Pharmaceutical Technology
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1 Pharmaceutical Technology Course Coordinator and list of t eachers 1. name of the course : Pharmaceutical Technology 3 rd year 2. Lecturer. in charge : Tara Abdulrahman abdula 3. Dept. : Pharmaceutics 4. Contact : Address: Hawler Medical University College of pharmacy / Dept. and pharmaceutics tara_abd@yahoo.com Website link: 5. Participant lecturers : 1. Dr. raad gasgos 2. Shahla sadeq smael Course Overview - Pharmaceutical technology teaches the different dosage forms with respect to their raw materials, composition, and method of preparations, stability, storage and uses. In the practical part of this course the students will learn the different techniques used to prepare these dosage forms. Course Reading List: 1. Reference American pharmacy by sprowl 2. Remington, the science and practice of pharmacy, 1-2 vol. Syllabus: 1. Course title: pharmaceutical technology 3 rd year. 2. course number 101/ number of credits 6: 3hr theory 3hr practice / 4. Course Participants 3 rd year pharmaceutical students. 5. Instructors : - Tara Abdulrahman - Shahla Sadeq - Raad Gasgos 6. Course length 30 weeks (yearly program) 7. Teaching methods Theory (power point presentation) / practical (power point presentation) with student center learning (SCL) method. Assessment (grading): summative assessment: 1 st semester 20%: 2 nd semester 20%: Final exam: 60%: 1
2 Outline of course: Subject Lecturer No of hrs 1-1 st semester Tara abdulrahman 45 Dispersed system, classification, comparision Dr. raad gasgos 2 Solutions, types of solutions Dr. raad gasgos 2 Solubility, factor affecting, expression of dissolution, rate Dr. raad gasgos 4 versus solubility, preparation of solution containing non volatile materials Official solutions, classification, preparation and uses. Tara abdulrahman 4 Aqueous solutions containing aromatic principles, aromatic Tara abdulrahman 4 waters, methods of preparations, stability. Syrups, sugar based, artificial, sorbitol based, stability Tara abdulrahman 4 Clarification, methods, filter aids Tara abdulrahman 3 Solution using mixed solvent systems, spirits, elixirs Tara abdulrahman 3 Extraction, maceration, percolation Tara abdulrahman 3 Tinctures, fluid extracts, extracts, resins and oleoresins Tara abdulrahman 4 Colloidal dispersions, lyophilic, lyophobic, associations Raad gasgos 6 colloids Coarse dispersion, suspension Tara abdulrahman 6 Subject Lecturer No of hrs 2- Second semester 45 Emulsions, purpose of emulsification, *methods of Dr. raad gasgos 10 emulsification, emulsifying agents, HLB systems, stability Suppositories Tara abdulrahman 6 Lotions, Liniments, colloidons Tara abdulrahman 5 Powdered dosage forms Tara abdulrahman 10 Semisolid dosage forms Tara abdulrahman 10 Incompatibilities Dr. raad gasgos 4 Practical Syllabus 45 hrs. 1x3 / week. First semester Subjects Aromatic waters 3 Solutions 3 Spirits 3 Tinctures 3 Extracts 3 Syrups 3 Drops 3 Suspensions 3 Lotions 3 Liniments 3 Second semester Subjects 2 hours hours
3 Emulsions 6 Oinments 3 Creams 3 Capsules 3 Powder dosage forms 3 Tablets 3 Preparation involving sterilization 3 Preparation involving aspecting technique 3 Tooth preparations 3 Shampoo preparation 3 Student's Feedback on the Subject Date: Course: Year: Lecturer/tutor No. Evaluation Question 1 The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The material were prepared carefully as needed 4 The lecturer/tutor while lecturing tried to analyze the principles, contents and the important points of the subject simply and properly. 5 The lecturer/tutor while lecturing kept my attention. 6 The lecturer/tutor came into the classroom on time and was committed to the duration of the lecture. 7 The lecturer's behavior in the classroom was clam and respectful 8 The slides used in the lecturer were clear and attractive 9 At the end of the lecture, the lecturer gave the students a chance for question and comments. His/her answers were complete 10 The reading sources are new and compliable with the subject. Total of the level Subject's Level 1-5 Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good 3
4 Student's Feedback on the Subject Date: Course: Year: Lecturer/tutor N Evaluation Question o. 1 The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The material were prepared carefully as needed 4 The lecturer/tutor while lecturing tried to analyze the principles, contents and the important points of the subject simply and properly. 5 The lecturer/tutor while lecturing kept my attention. 6 The lecturer/tutor came into the classroom on time and was committed to the duration of the lecture. 7 The lecturer's behavior in the classroom was clam and respectful 8 The slides used in the lecturer were clear and attractive 9 At the end of the lecture, the lecturer gave the students a chance for question and comments. His/her answers were complete 1 The reading sources are new and compliable with the subject. 0 Total of the level Students to evaluate the level of the contents Poor Accept Medium Good Very good Student's Feedback on the Subject Date: Course: Year: Lecturer/tutor N Evaluation Question o. 1 The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The material were prepared carefully as needed 4 The lecturer/tutor while lecturing tried to analyze the principles, contents and the important points of the subject simply and properly. 5 The lecturer/tutor while lecturing kept my attention. 6 The lecturer/tutor came into the classroom on time and was committed to the duration of the lecture. 7 The lecturer's behavior in the classroom was clam and respectful 8 The slides used in the lecturer were clear and attractive 9 At the end of the lecture, the lecturer gave the students a chance for question and comments. His/her answers were complete 1 The reading sources are new and compliable with the subject. 0 Total of the level Subject's Level 1-5 Subject's Level 1-5 Subjective Remarks Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good 4
5 Examinations: - The exams will be held during the course. - Quizzes during the practical hours. - Theoretical exams: one per semester. - Practical exams: one or two per semester. - Final exam Theoretical, Practical. Theoretical: exams will be mixed - SCQ. (Single choices Questions) - Short Essays - Definition - Differentiation - True or false - Practical exam: - Short essay - Prescription - Preparations (practically) On Answering: the student should - read the question carefully - Think carefully before answering - Plan your answering - Answer should contain preface, content and conclusion - Answer should be precise and to the point Samples of the expected questions *SCQ sample - (A) Choose one most appropriate word or statement for the followings: - Which of the following is not a type of powder a. Lozenges b. Insufflations c. Dentifrices d. Douches - Short essays- sample - What is antagonism and synergism of drugs? Explain giving suitable examples. - Definition- sample - Define the following 1. solutions 2. Suspensions - Briefly differentiate between the followings - sample Deliquescence and efflorescence (Note: specify your answers in form of table which shows below). Deliquescence efflorescence True or false sample Answer the following by True or False -Suppositories are used to produce local, systemic and mechanical action. 5
6 Student's Feedback on the Course Date: Course: Year: Lecturer/tutor N Evaluation Question o. 1 The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The coordinator teacher had worked hard to cooperate and prepare the material 4 The coordinator teacher had worked hard to cooperate and prepare the course 5 The lecturer were carefully selected and were expert in their field 6 The coordinator teacher gave a good attention to the student's criticism and claim 7 Information on the Examination process was well provided 8 The questions of the exam were related to the content of the course 9 Total of the level 1 There is a potential to promote and develop the course in the following 0 areas: Subject's Level 1-5 Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good 6
7 Hawler Medical University College of Pharmacy Dept. of Pharmacognosy Course Book Pharmacognosy I and II, 3 rd year Course Coordinator: Dr. Alaadin M. Naqishbandi Lecturer 7
8 Pharmacognosy Course Coordinator and list of teachers 5. name of the course : Pharmacognosy I and II, 3 rd year 6. Lecturer. in charge : Dr. Alaadin M. Naqishbandi 7. Dept. : Pharmacognosy 8. Contact : Address: Hawler Medical University College of Pharmacy/ Dept. of pharmacognosy alaadinmn@hotmail.com Website link: 6. Participant lecturers : 1. Lana Yusef Mutaleb 2. Hazhar Muhamad 3. Shokhan uthman Course Overview The aim of pharmacognosy department is to provide a modern lecture courses covering a descriptive study of medicinal plants, the importance of plant- derived natural products in medicine & their biosyntheses. These courses include teaching the student the chemistry of natural products, how to identify & evaluate the active constituents of the plant, with emphasis on methods of extraction, separation of these constituents in a pure form using different type techniques, such as chromatography. In addition to the phytotherapy and information on herbal medicine used in the treatment of different diseases. Course Objectives At the end of this course, students are expected to: 1. Have a comprehensive knowledge of all the basic principles in Pharmacognosy. 2. Understand and classify the plants according to their source, morphology, active constituents and therapeutic uses. In addition, recognition of the methods used in natural product chemistry 3. Integrate their knowledge with data and information provided about certain species to expect the phytotherapeutic uses. 4. Understanding the methods in natural products chemistry which include extraction, identification and standardization. 5. Identify the most important families in the plant kingdom which yield the most important compounds and give examples on each one. 8
9 6. Transfer all the provided knowledge about taxonomy, morphology, extraction of natural compounds and different families in the plants kingdom into practical aspects in regard to their therapeutic uses. 7. Employ the theoretical information about the different analytical techniques used in the chemistry of natural compounds. 8. Accounting for use, and increasing interest in medicinal plants, and integrating them into national health care system. Promote the safety, efficacy, and quality of medicinal plants by expanding the knowledge base on regulatory and quality assurance standards. 9. Rationale usage of medicinal plants as drug categories in alternative medicine, their doses and dosage forms, drug-drug interactions, and drug-food interactions. 10. Exploitation of acquired knowledge about medicinal plants to the pharmaceutical industry including the search for pharmacokinetically optimum dosage formulations. Course Reading List: 1- trease & Evans pharmacognosy- 15 th ed. W.B sanders Edinburg London New York Philadilphia St Louis sydne tornto (2002) 2- pharmacognosy & pharmcobiotechnology by Ashutosh Kar, K.K. Gupta for new international Ltd (2003) 3- Pharmacognosy, 9 th ed. Tyler. Lea and Febiger, Philadilphia (1988) 4- Herbal medicine, 2 nd ed. Rudolf, Thieme (2000) 5- Fundamentals of Pharmacognosy and Phytotherapy, Michael Heinrich, Joanne Barnes, Simon Gibbons and Elizabeth M. Williamson (2004). Syllabus: 1. Course title: Pharmacognosy I, 3 rd year, 1 st course 2. number of credits (3) 2hr theory, 3hr practice 3- The course complies the following: The course comprises two main themes, the first is an introduction to pharmacognosy covering drugs of natural origin. This includes history and importance of natural products, Botanical characters of medicinal plants and study the different cell contents; Natural health products as herbal medicines, homeopathy, complementary and alternative medicine and related subjects; Production of natural product derived drugs including their collection, preparation, storage conditions and their preparation for use either in the crude form or as extracts. The second part of the course covers chromatographic principles and methodologies specially column and planer chromatography as well as their applications in evaluation of natural products. Also the course will introduce the students to the active constituents of drugs containing: Carbohydrates, Tannins, Volatile oils, lipids and unorganized drugs. 9
10 4- Course Participants: 3 rd year pharmacy students, 1 st course. 5- Instructors : - Dr. Alaadin M. Naqishbandi - Lana Yusef Mutaleb - Hazhar Muhamad 6- Course length 15 weeks 30 hr theory (15 X 2 hr), 45hr practice (15 X 3 hr) 7- Teaching methods Theory (power point presentation) practical (practical experiments, seminars) 8- Assessment (grading): summative assessment: Midterm exam (theory subjects): 25% Practical assessment 15%: Final exam: 60% (50% theoretical subjects, 10% practical subjects) Outline of course: A-Theoretical Syllabus Subject Lecturer No of hrs General introduction-the scope of pharmacognosy Dr. Alaadin Naqishbandi 1 Complementary and alternative medicine 1 Production of crude drug-cultivation, collection, 2 drying and storage Authentication and adulteration of crude drugs 1 Evaluation of crude drugs 2 Extraction of the plant material 2 Chromatographic separation techniques 12 Screening, regulations, and quality control of herbal drugs 1 Carbohyrates 2 Volatile oils 4 Tannins 1 Lipids 1 B-Practical Syllabus 1- Microscopical evaluation of crude drugs (starch, calcium oxalate crystals) 2- Microscopical evaluation of crude drugs (Epidermis, epidermal trichomes) 3- Extraction methods 4- Ascending paper chromatography 5- Thin layer chromatography (effect of activity of adsorbent on Rf value) 6- Thin layer chromatography(effect of solvent polarity on Rf value) 7- Thin layer chromatography (two dimentional chromatography) 8- -Column chromatography (separation of dye mixture) 9- Carbohydrates (extraction and identification of starch, identification tests of carbohydrates) 10- Extraction and identification of tannins 10
11 Syllabus: 1. Course title: Pharmacognosy II, 3 rd year, 2 nd course 2. number of credits (3) 2hr theory, 3hr practice 3- The course complies the following: The course deals with the chemistry of crude drugs (Phytochemistry). Emphasis will be given to the study of bioactive constituents including glycosides and alkaloids. The study deals with their isolation, identification, structure activity relationship (SAR), medicinal uses and determination of these constituents, using chromatographic and spectroscopic methods. 4- Course Participants: 3 rd year pharmacy students, 2 nd course. 5- Instructors : - Dr. Alaadin M. Naqishbandi - Lana Yusef Mutaleb - Hazhar Muhamad 6- Course length 15 weeks 30 hr theory (15 X 2 hr), 45hr practice (15 X 3 hr) 4. Teaching methods Theory (power point presentation) practical (practical experiments, seminars) 5. Assessment (grading): summative assessment: Midterm exam (theory subjects): 25% Practical assessment 15%: Final exam: 60% (50% theoretical subjects, 10% practical subjects) 11
12 Outline of course: A-Theoretical Syllabus Subject Lecturer No of hrs Glycosides physical and chemical properties Dr. Alaadin Naqishbandi 1 Cardiac glycosides 3 Saponin glycosides Anthraquinone glycosides 3 Flavonoid glycosides Cyanogenetic glycosides 1 Isothiocyanate glycosides Alcohol glycosides 3 Phenol glycosides Lactone glycoside Alkaloids, physical and chemical properties 2 Pyridine-piperidine alkaloids 2 Tropane alkaloids 3 Quinoline alkaloids 1 Isoquinoline alkaloids 4 Imidazol alkaloids 1 Indole alkaloids 4 Purine bases 1 Alkaloidal amines 1 B-Practical Syllabus 1- Extraction and identification of cardioactive glycosides 2- Extraction and identification of saponin glycosides 3- Extraction and identification of anthraquinone glycosides 4- Extraction and identification of flavonoid glycosides 5- Extraction and identification of Pyridine-piperidine alkaloids Extraction and identification of tropane alkaloids 6- Extraction and identification of Indole alkaloids 7- Extraction and identification of Purine alkaloids. 8- Seminars prepared and presented by groups of students related to medicinal plants. 12
13 Student's Feedback on the Subject Date: Course: Year: Lecturer/tutor No. Evaluation Question Subject's Level The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The material were prepared carefully as needed 4 The lecturer/tutor while lecturing tried to analyze the principles, contents and the important points of the subject simply and properly. 5 The lecturer/tutor while lecturing kept my attention. 6 The lecturer/tutor came into the classroom on time and was committed to the duration of the lecture. 7 The lecturer's behavior in the classroom was clam and respectful 8 The slides used in the lecturer were clear and attractive 9 At the end of the lecture, the lecturer gave the students a chance for question and comments. His/her answers were complete 10 The reading sources are new and compliable with the subject. Total of the level Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good Student's Feedback on the Subject Date: Course: Year: Lecturer/tutor Evaluation Question N o. 1 The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The material were prepared carefully as needed 4 The lecturer/tutor while lecturing tried to analyze the principles, contents and the important points of the subject simply and properly. 5 The lecturer/tutor while lecturing kept my attention. 6 The lecturer/tutor came into the classroom on time and was committed to the duration of the lecture. 7 The lecturer's behavior in the classroom was clam and respectful 8 The slides used in the lecturer were clear and attractive 9 At the end of the lecture, the lecturer gave the students a chance for question and comments. His/her answers were complete 1 0 The reading sources are new and compliable with the subject. Total of the level Subject's Level 1-5 Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good 13
14 Student's Feedback on the Subject Date: Course: Year: Lecturer/tutor No. Evaluation Question 1 The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The material were prepared carefully as needed 4 The lecturer/tutor while lecturing tried to analyze the principles, contents and the important points of the subject simply and properly. 5 The lecturer/tutor while lecturing kept my attention. 6 The lecturer/tutor came into the classroom on time and was committed to the duration of the lecture. 7 The lecturer's behavior in the classroom was clam and respectful 8 The slides used in the lecturer were clear and attractive 9 At the end of the lecture, the lecturer gave the students a chance for question and comments. His/her answers were complete 10 The reading sources are new and compliable with the subject. Total of the level Subject's Level 1-5 Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good Examinations: - The exams will be held during the course. - Quizzes during the practical hours. - Theoretical exams: midterm and final exam. - Final exam Theoretical, Practical and Oral. Theoretical: exams will be mixed - MCQ. (Multiple choices questions) - SCQ. (Single choices Questions) - Short Essays - Diagrams - T and F statement selection Practical exam: - Written exam on practical subjects - Seminar presentation exam: will be held through a committee On Answering: the student should - read the question carefully - Think carefully before answering - Plan for answering - Answer should contain preface, content and conclusion - Answer should be precise and to the point 14
15 Samples of the expected questions and their answers: *T and F statement selection 1- Ginkgo biloba leaves contains aescin a saponin active constituents. * Short Essays Summarize the advantages of using herbal drugs. *MCQ sample: 1- Strychnine is a a- CNS stimulant belongs to indole alkaloids b- obtained from the bark of Erythroxylum plant c- obtained from the seeds of a beautiful palm that is cultivated in India, Asia and East Africa. d- Is an indole alkaloid with antidepressant activity Student's Feedback on the Course Date: Course: Year: Lecturer/tutor No. Evaluation Question Subject's Level The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The coordinator teacher had worked hard to cooperate and prepare the material 4 The coordinator teacher had worked hard to cooperate and prepare the course 5 The lecturer were carefully selected and were expert in their field 6 The coordinator teacher gave a good attention to the student's criticism and claim 7 Information on the Examination process was well provided 8 The questions of the exam were related to the content of the course 9 There is a potential to promote and develop the course in the following areas: 10 Total of the level Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good 15
16 Medicinal Chemistry Course Coordinator and list of teachers 1. Name of the course : Medicinal Chemistry 3 rd year 2. Lecturer in charge: Dana Muhammad H. A. Jaf 3. Department: Pharmaceutical Chemistry 4. Contact : Address: Hawler Medical University College of Pharmacy / Dept. of Pharmaceutical Chemistry dana_pharma@yahoo.com danapharm@hotmail.com Website link: 5. Participant lecturers : Dr. Shahla Jihad Ahmad Course Overview First, this course will present a review of those principles of inorganic chemistry those apply to medicine and/ or pharmaceutical chemistry. The first chapter atomic and molecular structure is devoted to the explanation of atomic structures as it relates to bonding forces and complexation, the other chapter represent detailed discussion of those inorganic agents used as pharmaceutical aids and necessities or as therapeutic and diagnostic agents. Secondly, it will give an understanding of the mechanism of drug action at molecular level, stimulate the interest in understanding the role of medicinal chemistry in the discovery and development of synthetic therapeutic agents, and study the effect of physicochemical properties and drug biotransformation on drug action and therefore cam compare the rational drug design with the classical drug design. 16
17 In addition this course is designed to incorporate a number of experiments for the identification of certain drugs which are included in the theoretical course of inorganic and organic pharmaceutical chemistry. The experiments are intended to train the undergraduate pharmacy students to use different chemical reactions and various analytical methods for preparation and assay of some representative drugs of different classes and also to meet the students need for a concise skill on practical analytical pharmaceutical chemistry. Course Objectives 1. Describe those products including: buffers, antioxidants, fluid electrolytes, topical agents, biochemically important ions and therapy-ethically important ions as antacids, cathartics, antidote and radiopharmaceuticals both as diagnostic and therapeutic agents. 2. Relates the following physicochemical properties on drug action: a. Partition coefficient b. Acid base properties 3. Explain the theories that have evolved to account for the mechanism of drug action and the type of force involved. 4. Drug distribution after different dosage forms. 5. The theoretical aspects and mechanisms of drug biotransformation and its effect on drug action 6. Course Reading List: 1. Text Book Wilson and Gisvold's Organic Medicinal and Pharmaceutical Chemistry, edited by Delgado and W. A. Remer's, 11 th edition (2004). 2. Reference Medicinal Chemistry by Ashutosh Kar 3. Introduction to medicinal chemistry by Alex Gringauz 4. Inorganic Medicinal and Pharmaceutical Chemistry by Block, Roche, Soine, and Wilson 17
18 Syllabus: 1. Course title: Medicinal Chemistry 3 rd year 2. Number of credits 8: 3hr theory 3hr practice (2 semester = 30 weeks) The course complies the following: Atomic and molecular structure/ complexation: Electrolytes: - Major extra and intra cellular electrolytes - Electrolyte replacement therapy - Essential and trace ions - Non essential ions - Acid-base imbalance Dental Products - Fluoride supplements - Inorganic substances included in toothpaste GIT Agents - Antacids - Protective and adsorbents - Official saline cathartics Radiopharmaceuticals and contrast media - Radiopharmaceutical agents - Contrast media Topical Agents - Deodorant - Antiseptic - Disinfectant - Antifungal Physicochemical properties in relation to biological action - Complex of events between drug administration and drug action - Sites of loss - Sites of action - Drug-receptor interactions - The drug receptor - The Drug-receptor interaction and subsequent events - Rational drug design - Selected physicochemical properties Metabolism - General pathways of drug metabolism and sites of drug biotransformation 18
19 - Role of cytochrome P-450 monooxygenases in oxidative biotransformation - Oxidative reactions - Reductive reactions - Hydrolytic reactions - Conjugation reactions - Factors affecting drug metabolism Drug stability - Chemical stability - Physical stability Assessment (grading): summative assessment: First semester: 20% Second semester: 20% Final exam: 60% Outline of course: Subject Lecturer No. of hrs 1- Electrolytes: Dana Muhammad 11 Major extra and intra cellular electrolytes 2 Electrolyte replacement therapy 2 Essential and trace ions 3 Non essential ions 2 Acid-base imbalance 2 Subject Lecturer No. of hrs 2- Dental Products: Dana Muhammad 2 Fluoride supplements 1 Inorganic substances included in toothpaste 1 Subject Lecturer No. of hrs 3- G.I.T Agents: Dana Muhammad 4 Antacids 2 Protective and adsorbents 1 Official saline cathartics 1 Subject Lecturer No. of hrs 4- Radiopharmaceuticals and contrast media: Dana Muhammad 6 19
20 Radiopharmaceutical agents 4 Contrast media 2 Subject Lecturer No. of hrs 6- Topical Agents: Dana Muhammad 15 Disinfectant 4 Antiseptic 4 Antifungal 6 Deodorant 1 Subject Lecturer No. of hrs 5- Physicochemical properties in relation to biological Dana Muhammad 27 action: Complex of events between drug administration and drug 3 action Sites of loss 2 Sites of action 2 The drug receptor 5 Drug-receptor interactions 2 The Drug-receptor interaction and subsequent events 3 Rational drug design 2 Selected physicochemical properties 8 Subject Lecturer No. of hrs 8- Drug stability: Dana Muhammad 4 Chemical stability 2 Physical stability 2 Subject Lecturer No. of hrs 8- Atomic and molecular structure/ Dr. Shahla Jihad 6 complexation: Complexes and chelating agents 2 Acids and bases 2 Oxidation-reduction reactions 2 20
21 Practical Syllabus 90 hr. 3 hr / week 1- Introduction 3 2- Analytical Methods 3 3-Preparation and standardization of 1 N hydrochloric acid 3 4- Preparation and standardization of 1 N sodium hydroxide 3 5- Assay of sodium hydroxide solution 3 6- Assay of sodium benzoate solution 3 7- Assay of sodium salicylate solution 3 8- Assay of borax 3 9- Assay of citric acid Assay of ammoniated mercury Preparation and standardization of 0.1 N potassium permanganate Assay of hydrogen peroxide solution Preparation and standardization of 0.1 N sodium thiosulfate Assay of copper sulfate Assay of chlorinated lime in bleaching powder Preparation and assay of aqueous iodine solution Assay of ferric ammonium citrate Assay of ferrous gluconate tablets Assay of ferrous fumarate tablets Assay of ferric ion by iodometric method Assay of magnesium sulfate Assay of alum Assay of sodium lactate injection Determination of % w/v of total chloride by Volhard's method Determination of % w/v of calcium chloride by complexometric titration Assay of ascorbic acid Assay of fluoride ion in toothpaste Assay of magnesium sulfate injection Assay of lactate in Ringer solution Assay of methylparaben 3 21
22 Student's Feedback on the Subject Date: Course: Year: Lecturer/tutor No Evaluation Question. 1 The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The material were prepared carefully as needed 4 The lecturer/tutor while lecturing tried to analyze the principles, contents and the important points of the subject simply and properly. 5 The lecturer/tutor while lecturing kept my attention. 6 The lecturer/tutor came into the classroom on time and was committed to the duration of the lecture. 7 The lecturer's behavior in the classroom was clam and respectful 8 The slides used in the lecturer were clear and attractive 9 At the end of the lecture, the lecturer gave the students a chance for question and comments. His/her answers were complete 10 The reading sources are new and compliable with the subject. Total of the level Subject's Level 1-5 Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good Student's Feedback on the Subject Date: Course: Year: Lecturer/tutor No. Evaluation Question Subject's Level The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The material were prepared carefully as needed 4 The lecturer/tutor while lecturing tried to analyze the principles, contents and the important points of the subject simply and properly. 5 The lecturer/tutor while lecturing kept my attention. 6 The lecturer/tutor came into the classroom on time and was committed to the duration of the lecture. 7 The lecturer's behavior in the classroom was clam and respectful 8 The slides used in the lecturer were clear and attractive 9 At the end of the lecture, the lecturer gave the students a chance for question and comments. His/her answers were complete 10 The reading sources are new and compliable with the subject. Total of the level Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good 22
23 Student's Feedback on the Subject Date: Course: Year: Lecturer/tutor Evaluation Question N o. 1 The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The material were prepared carefully as needed 4 The lecturer/tutor while lecturing tried to analyze the principles, contents and the important points of the subject simply and properly. 5 The lecturer/tutor while lecturing kept my attention. 6 The lecturer/tutor came into the classroom on time and was committed to the duration of the lecture. 7 The lecturer's behavior in the classroom was clam and respectful 8 The slides used in the lecturer were clear and attractive 9 At the end of the lecture, the lecturer gave the students a chance for question and comments. His/her answers were complete 10 The reading sources are new and compliable with the subject. Total of the level Subject's Level 1-5 Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good Examinations: - The exams will be held during the course. - Quizzes during the practical hours. - Theoretical exams: one per semester. - Practical exams: one or two per semester. - Final exam Theoretical, Practical and Oral. Theoretical: exams will be mixed - MCQ. (Multiple choices questions) - SCQ. (Single choices Questions) - Short Essays - Diagrams Practical exam: - Practical related Questions - Theoretical related Questions - Assay of unknown drug 23
24 - Identification of unknown drug On Answering: the student should - Read the question carefully - Think carefully before answering - Plan your answering - Answer should contain preface, content and conclusion - Answer should be precise and to the point Samples of the expected questions and their answers: *MCQ sample: In the Becket hypothesis (for proper binding): - (T) a Tertiary nitrogen is required. - (T) b Central carbon is essential. - (T) c Phenyl ring attached to central carbon is needed. - (F) d The central carbon should be far from tertiary nitrogen by three carbon atom *SCQ sample - All of the following are factors affecting drug metabolism except: A Age B Sex C Food D Strain - Short essays Give a the ideal properties of preservative 24
25 Student's Feedback on the Course Date: Course: Year: Lecturer/tutor No. Evaluation Question 1 The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The coordinator teacher had worked hard to cooperate and prepare the material 4 The coordinator teacher had worked hard to cooperate and prepare the course 5 The lecturer were carefully selected and were expert in their field 6 The coordinator teacher gave a good attention to the student's criticism and claim 7 Information on the Examination process was well provided 8 The questions of the exam were related to the content of the course 9 Total of the level 10 There is a potential to promote and develop the course in the following areas: Subject's Level 1-5 Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good 25
26 Biochemistry Course Coordinator and list of teachers 1. name of the course : Biochemistry 3 rd year 2. Lecturer. in charge : Dr. Showan D. Husain 3. Dept. : Clinical Analysis 4. Contact : Address: Hawler Medical University College of Pharmacy / Dept. Clinical Analysis showand_2000@yahoo.com Website link: 5. Participant lecturers : a - Dr.Sanna Ghadhban b- Dr.Shatha Rouf c- Dr.Basima Sadiq d- Course Overview: To understand the main concept of human biochemisty that is relevant to pharmaceutical sciences Course Objectives : At the end of this course the student should be able to: a. Understand the principle of biochemistry by studing the biochemistry of carbohydrate,protein,hormones,enzymes & lipids. b. Understand the storage and expression of genetic information. Syllabus: 6. Course title: Biochemistry 3 rd year. 7. Theoritical Biochemistry,Credit hours = 3 hours 8. Practical Biochemistry,Credit hour = 1 hour First Course Introduction to biochemistry 1- Biochemistry of carbohydrate / Six hours / Dr. Showan - Definition - Biomedical importance - Isomerism & their types - Carbohydrate chemistry - Classification - Monosaccharides&their chemical reaction - Trioses - Tetroses - Pentoses 26
27 - Hexoses - Pyranose &Furanose structures - Mutarotation - Formation of O- Glycosidic linkage & N glycosidic linkage - Disaccharides - Physical Properties - Structure - Reducing properties - Sucrose &its synthesis - Maltose &its synthesis - Lactose & its synthesis - Polysaccharides - Homopolysaccharides - Hetropolysaccharides - Glycogen - Starch (amylose &amylopectin) - Dextran - Cellulose - Carbohydrate Derivatives - Amino Sugar - Glycosugar - Mucopolysaccharides a- Proteoglycan b- Hepatin c- Chondriotin Sulphate d- Keratin Sulphate e- Dermatin Sulphate II. Protein / Six hours / Dr. Shatha - Primary structure of protein - Secondary structure of protein - Tertiary structure of protein - Quaternary structure of protein - Biomedical Importance III. Amino Acid & peptides structure / six hours / Dr. Shatha - Biomedical Importance - Classification of amino acids - Physical properties - Reactions of amino acid - Biological active amines - Zwitterr ion - Isoelectric point - Peptide Structure - Medical importance - Glutathion - Chemotactic peptides - Analgesic peptides - Cyclic peptides - Toxic peptides IV. Lipids physiology & Biochemistry / five hours /Dr. Showan 27
28 - Biomedical Importance - General properties &classification - Fats & oils - Waxes - Phospholipids - Glycolipids - Prostaglandins - Steroids - Lipid peroxidation - Antioxidants V.Nucleotides / three hours / Dr. Sanna - Nucleosides & Nucleotides - Nucleic acid (DNA,RNA) Structure & Function VI.Storage & Expression of Genetic Information / six hours/ Dr. Sanna - The Genetic code - Transcription & translation mechanism - Mitation - Protein biosynthesis VII.Enzymes: / six hours / Dr. Basima - Properties - Activators & Inhibitors - Mode of enzyme action - Apoenzyme &Co enzyme - Nomenclature - Classification - Role of metal in enzyme activity Second Course I. Effect of hormones on body tissue eight hours / Dr. Shatha - Endocrine gland - Classification of Hormones - Types of messengers ( mode of action) - Physiological factors effect on hormone secretion - Growth Hormone - Glucocorticoid - Insulin - Androgen - Estrogen - Thyroxin II. carbohydrate Metabolism / eight hours / Dr. Showan - Digestion & Absorption - Glycolysis &the Oxidation of Pyruvate - Citric acid cycle - Electron Tranport Chain 28
29 - Gluconeogenesis - Pentose Mono Phosphate Shunt - Glycogen metabolism - Interconversion of carbohydrate to lipid and protein metabolism III. Protein Metabolism / six hours / Dr.sanna - Digestion & Absorption of protein - General metabolism of nitrogen - Fate of absorbed of amino acid - Fate of the amino removed - Role of liver in protein metabolim - Urea Formation - Fate of carbon skeleton IV. Lipid Metabolism / six hours / Dr.Showan - Digestion & absorption - Metabolism of plasma lipoproteins - Metabolism of free fatty acids - Metabolism - cholesterol - Ketone bodies V. Nucleotide Metabolism / three hours /Dr.sanna - Purine & Pyrimidin metabolism - Uric acid excretion VI. Vitamins / six hours / Dr.Basima - Classification - Fat soluble vitamin - water soluble vitamin VII. Metabolism of creatine / three hours/ Dr. Basima - Chemistry,synthesis,function,fate &excretion - Creatin metabolism VIII. Metabolism of Heme / six hours/ Dr.Basima - Biochemistry of Heme - Synthesis Assessment (grading): summative assessment: 1 st semester 20%: 2 nd semester 20%: Final exam: 60% Text book and references: - Lippincotts Illustrated Reviews : Biochemistry by Richard A. Harvey, Pamela C. and Denise R. Ferrier.4 th edition Chemistry for the health Sciences by George I sackheim and Dennis D. Lehman 8 th edition - Harper Biochemistery by D.W. Martin,P.A. Mayes V.W. Rodwell 29
30 Practical Syllabus. Week Subject 1 st - General reaction of carbohydrates effects of acid & heat - Effect of strong acid and heat 2 nd - Effects of alkali and heat on carbohydrates - Iodine test 3 rd - Identification of unknown carbohydrates 4 th - Color reaction of proteins 5 th - Color reaction of proteins 6 th - Lipids - Solubility of lipids in different solution - presence of fats and oils in solution 7 th - Lipids - Preparation of soap - Salting out of the soap - Formation of insoluble soap - Saturated and unsaturated fatty acid 8 th General reaction of carbohydrate II Effect of weak acid &heat 9 th Fermentation reaction 10 th Osazon reaction 11 th Precipitation of proteins PH Concentration of neutral salts 12 th - Dielectic constant of solvent - Alkaloidal agent. - Heat 13 th -Enzymes - Catalase,Acid phosphatase and Urase 14 th - Factors effect on enzymatic activity - Temperature 15 th - Concentration of enzyme - Subcellular location of enzyme 16 th - Nucleic acids - Alkaline phosphatase 17 th - Acid phosphatase 18 th - Vitamin. -Vitamin C 19 th - Final examination 30
31 Student's Feedback on the Subject Date: Course: Year: Lecturer/tutor No. Evaluation Question Subject's Level The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The material were prepared carefully as needed 4 The lecturer/tutor while lecturing tried to analyze the principles, contents and the important points of the subject simply and properly. 5 The lecturer/tutor while lecturing kept my attention. 6 The lecturer/tutor came into the classroom on time and was committed to the duration of the lecture. 7 The lecturer's behavior in the classroom was clam and respectful 8 The slides used in the lecturer were clear and attractive 9 At the end of the lecture, the lecturer gave the students a chance for question and comments. His/her answers were complete 10 The reading sources are new and compliable with the subject. Total of the level Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good Student's Feedback on the Subject Date: Course: Year: Lecturer/tutor N Evaluation Question o. 1 The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The material were prepared carefully as needed 4 The lecturer/tutor while lecturing tried to analyze the principles, contents and the important points of the subject simply and properly. 5 The lecturer/tutor while lecturing kept my attention. 6 The lecturer/tutor came into the classroom on time and was committed to the duration of the lecture. 7 The lecturer's behavior in the classroom was clam and respectful 8 The slides used in the lecturer were clear and attractive 9 At the end of the lecture, the lecturer gave the students a chance for question and comments. His/her answers were complete 10 The reading sources are new and compliable with the subject. Total of the level Subject's Level 1-5 Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good 31
32 Student's Feedback on the Subject Date: Course: Year: Lecturer/tutor N Evaluation Question o. 1 The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The material were prepared carefully as needed 4 The lecturer/tutor while lecturing tried to analyze the principles, contents and the important points of the subject simply and properly. 5 The lecturer/tutor while lecturing kept my attention. 6 The lecturer/tutor came into the classroom on time and was committed to the duration of the lecture. 7 The lecturer's behavior in the classroom was clam and respectful 8 The slides used in the lecturer were clear and attractive 9 At the end of the lecture, the lecturer gave the students a chance for question and comments. His/her answers were complete 10 The reading sources are new and compliable with the subject. Total of the level Subject's Level 1-5 Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good Examinations: - The exams will be held during the course. - Quizzes during the practical hours. - Theoretical exams: one per semester. - Practical exams: one or two per semester. - Final exam Theoretical, Practical and Oral. Theoretical: exams will be mixed - MCQ. (Multiple choices questions) - SCQ. (Single choices Questions) - Short Assays 32
33 Student's Feedback on the Course Date: Course: Year: Lecturer/tutor N Evaluation Question o. 1 The objectives and key massages of the subject were clear 2 The contents of the subject of the were useful and related to the main objects of the course 3 The coordinator teacher had worked hard to cooperate and prepare the material 4 The coordinator teacher had worked hard to cooperate and prepare the course 5 The lecturer were carefully selected and were expert in their field 6 The coordinator teacher gave a good attention to the student's criticism and claim 7 Information on the Examination process was well provided 8 The questions of the exam were related to the content of the course 9 Total of the level 1 There is a potential to promote and develop the course in the following 0 areas: Subject's Level 1-5 Subjective Remarks Students to evaluate the level of the contents Poor Accept Medium Good Very good 33
34 Hawler Medical University College of Pharmacy Depretment of Pharmacology and Toxicology Course Book Pharmacology 3 rd Year Pharmacology Course Coordinator and list of Teachers 1. Name of the course: Pharmacology 3 rd year 2. Lecture in charge: Dr. Mohamad Sherwan + Dr.Taghrid Al-Taei 3. Department: Pharmacology and Toxicology 4. Contact: Hawler Medical University Collage of Pharmacy Department of Pharmacology and Toxicology sherwan-10@hotmil, tagreedaltaei@yahoo.com Website link: 5. Participant lecturers: a. Dr. Muhamad Sherwan b. Dr. Taghrid Al-Taei c. MSc. Muhammad Abdulla d. MSc. Sazan Dakhil e. MSc. Feras Majid Adwar f. BSc. Maysoon Abdulwahab Course Overview The develop an understanding of basic knowledge in drug and the pharmacological bases of drug classes to enable students to practice the proper, effective and safe use of drug. Course Objective the students should be able define different pharmacological terms and activities of drug in biological system and demonstrate the mechanism behind the drug action, the processes which occur during movement of drug through body compartments. In addition emphases is directed towards the study of activity of drug in different physiological system of the body, this done on molecular, cellular and tissue levels to illustrate the role of these drugs in corrections of different pathophysiological condition. At the end of the course the student should have learned all the individual drugs, thei Pharmacology 3 rd r indications, contraindications, side effects, interactions, toxicities. etc. Course Reading List 1. Goodman and Gilman: The pharmacological Basis of Therapeutic, 10 th Ed., Joel G. Hardman and Lee E. limited, 2003, McGraw-Hill. 2. Clinical Pharmacology, 9 th Ed., D. R. Laurence, P. N. Bennett and M. J. Brown, 2002, Clinical Living Stone. 34
35 Syllabus 1. Course title: Pharmacology 3 rd year. 2. 3hr. theory and 3hr. practice. The course complies the following: Introduction: Pharmacodynamic, pharmacokinetic. Pharmacology of Autonomic nervous system. Chemotherapy of infection. Antibacteral drug. Course Participants: 3 rd year pharmacy students. Instructors: Dr. Muhamad Sherwan Dr. Nedal Abdulkader M. Muslih A. Ibrahim Course length 30 weeks (yearly program) Outline of Course Subject Lecturer No. of hrs. General principles of pharmacology A. Historical review and definitions in pharmacology B. Pharmacodynamics General principles of drug action Classification of receptors Quantitative aspects of drug-receptor interation Agonists (full, partial and inverse) Antagonists Desensitisation and tachyphylaxis Pharmacokinetics: A. Absorption and distribution of drugs Movement of drug molecules across cell barriers Binding of drugs to plasma proteins Partition into body fat and other tissues Routes of drug administration Drug disposition B. Drug Metabolism and Elimination Phase I reaction Enzyme induction and inhibition Phase II reaction First pass effect Half life time Renal excretion of drugs Biliary excretion and enterohepatic circulation Pharmacology of Autonomic Nervous System Introduction Transmitters and co-transmitters in the autonomic nervous system General principles of neurotransmission 35 Dr. Needal 6 Dr. Needal 6 Dr. Sherwan M. Muslih 15
36 Physiological role of noradrenergic transmission Noradrenaline synthesis, storage, re-uptake and metabolism Adrenoceptors and their classification Drugs acting on noradrenergic transmission A. Sympathomimetices 1. directly acting (catecholamine and adrenergic) 2. indirectly acting B. Sympatholytics 1. adrenoceptors antagonists (α and β) 2. other affecting synthesis, release and uptake of noradrenaline. Physiological role of cholinergic transmission. Acetylcholine synthesis and release. Muscarinic and nicotinic receptors Drugs acting on cholinergic transmission A. parathympathomimetics 1. muscarinic agonists 2. anticholineesterases (reversible and irreversible) B. muscarinic receptors antagonists Drugs affecting ganglia A. ganglionic stimulants B. ganglionic blocking drugs Neuromuscular Blooking Drugs A. non-depolarising competieive blocking drugs B. depolarising blocking drugs Chemotherapy of Infections A. biochemical basis of chemotherapy B. biochemical reaction as potential targets (cell wall synthesis, protein synthesis, nucleic acid synthesis..) C. resistance to antibiotics D. biochemical mechanisms to antibiotics Antibacterial Drugs A. beta-lactam antibiotics (penicillin, cephalosprin and cephamycins, other beta-lactam antibiotics) B. anti-microbial agents affecting bacterial protein synthesis (tetracyclins, chloramphinicol, aminoglycosides, macrolides, lincosamides, fucidic acid) C. anti-microbials which interfere with the synthesis or action of folate (sulphonamides and trimethoprim). D. anti-microbial agents affecting topoisomerase II (fluoroquinolones). E. anti-mycobacterial agents (drug used for treatment of TB and drug used to treat leprosy). F. miscellaneous antibacterial agents (glycopeptide antibiotics, polymixin antibiotics, metronidazole, nitrofurantoin Anti-fungal drugs A. antifungal antibiotics (amphotericin, nystatin, grisofulvin) 36 Dr. Needal 6 Dr. Needal 9 Dr. Sherwan 3
37 B. synthetic antifungal agents (azoles, terbinafine, naftifine) Reference Books: A. Goodman and Gilman: The pharmacological Basis of Therapeutic, 10th Ed., Joel G. Hardman and Lee E. limited, 2003, McGraw-Hill. B. Clinical Pharmacology, 9th Ed., D. R. Laurence, P. N. Bennett and M. J. Brown, 2002, Clinical Living Stone. Teaching methods- Theory (power point presentation) / practical (experiments) Assessment (grading): summative assessment. 1st semester 20% 2nd semester 20% Final exam 60% 37
38 Hawler Medical University College of Pharmacy Department of Clinical Analysis Course Book Pathology 3 rd year Students Course Coordinator: Dr. Maysoon Al-Haideri Pathology Course description: Pathology is regarded as a backbone for medical science; it acts as a bridge between preclinical and clinical cases. Pathology is essential for the diagnosis of diseases, modern therapeutics, and the formulation of prognosis and restoration of health. This Pathology course will apply knowledge of normal anatomy and physiology to promote a clear understanding of disease processes. It introduces the student to the common body responses and manifestations of disease that result from imbalance in homeostasis of the body. The course will address common well-defined alterations involving: cell injury, necrosis, inflammation, wound healing, and neoplasia. These concepts are applied in a systems-oriented approach to disease processes affecting musculoskeletal, cardiopulmonary, renal, nervous, gastrointestinal, immune, hematological and endocrine systems. The aim of the course is to teach students the pathogenesis of various symptoms and diseases affecting the human body. Altered, physiological functions of human organs are explained. By the end of the course, students should be able to understand the relation between the symptoms and the disease, which might be helpful in differential diagnosis. At the end of each lecture and laboratory session we give the students questions and divide them into groups then we discuss the questions. 38
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