,2-Tetrachloroethane 0.50 U ug/l ,1,1-Trichloroethane 0.50 U ug/l ,1,1,2-Tetrachloroethane 0.50 U ug/l Vinyl chloride 0.50 U ug/l Method: Rev 4.4 Date Analyzed: 11/20/ Prep Method: 200 Date Prepared: 11/12/ Ag 10 U ^ ug/l Fe 60 U ug/l Mn 29 ug/l Na ug/l Zn 20 U ug/l Method: Date Analyzed: 11/18/ Prep Method: Date Prepared: 11/12/ Pb 1.0 U ug/l As 1.9 ug/l Be 0.30 U ug/l Cd 1.0 U ug/l Cr 1.7 ug/l Cu 1.0 U ug/l Ni 0.50 U ug/l Tl 0.30 U ug/l Ba 170 ug/l Se 2.0 U ug/l Method: Date Analyzed: 11/30/ Sb 0.43 ug/l Method: Date Analyzed: 11/20/ Prep Method: Date Prepared: 11/19/ Hg 0.20 U ug/l Method: Date Analyzed: 11/13/ Nitrate as N U mg/l Page 7 of 22 12/09/2009

8 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-O Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /12/ Drinking Water Analyte Result/Qualifier Unit RL RL Dilution Nitrite as N U mg/l Sulfate 7.1 mg/l Fluoride 0.50 U mg/l Method: Date Analyzed: 11/17/ Chloride 7.9 mg/l Method: SM 2130B Date Analyzed: 11/13/ Turbidity 0.38 NTU Method: SM 2150B Date Analyzed: 11/12/ Odor 2.0 Units for Odor Method: SM 4500 CN E Date Analyzed: 11/20/ Prep Method: SM 4500 CN C Date Prepared: 11/20/ Cyanide, Total U mg/l Method: SM 9222D Date Analyzed: 11/12/ Coliform, Fecal 1.0 U CFU/100mL Method: SM 9223 Date Analyzed: 11/12/ Coliform, Total 1.0 U CFU/100mL Escherichia coli 1.0 U CFU/100mL Page 8 of 22 12/09/2009

9 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-P Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /12/ Drinking Water Analyte Result/Qualifier Unit NONE NONE Dilution Method: 2120B Date Analyzed: 11/12/ Apparent Color 10 Color Units 1.0 Page 9 of 22 12/09/2009

10 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-P Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /12/ Drinking Water Analyte Result/Qualifier Unit RL RL Dilution Method: Date Analyzed: 11/20/ Trichlorofluoromethane 0.50 U ug/l Trichloroethene 0.50 U ug/l trans-1,3-dichloropropene 0.50 U ug/l trans-1,2-dichloroethene 0.50 U ug/l Toluene 0.50 U ug/l Tetrachloroethene 0.50 U ug/l tert-butylbenzene 0.50 U ug/l Styrene 0.50 U ug/l sec-butylbenzene 0.50 U ug/l o-xylene 0.50 U ug/l N-Propylbenzene 0.50 U ug/l n-butylbenzene 0.50 U ug/l Methylene Chloride 1.0 U ug/l MTBE 1.0 U ug/l m-xylene & p-xylene 0.50 U ug/l Isopropylbenzene 0.50 U ug/l Hexachlorobutadiene 0.50 U ug/l Ethylbenzene 0.50 U ug/l Dichlorodifluoromethane 0.50 U ug/l Dibromomethane 0.50 U ug/l cis-1,3-dichloropropene 0.50 U ug/l cis-1,2-dichloroethene 0.50 U ug/l Chloromethane 0.50 U ug/l Chloroethane 0.50 U ug/l Bromochloromethane 0.50 U ug/l Chlorobenzene 0.50 U ug/l Carbon tetrachloride 0.50 U ug/l Bromomethane 0.50 U ug/l Bromobenzene 0.50 U ug/l Benzene 0.50 U ug/l p-isopropyltoluene 0.50 U ug/l Chlorotoluene 0.50 U ug/l Chlorotoluene 0.50 U ug/l ,2-Dichloropropane 0.50 U ug/l ,4-Dichlorobenzene 0.50 U ug/l ,3-Dichloropropane 0.50 U ug/l ,3-Dichlorobenzene 0.50 U ug/l ,3,5-Trimethylbenzene 0.50 U ug/l ,2-Dichloropropane 0.50 U ug/l ,2-Dichloroethane 0.50 U ug/l Page 10 of 22 12/09/2009

11 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-P Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /12/ Drinking Water Analyte Result/Qualifier Unit RL RL Dilution 1,2-Dichlorobenzene 0.50 U ug/l ,2,4-Trimethylbenzene 0.50 U ug/l ,2,4-Trichlorobenzene 0.50 U ug/l ,2,3-Trichloropropane 0.50 U ug/l ,2,3-Trichlorobenzene 0.50 U ug/l ,1-Dichloropropene 0.50 U ug/l ,1-Dichloroethene 0.50 U ug/l ,1-Dichloroethane 0.50 U ug/l ,1,2-Trichloroethane 0.50 U ug/l ,1,2,2-Tetrachloroethane 0.50 U ug/l ,1,1-Trichloroethane 0.50 U ug/l ,1,1,2-Tetrachloroethane 0.50 U ug/l Vinyl chloride 0.50 U ug/l Method: Rev 4.4 Date Analyzed: 11/20/ Prep Method: 200 Date Prepared: 11/16/ Ag 10 U ^ ug/l Fe 150 ug/l Mn 15 U ug/l Na B ug/l Zn 20 U ug/l Method: Date Analyzed: 11/18/ Prep Method: 200 Date Prepared: 11/16/ Pb 1.0 U ug/l As 4.4 ug/l Be 0.30 U ug/l Cd 1.0 U ug/l Cr 1.0 U ug/l Cu 6.1 ug/l Ni 0.55 ug/l Sb 0.40 U ug/l Tl 0.30 U ug/l Ba 99 ug/l Se 2.0 U ug/l Method: Date Analyzed: 11/20/ Prep Method: Date Prepared: 11/19/ Hg 0.20 U ug/l Method: Date Analyzed: 11/13/ Nitrate as N U mg/l Nitrite as N U mg/l Page 11 of 22 12/09/2009

12 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-P Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /12/ Drinking Water Analyte Result/Qualifier Unit RL RL Dilution Sulfate 5.0 U mg/l Fluoride 0.50 U mg/l Method: Date Analyzed: 11/17/ Chloride 20 mg/l Method: SM 2130B Date Analyzed: 11/13/ Turbidity 6.8 g NTU Method: SM 2150B Date Analyzed: 11/12/ Odor 2.0 Units for Odor Method: SM 4500 CN E Date Analyzed: 11/20/ Prep Method: SM 4500 CN C Date Prepared: 11/20/ Cyanide, Total mg/l Method: SM 9222D Date Analyzed: 11/12/ Coliform, Fecal 1.0 U CFU/100mL Method: SM 9223 Date Analyzed: 11/12/ Coliform, Total 1.0 U CFU/100mL Escherichia coli 1.0 U CFU/100mL Page 12 of 22 12/09/2009

13 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-DD Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /12/ Drinking Water Analyte Result/Qualifier Unit NONE NONE Dilution Method: 2120B Date Analyzed: 11/12/ Apparent Color 5.0 Color Units 1.0 Page 13 of 22 12/09/2009

14 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-DD Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /12/ Drinking Water Analyte Result/Qualifier Unit RL RL Dilution Method: Date Analyzed: 11/20/ Trichlorofluoromethane 0.50 U ug/l Trichloroethene 0.50 U ug/l trans-1,3-dichloropropene 0.50 U ug/l trans-1,2-dichloroethene 0.50 U ug/l Toluene 0.50 U ug/l Tetrachloroethene 0.50 U ug/l tert-butylbenzene 0.50 U ug/l Styrene 0.50 U ug/l sec-butylbenzene 0.50 U ug/l o-xylene 0.50 U ug/l N-Propylbenzene 0.50 U ug/l n-butylbenzene 0.50 U ug/l Methylene Chloride 1.0 U ug/l MTBE 1.0 U ug/l m-xylene & p-xylene 0.50 U ug/l Isopropylbenzene 0.50 U ug/l Hexachlorobutadiene 0.50 U ug/l Ethylbenzene 0.50 U ug/l Dichlorodifluoromethane 0.50 U ug/l Dibromomethane 0.50 U ug/l cis-1,3-dichloropropene 0.50 U ug/l cis-1,2-dichloroethene 0.50 U ug/l Chloromethane 0.50 U ug/l Chloroethane 0.50 U ug/l Bromochloromethane 0.50 U ug/l Chlorobenzene 0.50 U ug/l Carbon tetrachloride 0.50 U ug/l Bromomethane 0.50 U ug/l Bromobenzene 0.50 U ug/l Benzene 0.50 U ug/l p-isopropyltoluene 0.50 U ug/l Chlorotoluene 0.50 U ug/l Chlorotoluene 0.50 U ug/l ,2-Dichloropropane 0.50 U ug/l ,4-Dichlorobenzene 0.50 U ug/l ,3-Dichloropropane 0.50 U ug/l ,3-Dichlorobenzene 0.50 U ug/l ,3,5-Trimethylbenzene 0.50 U ug/l ,2-Dichloropropane 0.50 U ug/l ,2-Dichloroethane 0.50 U ug/l Page 14 of 22 12/09/2009

15 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-DD Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /12/ Drinking Water Analyte Result/Qualifier Unit RL RL Dilution 1,2-Dichlorobenzene 0.50 U ug/l ,2,4-Trimethylbenzene 0.50 U ug/l ,2,4-Trichlorobenzene 0.50 U ug/l ,2,3-Trichloropropane 0.50 U ug/l ,2,3-Trichlorobenzene 0.50 U ug/l ,1-Dichloropropene 0.50 U ug/l ,1-Dichloroethene 0.50 U ug/l ,1-Dichloroethane 0.50 U ug/l ,1,2-Trichloroethane 0.50 U ug/l ,1,2,2-Tetrachloroethane 0.50 U ug/l ,1,1-Trichloroethane 0.50 U ug/l ,1,1,2-Tetrachloroethane 0.50 U ug/l Vinyl chloride 0.50 U ug/l Method: Rev 4.4 Date Analyzed: 11/20/ Prep Method: 200 Date Prepared: 11/12/ Ag 10 U ^ ug/l Fe 60 U ug/l Mn 15 U ug/l Na 4800 ug/l Zn 87 ug/l Method: Date Analyzed: 11/18/ Prep Method: 200 Date Prepared: 11/12/ Pb 1.0 U ug/l As 1.4 U ug/l Be 0.30 U ug/l Cd 1.0 U ug/l Cr 1.6 ug/l Cu 1.4 ug/l Ni 0.77 ug/l Sb 0.40 U ug/l Tl 0.30 U ug/l Ba 43 ug/l Se 2.0 U ug/l Method: Date Analyzed: 11/20/ Prep Method: Date Prepared: 11/19/ Hg 0.20 U ug/l Method: Date Analyzed: 11/13/ Nitrate as N mg/l Nitrite as N U mg/l Page 15 of 22 12/09/2009

16 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-DD Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /12/ Drinking Water Analyte Result/Qualifier Unit RL RL Dilution Sulfate 8.1 mg/l Fluoride 0.50 U mg/l Method: Date Analyzed: 11/17/ Chloride 2.2 mg/l Method: SM 2130B Date Analyzed: 11/13/ Turbidity 0.84 NTU Method: SM 2150B Date Analyzed: 11/12/ Odor 2.0 Units for Odor Method: SM 4500 CN E Date Analyzed: 11/20/ Prep Method: SM 4500 CN C Date Prepared: 11/20/ Cyanide, Total U mg/l Method: SM 9222D Date Analyzed: 11/12/ Coliform, Fecal 1.0 U CFU/100mL Method: SM 9223 Date Analyzed: 11/12/ Coliform, Total 1.0 U CFU/100mL Escherichia coli 1.0 U CFU/100mL Page 16 of 22 12/09/2009

17 DATA REPORTING QUALIFIERS Client: Tim Miller Associates, Inc. Job Number: Lab Section Qualifier Description GC VOA U The analyte was analyzed for but not detected at or above the stated limit. Metals ^ B U ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA or MRL standard: Instrument related QC exceeds the control limits. Compound was found in the blank and sample. The analyte was analyzed for but not detected at or above the stated limit. General Chemistry g U Result fails applicable drinking water standards The analyte was analyzed for but not detected at or above the stated limit. EnviroTest Laboratories, Inc. Page 17 of 22 12/09/2009

22 LOGIN SAMPLE RECEIPT CHECK LIST Client: Tim Miller Associates, Inc. Job Number: Login Number: Question T/F/NA Comment Radioactivity either was not measured or, if measured, is at or below background NA The cooler's custody seal, if present, is intact. NA The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. There are no discrepancies between the sample IDs on the containers and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. If necessary, staff have been informed of any short hold time or quick TAT needs Multiphasic samples are not present. Samples do not require splitting or compositing. EnviroTest Laboratories, Inc. Page 22 of 22 12/09/2009

23 ANALYTICAL REPORT Job Number: Job Description: For: EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Attention: Ms. Janine Rader Sheila Hoffman Project Manager I sheila.hoffman@testamericainc.com 11/30/2009 Approved for release. Sheila Hoffman Project Manager I 11/30/ :15 PM cc: Debbie Bayer Ms. Renee Cusack Ms. Joyce Esposito Ms. Alicia Labare The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the person who signed this report. Savannah Certifications and ID #s: A2LA: ; AL: 41450; ARDEQ: ; ARDOH; CA: 03217CA; CO; CT: PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: ; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA DEQ: 30690; LA DHH: LA080008; ME: ; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV: GA00006; NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: ; PR: GA00006; RI: LAO00244; SC: ; TN: TN0296; TX: T ; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV DHHR: 9950 C; WI DNR: ; WY/EPAR8: 8TMS-Q TestAmerica Laboratories, Inc. TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA Tel (912) Fax (912) Page 1 of 17 11/30/2009

24 Job Narrative Comments No additional comments. Receipt All samples were received in good condition within temperature requirements. GC/MS Semi VOA Method(s) 525.2: The laboratory control sample (LCS) for batch exceeded control limits for the following analytes: hexachlorocyclopentadiene. A low-level LCS (LLCS), spiked at the reporting limit (RL), was prepared with this batch. The affected target analytes recovered within acceptance limits; therefore, the LLCS demonstrates the analytical system had sufficient sensitivity to detect the compounds had they been present. Since the affected target compounds were not detected in the samples, the data have been reported and qualified. Method(s) 525.2: The large number of analytes included in the continuing calibration verification (CCV) gives a high probability that one or more analytes will be outside acceptance criteria. As indicated in the reference method, analysis may proceed as long as no more than 10% of the analytes of interest are outside the method-defined %D criteria. No other analytical or quality issues were noted. HPLC No analytical or quality issues were noted. GC Semi VOA Method(s) 504.1: The continuing calibration verification (CCV) for analytical batch exceeded control criteria for method 504. The data have been qualified and reported from column 1. Method(s) 504.1: Matrix spikes for batch could not be recovered due to sample matrix interferences which required sample dilution. The associated laboratory control sample (LCS) met acceptance criteria. Method(s) 508: Two surrogates are used for this analysis. The laboratory's SOP allows one of these surrogates to be outside acceptance criteria without performing re-extraction/re-analysis. The following sample(s) contained an allowable number of surrogate compounds outside limits: Well-O Lost Lake Resort ( ). These results have been reported and qualified. Method(s) 515.1: The matrix spike / matrix spike duplicate (MS/MSD) precision for batch was outside control limits. No other analytical or quality issues were noted. General Chemistry No analytical or quality issues were noted. Page 2 of 17 11/30/2009

25 METHOD SUMMARY Client: EnviroTest Laboratories Inc Job Number: Description Lab Location Method Preparation Method Matrix Water Semivolatile Organic Compounds (GC/MS) TAL SAV EPA Extraction of Semivolatile Compounds TAL SAV EPA EDB, DBCP and 1,2,3-TCP (GC) TAL SAV EPA-DW Microextraction TAL SAV EPA-DW Chlorinated Pesticides & PCBs (GC) TAL SAV EPA 508 Liquid-Liquid Extraction (Separatory Funnel) TAL SAV EPA 508 Herbicides (GC) TAL SAV EPA Extraction of Chlorinated Acids TAL SAV EPA-DW Disinfection By-Products, (IC) TAL SAV EPA 300.1B Disinfection By-Products, (IC) TAL SAV EPA 300.1B Carbamate Pesticides (HPLC) TAL SAV EPA Lab References: TAL SAV = TestAmerica Savannah Method References: EPA = US Environmental Protection Agency EPA-01 = "Methods For The Determination Of Nonconventional Pesticides In Municipal And Industrial Wastewater", EPA/821/R/92/002, April EPA-DW = "Methods For The Determination Of Organic Compounds In Drinking Water", EPA/600/4-88/039, December 1988 And Its Supplements. TestAmerica Savannah Page 3 of 17 11/30/2009

26 METHOD / ANALYST SUMMARY Client: EnviroTest Laboratories Inc Job Number: Method Analyst Analyst ID EPA EPA 300.1B EPA 300.1B EPA EPA-DW EPA 508 EPA Davis, Nancy Brazell, Connie Campbell, Sophia M Brazell, Connie Meincke, Griffin Meincke, Griffin Kellar, Joshua ND CB SMC CB GM GM JK TestAmerica Savannah Page 4 of 17 11/30/2009

27 SAMPLE SUMMARY Client: EnviroTest Laboratories Inc Job Number: Lab Sample ID Client Sample ID Client Matrix Date/Time Sampled Date/Time Received Well-O Lost Lake Resort Water Well-P Lost Lake Resort Water Well-DD Lost Lake Resort Water 11/12/ /13/ /12/ /13/ /12/ /13/ TestAmerica Savannah Page 5 of 17 11/30/2009

28 Ms. Janine Rader EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Job Number: Client Sample ID: Lab Sample ID: Well-O Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /13/ Water Analyte Result/Qualifier Unit MDL Dilution Method: Date Analyzed: 11/18/ Prep Method: Date Prepared: 11/16/ Alachlor <0.034 ug/l Atrazine <0.023 ug/l Benzo[a]pyrene <0.030 ug/l Bis(2-ethylhexyl) phthalate <0.63 ug/l Di(2-ethylhexyl)adipate <0.63 ug/l Hexachlorobenzene <0.043 ug/l Hexachlorocyclopentadiene <0.044 * ug/l Butachlor <0.033 ug/l Simazine <0.036 ug/l Metolachlor <0.021 ug/l Metribuzin <0.023 ug/l Propachlor <0.026 ug/l Surrogate Perylene-d12 90 % Acceptance Limits Method: 300.1B Date Analyzed: 11/21/ Bromate <2.6 ug/l Surrogate Dichloroacetic acid 96 % Acceptance Limits Method: Date Analyzed: 11/21/ Hydroxycarbofuran <0.31 ug/l Oxamyl <0.35 ug/l Carbofuran <0.43 ug/l Aldicarb <0.41 ug/l Aldicarb sulfone <0.25 ug/l Aldicarb sulfoxide <0.25 ug/l Carbaryl <0.31 ug/l Methomyl <0.49 ug/l Method: Date Analyzed: 11/18/ Prep Method: Date Prepared: 11/18/ ,2-Dibromo-3-Chloropropane < ug/l Ethylene Dibromide < ug/l Surrogate 1,2,3-Trichloropropane-(Surr) Surrogate 1,2,3-Trichloropropane-(Surr) 73 % 67 X % Acceptance Limits Acceptance Limits Page 6 of 17 11/30/2009

29 Ms. Janine Rader EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Job Number: Client Sample ID: Lab Sample ID: Well-O Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /13/ Water Analyte Result/Qualifier Unit MDL Dilution Method: 508 Date Analyzed: 11/20/ Prep Method: 508 Date Prepared: 11/16/ Aldrin < ug/l Chlordane (technical) <0.12 ug/l Endrin < ug/l gamma-bhc (Lindane) < ug/l Heptachlor < ug/l Heptachlor epoxide < ug/l Methoxychlor < ug/l Dieldrin < ug/l PCB-1016 <0.069 ug/l PCB-1221 <0.052 ug/l PCB-1232 <0.099 ug/l PCB-1242 <0.14 ug/l PCB-1248 <0.049 ug/l PCB-1254 <0.052 ug/l PCB-1260 <0.051 ug/l Toxaphene <0.059 ug/l Polychlorinated biphenyls, Total <0.045 ug/l Surrogate DCB Decachlorobiphenyl Tetrachloro-m-xylene Surrogate DCB Decachlorobiphenyl Tetrachloro-m-xylene 173 X % 101 % 165 X % 100 % Acceptance Limits Acceptance Limits Method: Date Analyzed: 11/24/ Prep Method: Date Prepared: 11/23/ ,4-D <0.037 ug/l Dalapon <1.0 ug/l Dinoseb <0.15 ug/l Pentachlorophenol <0.038 ug/l Picloram <0.077 ug/l Dicamba <0.085 ug/l Silvex (2,4,5-TP) <0.060 ug/l Surrogate 2,4-Dichlorophenylacetic acid Surrogate 2,4-Dichlorophenylacetic acid 103 % 72 % Acceptance Limits Acceptance Limits Page 7 of 17 11/30/2009

30 Ms. Janine Rader EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Job Number: Client Sample ID: Lab Sample ID: Well-O Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /13/ Water Analyte Result/Qualifier Unit RL Dilution Method: 300.1B Date Analyzed: 11/20/ Chlorite <20 ug/l Surrogate Dichloroacetic acid 109 % Acceptance Limits Page 8 of 17 11/30/2009

31 Ms. Janine Rader EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Job Number: Client Sample ID: Lab Sample ID: Well-P Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /13/ Water Analyte Result/Qualifier Unit MDL Dilution Method: Date Analyzed: 11/18/ Prep Method: Date Prepared: 11/16/ Alachlor <0.037 ug/l Atrazine <0.024 ug/l Benzo[a]pyrene <0.032 ug/l Bis(2-ethylhexyl) phthalate <0.67 ug/l Di(2-ethylhexyl)adipate <0.67 ug/l Hexachlorobenzene <0.046 ug/l Hexachlorocyclopentadiene <0.047 * ug/l Butachlor <0.036 ug/l Simazine <0.039 ug/l Metolachlor <0.022 ug/l Metribuzin <0.024 ug/l Propachlor <0.028 ug/l Surrogate Perylene-d12 78 % Acceptance Limits Method: 300.1B Date Analyzed: 11/21/ Bromate <2.6 ug/l Surrogate Dichloroacetic acid 95 % Acceptance Limits Method: Date Analyzed: 11/21/ Hydroxycarbofuran <0.31 ug/l Oxamyl <0.35 ug/l Carbofuran <0.43 ug/l Aldicarb <0.41 ug/l Aldicarb sulfone <0.25 ug/l Aldicarb sulfoxide <0.25 ug/l Carbaryl <0.31 ug/l Methomyl <0.49 ug/l Method: Date Analyzed: 11/18/ Prep Method: Date Prepared: 11/18/ ,2-Dibromo-3-Chloropropane < ug/l Ethylene Dibromide < ug/l Surrogate 1,2,3-Trichloropropane-(Surr) Surrogate 1,2,3-Trichloropropane-(Surr) 77 % 71 % Acceptance Limits Acceptance Limits Page 9 of 17 11/30/2009

32 Ms. Janine Rader EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Job Number: Client Sample ID: Lab Sample ID: Well-P Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /13/ Water Analyte Result/Qualifier Unit MDL Dilution Method: 508 Date Analyzed: 11/20/ Prep Method: 508 Date Prepared: 11/16/ Aldrin < ug/l Chlordane (technical) <0.11 ug/l Endrin < ug/l gamma-bhc (Lindane) < ug/l Heptachlor < ug/l Heptachlor epoxide < ug/l Methoxychlor < ug/l Dieldrin < ug/l PCB-1016 <0.065 ug/l PCB-1221 <0.049 ug/l PCB-1232 <0.094 ug/l PCB-1242 <0.13 ug/l PCB-1248 <0.047 ug/l PCB-1254 <0.049 ug/l PCB-1260 <0.048 ug/l Toxaphene <0.056 ug/l Polychlorinated biphenyls, Total <0.043 ug/l Surrogate DCB Decachlorobiphenyl Tetrachloro-m-xylene Surrogate DCB Decachlorobiphenyl Tetrachloro-m-xylene 101 p % 81 % 163 X % 64 X % Acceptance Limits Acceptance Limits Method: Date Analyzed: 11/24/ Prep Method: Date Prepared: 11/23/ ,4-D <0.037 ug/l Dalapon <0.99 ug/l Dinoseb <0.15 ug/l Pentachlorophenol <0.038 ug/l Picloram <0.076 ug/l Dicamba <0.084 ug/l Silvex (2,4,5-TP) <0.059 ug/l Surrogate 2,4-Dichlorophenylacetic acid Surrogate 2,4-Dichlorophenylacetic acid 91 % 75 % Acceptance Limits Acceptance Limits Page 10 of 17 11/30/2009

33 Ms. Janine Rader EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Job Number: Client Sample ID: Lab Sample ID: Well-P Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /13/ Water Analyte Result/Qualifier Unit RL Dilution Method: 300.1B Date Analyzed: 11/20/ Chlorite <20 ug/l Surrogate Dichloroacetic acid 97 % Acceptance Limits Page 11 of 17 11/30/2009

34 Ms. Janine Rader EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Job Number: Client Sample ID: Lab Sample ID: Well-DD Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /13/ Water Analyte Result/Qualifier Unit MDL Dilution Method: Date Analyzed: 11/18/ Prep Method: Date Prepared: 11/16/ Alachlor <0.034 ug/l Atrazine <0.022 ug/l Benzo[a]pyrene <0.030 ug/l Bis(2-ethylhexyl) phthalate <0.61 ug/l Di(2-ethylhexyl)adipate <0.61 ug/l Hexachlorobenzene <0.042 ug/l Hexachlorocyclopentadiene <0.043 * ug/l Butachlor <0.033 ug/l Simazine <0.036 ug/l Metolachlor <0.020 ug/l Metribuzin <0.022 ug/l Propachlor <0.026 ug/l Surrogate Perylene-d12 85 % Acceptance Limits Method: 300.1B Date Analyzed: 11/21/ Bromate <2.6 ug/l Surrogate Dichloroacetic acid 97 % Acceptance Limits Method: Date Analyzed: 11/21/ Hydroxycarbofuran <0.31 ug/l Oxamyl <0.35 ug/l Carbofuran <0.43 ug/l Aldicarb <0.41 ug/l Aldicarb sulfone <0.25 ug/l Aldicarb sulfoxide <0.25 ug/l Carbaryl <0.31 ug/l Methomyl <0.49 ug/l Method: Date Analyzed: 11/18/ Prep Method: Date Prepared: 11/18/ ,2-Dibromo-3-Chloropropane < ug/l Ethylene Dibromide < ug/l Surrogate 1,2,3-Trichloropropane-(Surr) Surrogate 1,2,3-Trichloropropane-(Surr) 84 % 83 % Acceptance Limits Acceptance Limits Page 12 of 17 11/30/2009

35 Ms. Janine Rader EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Job Number: Client Sample ID: Lab Sample ID: Well-DD Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /13/ Water Analyte Result/Qualifier Unit MDL Dilution Method: 508 Date Analyzed: 11/20/ Prep Method: 508 Date Prepared: 11/16/ Aldrin < ug/l Chlordane (technical) <0.11 ug/l Endrin < ug/l gamma-bhc (Lindane) < ug/l Heptachlor < ug/l Heptachlor epoxide < ug/l Methoxychlor < ug/l Dieldrin < ug/l PCB-1016 <0.065 ug/l PCB-1221 <0.049 ug/l PCB-1232 <0.093 ug/l PCB-1242 <0.13 ug/l PCB-1248 <0.047 ug/l PCB-1254 <0.049 ug/l PCB-1260 <0.048 ug/l Toxaphene <0.055 ug/l Polychlorinated biphenyls, Total <0.043 ug/l Surrogate DCB Decachlorobiphenyl Tetrachloro-m-xylene Surrogate DCB Decachlorobiphenyl Tetrachloro-m-xylene 110 % 79 % 106 % 78 % Acceptance Limits Acceptance Limits Method: Date Analyzed: 11/25/ Prep Method: Date Prepared: 11/23/ ,4-D <0.036 ug/l Dalapon <0.96 ug/l Dinoseb <0.14 ug/l Pentachlorophenol <0.037 ug/l Picloram <0.074 ug/l Dicamba <0.082 ug/l Silvex (2,4,5-TP) <0.058 ug/l Surrogate 2,4-Dichlorophenylacetic acid Surrogate 2,4-Dichlorophenylacetic acid 71 % 49 X % Acceptance Limits Acceptance Limits Page 13 of 17 11/30/2009

36 Ms. Janine Rader EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Job Number: Client Sample ID: Lab Sample ID: Well-DD Lost Lake Resort Date Sampled: Date Received: Client Matrix: 11/12/ /13/ Water Analyte Result/Qualifier Unit RL Dilution Method: 300.1B Date Analyzed: 11/20/ Chlorite <20 ug/l Surrogate Dichloroacetic acid 98 % Acceptance Limits Page 14 of 17 11/30/2009

37 DATA REPORTING QUALIFIERS Client: EnviroTest Laboratories Inc Job Number: Lab Section Qualifier Description GC/MS Semi VOA * LCS or LCSD exceeds the control limits GC Semi VOA p X The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported. Surrogate exceeds the control limits TestAmerica Savannah Page 15 of 17 11/30/2009

38 Page 16 of 17 11/30/2009

39 Login Sample Receipt Check List Client: EnviroTest Laboratories Inc Job Number: Login Number: Creator: Conner, Keaton List Number: 1 List Source: TestAmerica Savannah Question T / F/ NA Comment Radioactivity either was not measured or, if measured, is at or below background The cooler's custody seal, if present, is intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. There are no discrepancies between the sample IDs on the containers and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. If necessary, staff have been informed of any short hold time or quick TAT needs Multiphasic samples are not present. Samples do not require splitting or compositing. Is the Field Sampler's name present on COC? Sample Preservation Verified N/A N/A N/A N/A TestAmerica Savannah Page 17 of 17 11/30/2009

40 TestAmerica St. Louis Lot F9K F9K of F9K of 14

41 TestAmerica St. Louis Lot F9K F9K of F9K of 14

42 TestAmerica St. Louis Lot F9K F9K of F9K of 14

43 TestAmerica St. Louis Lot F9K F9K of F9K of 14

44 TestAmerica St. Louis Lot F9K F9K of F9K of 14

45 TestAmerica St. Louis Lot F9K F9K of F9K of 14

46 TestAmerica St. Louis Lot F9K F9K of F9K of 14

47 TestAmerica St. Louis Lot F9K F9K of F9K of 14

48 TestAmerica St. Louis Lot F9K F9K of F9K of 14

49 TestAmerica St. Louis Lot F9K F9K of F9K of 14

50 TestAmerica St. Louis Lot F9K F9K of F9K of 14

51 TestAmerica St. Louis Lot F9K F9K of F9K of 14

52 TestAmerica St. Louis Lot F9K F9K of F9K of 14

53 TestAmerica St. Louis Lot F9K F9K of F9K of 14

57 ANALYTICAL REPORT Job Number: Job Description: Tim Miller Associates, Inc. For: Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Attention: Ms. Maureen Fisher Debra Bayer Customer Service Manager 01/27/2010 The test results in this report meet all NELAP requirements unless specified within the case narrative. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory. EnviroTest Laboratories Inc. certifies that the analytical results contained herein apply only to the samples tested as received by our laboratory. All questions regarding this report should be directed to the EnviroTest Customer Service Representative. EnviroTest Laboratories, Inc. Certifications and Approvals: NELAP Accredited, NYSDOH 10142, NJDEP NY015, CTDOPH PH-0554, EPA NY Envirotest Laboratories, Inc. 315 Fullerton Avenue, Newburgh, NY Tel (845) Fax (845) Page 1 of 16 01/27/2010

58 Page 2 of 16 01/27/2010

59 METHOD SUMMARY Client: Tim Miller Associates, Inc. Description Matrix Water ICP Metals by Series Drinking Water Prep Determination Step Lab Location EnvTest EnvTest Job Number: Method Preparation Method EPA Rev 4.4 EPA 200 ICPMS Metals by Series Drinking Water Prep Determination Step EnvTest EnvTest EPA EPA 200 Apparent Color EnvTest SM B Mercury in Water by CVAA Digestion for CVAA Mercury in Waters EnvTest EnvTest EPA EPA Anions by Ion Chromatography EnvTest MCAWW Anions by Ion Chromatography EnvTest MCAWW Volatile Organic Compounds by Purge and Trap (Preserved) EnvTest EPA Turbidity Odor, Threshold Test Cyanide, Total: Colorimetric Method Cyanide: Distillation Membrane Filter Technique - Fecal Coliform Procedure Total Coliform and Escherichia coli by Colilert - Quantity Tray General Sub Contract Method Lab References: = EnvTest = EnviroTest EnvTest EnvTest EnvTest EnvTest EnvTest EnvTest SM20 SM 2130B SM20 SM 2150B SM18 SM 4500 CN E SM18 SM 4500 CN C SM18 SM 9222D SMWW SM 9223 Subcontract Method References: EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/ , March 1983 And Subsequent Revisions. SM18 = "Standard Methods For The Examination Of Water And Wastewater", 18th Edition, SM20 = "Standard Methods For The Examination Of Water And Wastewater", 20th Edition." SM21 = "Standard Methods For The Examination Of Water And Wastewater", 21st Edition SMWW = "Standard Methods for the Examination of Water and Wastewater" EnviroTest Laboratories, Inc. Page 3 of 16 01/27/2010

60 SAMPLE SUMMARY Client: Tim Miller Associates, Inc. Job Number: Lab Sample ID Client Sample ID Client Matrix Date/Time Sampled Date/Time Received Well-HH Lost Lake Resort Water 12/21/ /21/ EnviroTest Laboratories, Inc. Page 4 of 16 01/27/2010

61 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-HH Lost Lake Resort Date Sampled: Date Received: Client Matrix: 12/21/ /21/ Water Analyte Result/Qualifier Unit NONE NONE Dilution Method: 2120B Date Analyzed: 12/21/ Apparent Color 15 Color Units 1.0 Page 5 of 16 01/27/2010

62 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-HH Lost Lake Resort Date Sampled: Date Received: Client Matrix: 12/21/ /21/ Water Analyte Result/Qualifier Unit RL RL Dilution Method: Date Analyzed: 12/22/ ,1,1,2-Tetrachloroethane 0.50 U ug/l ,1,1-Trichloroethane 0.50 U ug/l ,1,2,2-Tetrachloroethane 0.50 U ug/l ,1,2-Trichloroethane 0.50 U ug/l ,1-Dichloroethane 0.50 U ug/l ,1-Dichloroethene 0.50 U ug/l ,1-Dichloropropene 0.50 U ug/l ,2,3-Trichlorobenzene 0.50 U ug/l ,2,3-Trichloropropane 0.50 U ug/l ,2,4-Trichlorobenzene 0.50 U ug/l ,2,4-Trimethylbenzene 0.50 U ug/l ,2-Dichloroethane 0.50 U ug/l ,2-Dichlorobenzene 0.50 U ug/l ,2-Dichloropropane 0.50 U ug/l ,3,5-Trimethylbenzene 0.50 U ug/l ,3-Dichlorobenzene 0.50 U ug/l ,3-Dichloropropane 0.50 U ug/l ,4-Dichlorobenzene 0.50 U ug/l ,2-Dichloropropane 0.50 U ug/l Benzene 0.50 U ug/l Bromobenzene 0.50 U ug/l Bromochloromethane 0.50 U ug/l Bromomethane 0.50 U ug/l n-butylbenzene 0.50 U ug/l cis-1,2-dichloroethene 0.50 U ug/l cis-1,3-dichloropropene 0.50 U ug/l Carbon tetrachloride 0.50 U ug/l Chlorobenzene 0.50 U ug/l Chloroethane 0.50 U ug/l Chloromethane 0.50 U ug/l Dibromomethane 0.50 U ug/l Dichlorodifluoromethane 0.50 U ug/l Ethylbenzene 0.50 U ug/l Hexachlorobutadiene 0.50 U ug/l Isopropylbenzene 0.50 U ug/l p-isopropyltoluene 0.50 U ug/l Methylene Chloride 1.0 U ug/l m-xylene & p-xylene 0.50 U ug/l Chlorotoluene 0.50 U ug/l o-xylene 0.50 U ug/l Page 6 of 16 01/27/2010

63 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-HH Lost Lake Resort Date Sampled: Date Received: Client Matrix: 12/21/ /21/ Water Analyte Result/Qualifier Unit RL RL Dilution Tetrachloroethene 0.50 U ug/l Chlorotoluene 0.50 U ug/l N-Propylbenzene 0.50 U ug/l sec-butylbenzene 0.50 U ug/l Styrene 0.50 U ug/l trans-1,2-dichloroethene 0.50 U ug/l trans-1,3-dichloropropene 0.50 U ug/l tert-butylbenzene 0.50 U ug/l Trichloroethene 0.50 U ug/l Trichlorofluoromethane 0.50 U ug/l Toluene 0.50 U ug/l Vinyl chloride 0.50 U ug/l Methyl tert-butyl ether 1.0 U ug/l Xylenes, Total 1.0 U ug/l Surrogate 4-Bromofluorobenzene (Surr) Dibromofluoromethane (Surr) 4-Bromofluorobenzene (HALL) 87 % 69 % 75 % Acceptance Limits Method: Rev 4.4 Date Analyzed: 01/05/ Prep Method: 200 Date Prepared: 12/24/ Ag 10 U ug/l Fe 60 U ug/l Mn 15 U ug/l Na 4500 ug/l Zn 41 ug/l Method: Date Analyzed: 12/30/ Prep Method: 200 Date Prepared: 12/24/ Pb 1.0 U ug/l As 1.4 U ug/l Be 0.30 U ug/l Cd 1.0 U ug/l Cr 1.0 U ug/l Cu 1.1 ug/l Ni 0.95 ug/l Sb 0.40 U ug/l Tl 0.30 U ug/l Ba 43 ug/l Se 2.0 U ^ ug/l Method: Date Analyzed: 12/29/ Page 7 of 16 01/27/2010

64 Ms. Maureen Fisher Tim Miller Associates, Inc. 10 North Street Cold Spring, NY Job Number: Client Sample ID: Lab Sample ID: Well-HH Lost Lake Resort Date Sampled: Date Received: Client Matrix: 12/21/ /21/ Water Analyte Result/Qualifier Unit RL RL Dilution Prep Method: Date Prepared: 12/28/ Hg 0.20 U ug/l Method: Date Analyzed: 12/21/ Nitrate as N mg/l Chloride 2.4 mg/l Nitrite as N U mg/l Sulfate 8.7 mg/l Fluoride 0.50 U mg/l Method: SM 2130B Date Analyzed: 12/21/ Turbidity 1.5 NTU Method: SM 2150B Date Analyzed: 12/21/ Odor 1.0 Units for Odor Method: SM 4500 CN E Date Analyzed: 12/28/ Prep Method: SM 4500 CN C Date Prepared: 12/28/ Cyanide, Total U mg/l Method: SM 9222D Date Analyzed: 12/21/ Coliform, Fecal 1.0 U CFU/100mL Method: SM 9223 Date Analyzed: 12/21/ Coliform, Total 1.0 U CFU/100mL Escherichia coli 1.0 U CFU/100mL Page 8 of 16 01/27/2010

65 DATA REPORTING QUALIFIERS Client: Tim Miller Associates, Inc. Job Number: Lab Section Qualifier Description GC VOA U The analyte was analyzed for but not detected at or above the stated limit. Metals ^ U ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA or MRL standard: Instrument related QC exceeds the control limits. The analyte was analyzed for but not detected at or above the stated limit. General Chemistry U The analyte was analyzed for but not detected at or above the stated limit. EnviroTest Laboratories, Inc. Page 9 of 16 01/27/2010

72 LOGIN SAMPLE RECEIPT CHECK LIST Client: Tim Miller Associates, Inc. Job Number: Login Number: Question T/F/NA Comment Radioactivity either was not measured or, if measured, is at or below background NA The cooler's custody seal, if present, is intact. NA The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. There are no discrepancies between the sample IDs on the containers and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. If necessary, staff have been informed of any short hold time or quick TAT needs Multiphasic samples are not present. Samples do not require splitting or compositing. EnviroTest Laboratories, Inc. Page 16 of 16 01/27/2010

ANALYTICAL REPORT Job Number: 680-53749-1 Job Description: 420-32173 For: EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY 12550 Attention: Ms.

73 ANALYTICAL REPORT Job Number: Job Description: For: EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Attention: Ms. Janine Rader Sheila Hoffman Project Manager I sheila.hoffman@testamericainc.com 01/08/2010 Approved for release. Sheila Hoffman Project Manager I 1/8/2010 3:00 PM cc: Debbie Bayer Ms. Renee Cusack Ms. Joyce Esposito Ms. Alicia Labare The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the person who signed this report. Savannah Certifications and ID #s: A2LA: ; AL: 41450; ARDEQ: ; ARDOH; CA: 03217CA; CO; CT: PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: ; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA DEQ: 30690; LA DHH: LA080008; ME: ; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV: GA00006; NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: ; PR: GA00006; RI: LAO00244; SC: ; TN: TN0296; TX: T ; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV DHHR: 9950 C; WI DNR: ; WY/EPAR8: 8TMS-Q TestAmerica Laboratories, Inc. TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA Tel (912) Fax (912) Page 1 of 12 01/08/2010

74 Job Narrative Comments No additional comments. Receipt All samples were received in good condition within temperature requirements. GC/MS Semi VOA Method(s) 525.2: The laboratory control sample (LCS) for batch exceeded control limits for the following nonregulated analytes: metribuzin. Method(s) 525.2: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch were outside control limits. No other analytical or quality issues were noted. HPLC No analytical or quality issues were noted. GC Semi VOA Method(s) 504.1: The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for preparation batch exceeded control limits for the following analytes:edb. Method(s) 508: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. No other analytical or quality issues were noted. General Chemistry No analytical or quality issues were noted. Page 2 of 12 01/08/2010

75 METHOD SUMMARY Client: EnviroTest Laboratories Inc Job Number: Description Lab Location Method Preparation Method Matrix Water Semivolatile Organic Compounds (GC/MS) TAL SAV EPA Extraction of Semivolatile Compounds TAL SAV EPA EDB, DBCP and 1,2,3-TCP (GC) TAL SAV EPA-DW Microextraction TAL SAV EPA-DW Chlorinated Pesticides & PCBs (GC) TAL SAV EPA 508 Liquid-Liquid Extraction (Separatory Funnel) TAL SAV EPA 508 Herbicides (GC) TAL SAV EPA Extraction of Chlorinated Acids TAL SAV EPA-DW Disinfection By-Products, (IC) TAL SAV EPA 300.1B Disinfection By-Products, (IC) TAL SAV EPA 300.1B Carbamate Pesticides (HPLC) TAL SAV EPA Lab References: TAL SAV = TestAmerica Savannah Method References: EPA = US Environmental Protection Agency EPA-01 = "Methods For The Determination Of Nonconventional Pesticides In Municipal And Industrial Wastewater", EPA/821/R/92/002, April EPA-DW = "Methods For The Determination Of Organic Compounds In Drinking Water", EPA/600/4-88/039, December 1988 And Its Supplements. TestAmerica Savannah Page 3 of 12 01/08/2010

76 METHOD / ANALYST SUMMARY Client: EnviroTest Laboratories Inc Job Number: Method Analyst Analyst ID EPA EPA 300.1B EPA EPA-DW EPA 508 EPA Davis, Nancy Brazell, Connie Brazell, Connie Meincke, Griffin Kellar, Joshua Kellar, Joshua ND CB CB GM JK JK TestAmerica Savannah Page 4 of 12 01/08/2010

77 SAMPLE SUMMARY Client: EnviroTest Laboratories Inc Job Number: Lab Sample ID Client Sample ID Client Matrix Date/Time Sampled Date/Time Received Well-HH Lost Lake Resort Drinking Water 12/21/ /22/ TestAmerica Savannah Page 5 of 12 01/08/2010

78 Ms. Janine Rader EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Job Number: Client Sample ID: Lab Sample ID: Well-HH Lost Lake Resort Date Sampled: Date Received: Client Matrix: 12/21/ /22/ Drinking Water Analyte Result/Qualifier Unit MDL Dilution Method: 300.1B Date Analyzed: 01/04/ Bromate <2.6 ug/l Surrogate Dichloroacetic acid 105 % Acceptance Limits Page 6 of 12 01/08/2010

79 Ms. Janine Rader EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Job Number: Client Sample ID: Lab Sample ID: Well-HH Lost Lake Resort Date Sampled: Date Received: Client Matrix: 12/21/ /22/ Drinking Water Analyte Result/Qualifier Unit RL Dilution Method: Date Analyzed: 12/30/ Prep Method: Date Prepared: 12/29/ Alachlor <0.20 ug/l Atrazine <0.20 ug/l Benzo[a]pyrene <0.20 ug/l Bis(2-ethylhexyl) phthalate <2.0 ug/l Bis(2-ethylhexyl) adipate <1.5 ug/l Hexachlorobenzene <0.20 ug/l Hexachlorocyclopentadiene <2.0 ug/l Butachlor <0.51 ug/l Simazine <0.51 ug/l Metolachlor <0.20 ug/l Metribuzin <0.20 * ug/l Propachlor <0.20 ug/l Surrogate Triphenylphosphate 2-Nitro-m-xylene Perylene-d12 99 % 90 % 103 % Acceptance Limits Method: 300.1B Date Analyzed: 12/24/ Chlorite <20 ug/l Surrogate Dichloroacetic acid 103 % Acceptance Limits Method: Date Analyzed: 12/30/ Hydroxycarbofuran <2.5 ug/l Oxamyl <2.5 ug/l Carbofuran <2.5 ug/l Aldicarb <2.5 ug/l Aldicarb sulfone <2.5 ug/l Aldicarb sulfoxide <2.5 ug/l Carbaryl <2.5 ug/l Methomyl <2.5 ug/l Method: Date Analyzed: 12/23/ Prep Method: Date Prepared: 12/23/ ,2-Dibromo-3-Chloropropane <0.020 ug/l Ethylene Dibromide <0.020 * ug/l Surrogate 1,2,3-Trichloropropane-(Surr) 114 % Acceptance Limits Page 7 of 12 01/08/2010

80 Ms. Janine Rader EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Job Number: Client Sample ID: Lab Sample ID: Well-HH Lost Lake Resort Date Sampled: Date Received: Client Matrix: 12/21/ /22/ Drinking Water Analyte Result/Qualifier Unit RL Dilution Surrogate 1,2,3-Trichloropropane-(Surr) 86 % Acceptance Limits Method: 508 Date Analyzed: 12/30/ Prep Method: 508 Date Prepared: 12/28/ Aldrin <0.024 ug/l Chlordane (technical) <0.24 ug/l Endrin <0.048 ug/l gamma-bhc (Lindane) <0.024 ug/l Heptachlor <0.024 ug/l Heptachlor epoxide <0.024 ug/l Methoxychlor <0.096 ug/l Dieldrin <0.048 ug/l PCB-1016 <0.48 ug/l PCB-1221 <0.48 ug/l PCB-1232 <0.48 ug/l PCB-1242 <0.48 ug/l PCB-1248 <0.48 ug/l PCB-1254 <0.48 ug/l PCB-1260 <0.48 ug/l Toxaphene <2.4 ug/l Polychlorinated biphenyls, Total <0.48 ug/l Surrogate DCB Decachlorobiphenyl Tetrachloro-m-xylene Surrogate DCB Decachlorobiphenyl Tetrachloro-m-xylene 128 % 122 % 88 % 96 % Acceptance Limits Acceptance Limits Method: Date Analyzed: 12/30/ Prep Method: Date Prepared: 12/29/ ,4-D <0.48 ug/l Dalapon <9.6 ug/l Dinoseb <2.9 ug/l Pentachlorophenol <0.96 ug/l Picloram <0.48 ug/l Dicamba <0.48 ug/l Silvex (2,4,5-TP) <0.48 ug/l Surrogate 2,4-Dichlorophenylacetic acid 87 % Acceptance Limits Page 8 of 12 01/08/2010

81 Ms. Janine Rader EnviroTest Laboratories Inc 315 Fullerton Avenue Newburgh, NY Job Number: Client Sample ID: Lab Sample ID: Well-HH Lost Lake Resort Date Sampled: Date Received: Client Matrix: 12/21/ /22/ Drinking Water Analyte Result/Qualifier Unit RL Dilution Surrogate Acceptance Limits 2,4-Dichlorophenylacetic acid 82 % Page 9 of 12 01/08/2010

82 DATA REPORTING QUALIFIERS Client: EnviroTest Laboratories Inc Job Number: Lab Section Qualifier Description GC/MS Semi VOA * LCS or LCSD exceeds the control limits GC Semi VOA * RPD of the LCS and LCSD exceeds the control limits TestAmerica Savannah Page 10 of 12 01/08/2010

83 Page 11 of 12 01/08/2010

84 Login Sample Receipt Check List Client: EnviroTest Laboratories Inc Job Number: Login Number: Creator: Conner, Keaton List Number: 1 List Source: TestAmerica Savannah Question T / F/ NA Comment Radioactivity either was not measured or, if measured, is at or below background The cooler's custody seal, if present, is intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. There are no discrepancies between the sample IDs on the containers and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. If necessary, staff have been informed of any short hold time or quick TAT needs Multiphasic samples are not present. Samples do not require splitting or compositing. Is the Field Sampler's name present on COC? Sample Preservation Verified N/A N/A N/A False TestAmerica Savannah Page 12 of 12 01/08/2010

85 TestAmerica St. Louis LOT# F9L of 13

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97 TestAmerica St. Louis LOT# F9L of 13

Contact: Rick Muir Phone Number: Company: Sagan LLC. Equipment. Pump

Page 1 of 7 Client Information Contact: Rick Muir Phone Number: 832-675-3088 Company: Sagan LLC. E-mail: rick@saganfilters.com Address: 11035 Technology Place Suite 100 San Diego, CA 92127 Test Sample