Specifications of 999 Prime Quality Fish Meal

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2 Specifications of 999 Prime Quality Fish Meal 999 Prime Quality fish meal is made of fresh, but unspecified fish, as a wholemeal. 999 Prime Quality fish meal is especially intended for mixed feed for poultry and pigs. For early-weaned piglets, mink, aquaculture as well as pets we recommend our special fish meals. Please, study the specifications of our special»999«fish meals: LT and Con-Kix. Sales conditions: Crude protein : Basis 70% /72%/ 74%/ 76% Crude fat : Max. 14% (acid hydrolysis) = 12% soxhlet Moisture : Max. 10%, min. 4% Chlorides (salt) : Max. 3% as NaCl Antioxidant : ppm ethoxyquin added Normal content Packings: 50 kg bags (gross for net), minimum 10 tonnes per delivery. Big-bags (gross for net), minimum 10 tonnes per delivery. Pellets, bulk Meal, bulk Remarks: Bags are in combination with the internal 999 code on the side of the bags, marked differently according to sales basis of crude protein: P74 for basis 74% and P76 for basis 76%, no marking means basis 70% /72%. Our internal and external microbiological control, secures that the meal is in accordance with the EU-directive for fish meal. (Salmonellae not proved; Entero < 300/g) HSO

3 Typical Analyses of 999 Prime Quality Fish Meal No. of Average Minimum Maximum Standard samples Deviation Crude Protein, % 44 71,3 64,8 75,5 2,0 Moisture, % 43 7,7 5,3 10,3 1,1 Crude Fat, %*) 45 9,3 5,7 14,0 1,7 Salt, % 22 2,1 1,4 3,2 0,6 Ash, % 45 12,9 10,0 16,8 1,4 TVN mg N/100g ,3 Ttitration value ml 0,1 N NaOH/10 g dry matter , ,8 All analyses are carried out by Eurofins Laboratorium. *) Soxhlet, diethylether extract. Biogenic Amine Analyses of 999 Prime Quality Fish Meal Biogenic Amines No. of Average Minimum Maximum Standard ppm samples Deviation Tyramine Putrescine Cadaverine Histamine The samples have been analysed at the Eurofins Steins Laboratorium HSO

4 Amino Acid Analyses of 999 Prime Quality Fish Meal g Amino Acid pr 16g N sample No. of samples Average Minimum Maximum Standard Deviation Lysine 30 7,7 6,8 9,4 0,66 Methionine 30 2,8 2,6 3,1 0,12 Cystine 30 0,9 0,6 1,1 0,12 Threonine 30 4,1 3,5 4,5 0,23 Tryptophan 25 1,1 1,1 1,3 0,05 Isoleucine 30 4,3 3,8 4,9 0,27 Leucine 30 7,2 6,7 7,8 0,24 Histidine 30 2,3 1,8 2,8 0,22 Phenylalanine 30 3,8 3,2 4,1 0,17 Tyrosine 30 2,8 1,4 3,7 0,56 Valine 30 5,1 4,5 5,5 0,27 Aspartic acid 30 9,1 8,3 10,0 0,41 Serine 30 3,9 2,8 4,5 0,46 Glutamic acid 30 13,4 12,1 15,5 0,78 Proline 30 3,7 3,0 4,4 0,26 Glycine 30 5,9 5,2 7,2 0,50 Alanine 30 6,1 5,6 6,9 0,27 Ornithine 30 0,1 0,0 0,2 0,05 Arginine 30 5,6 5,0 6,3 0,36 Hydroxyproline 25 0,5 0,4 1,0 0,15 The samples have been analysed at Eurofins Steins laboratory, method used: ISO HSO

5 Specifications of 999 LT Fish Meal 999 LT is a wholemeal made of absolutely fresh fish. This ensures a specifically low level of biogenic amines. 999 LT is produced under very mild conditions. This includes gentle evaporation and low temperature vacuum drying. The protein digestibility of 999 LT is determined by biological tests with mink. 999 LT is especially suited for all aquaculture species and early-weaned piglets. 999 LT can also be used for young animals of other species. Guarantees: Crude protein : Min. 70% Crude fat : Max. 13,5% (acid hydrolysis) = 11,5% soxhlet Moisture : Max. 10%, min. 6% True Protein Digestibility : Min. 90% determined with mink Chlorides (salt) : Max. 3% as NaCl Ash : Max. 14% TVN : Max. 0.18% NH3-N Water soluble protein : Min. 18%, max. 32% Cadaverine : Max ppm Histamine : Max. 150 ppm Antioxidant : 150 ppm ethoxyquin is added both before and after drying Quality of raw material : TVN max. 50 mg N/100g at entrance to cooker Salmonellae : Not proved Packings: 50 kg bags (gross for net), minimum 10 tonnes per delivery. Big-bags (gross for net), minimum 10 tonnes per delivery. Meal, bulk Remarks: Our internal and external microbiological control, secures that the meal is in accordance with the EU-directive for fish meal. (Salmonellae not proved; Entero < 300/g) HSO

6 Typical Analyses of 999 LT Fish Meal No. of Average Minimum Maximum Standard Samples Deviation Mink digestibility, % 51 91,1 90,0 93,1 0,80 Crude Protein, % 51 72,7 70,3 74,9 0,91 Moisture, % 51 7,7 6,3 9,3 0,65 Ash, % 51 11,8 9,0 14,0 1,21 Crude Fat, % *) 51 9,2 7,6 11,5 0,78 Salt, % 51 1,7 0,8 2,8 0,47 TVN, % as NH3-N 51 0,15 0,12 0,19 0,01 Water Soluble Protein, % 51 22,1 18,6 29 2,38 Cadaverine, ppm Histamine, ppm Putrescine, ppm Particle size > ,19 0,1 0,8 0,16 Particle size > ,66 0,3 4,6 0,89 All analyses are carried out by NOFIMA, Norway. Average over the last 5 years. *) Soxhlet, diethylether extract. Amino Acid Analyses of 999 LT Fish Meal g Amino Acid pr 16g N sample No. of samples Average Minimum Maximum Standard Deviation Lysine 26 8,1 7,1 11,2 0,81 Methionine 26 3,0 2,7 3,5 0,17 Cystine 26 1,0 0,7 1,1 0,12 Threonine 26 4,3 3,7 4,7 0,20 Tryptophan 26 1,2 0,6 1,3 0,19 Isoleucine 26 4,6 4,0 5,3 0,31 Leucine 26 7,5 6,9 8,4 0,32 Histidine 26 2,4 2,0 3,4 0,33 Phenylalanine 26 4,0 3,7 4,5 0,20 Tyrosine 26 3,1 1,4 3,7 0,54 Valine 26 5,4 4,7 7,5 0,54 Aspartic acid 26 9,5 8,5 11,3 0,52 Serine 26 4,2 3,3 4,7 0,36 Glutamic acid 26 13,6 12,1 17,4 0,98 Proline 26 3,8 3,5 4,2 0,18 Glycine 26 5,7 5,3 7,1 0,40 Alanine 26 6,0 5,7 7,1 0,30 Ornithine 26 0,1 0,0 0,1 0,04 Arginine 26 5,8 5,5 6,7 0,26 Hydroxyproline 23 0,5 0,3 0,8 0,18 The samples have been analysed at Eurofins Steins laboratory, method used: ISO HSO

7 Specifications of 999 Con-Kix Fish Meal 999 Con-Kix is a wholemeal made of absolutely fresh fish. This ensures a specifically low level of biogenic amines. 999 Con-Kix is produced under very mild and gentle conditions at low temperature. The total process time is merely 15 minutes and the drying takes place in an air-dryer within few seconds. 999 Con-Kix has a very high biological value, and the protein digestibility of Con-Kix is determined by biological tests with mink. 999 Con-Kix is especially suited for very young animals where the health of the animal is in focus. 999 Con-Kix is recommended for fingerlings, smolts, and pre-starters. Guarantees: Crude protein : Min. 70% Crude fat : Max. 13,5% (acid hydrolysis) = 11,5% soxhlet Moisture : Max. 10%, min. 6% True Protein Digestibility : Min. 92% determined with mink Chlorides (salt) : Max. 2.5% as NaCl Ash : Max. 14% TVN : Max. 0.18% NH3-N Water soluble protein : Min. 18%, max. 32% Cadaverine : Max ppm Histamine : Max. 300 ppm Antioxidant : 150 ppm ethoxyquin is added both before and after drying Quality of raw material : TVN max. 45 mg N/100g at entrance to cooker Salmonellae : Not proved Packings: Big-bags (gross for net), minimum 10 tonnes per delivery. Meal, bulk Remarks: Our internal and external microbiological control, secures that the meal is in accordance with the EU-directive for fish meal. (Salmonellae not proved; Entero < 300/g) HSO

8 Typical Analyses of 999 Con-Kix Fish Meal No. of Average Minimum Maximum Standard Samples Deviation Mink digestibility, % 37 94,0 92,2 95,4 0,66 Crude Protein, % 37 72,7 70,7 75,5 0,86 Moisture, % 37 8,6 6,7 9,9 0,68 Ash, % 37 12,1 10,1 14,7 1,30 Crude Fat, % *) 37 7,6 5,5 9,7 1,29 Salt, % 37 1,5 0,8 2,3 0,44 TVN, % as NH3-N 37 0,14 0,12 0,16 0,01 Water Soluble Protein, % 37 21,5 18,0 27,7 2,22 Cadaverine, ppm Histamine, ppm Putrescine, ppm Particle size > ,14 0,1 0,8 0,14 Particle size > ,69 0,3 5,2 1,26 All analyses are carried out by NOFIMA, Norway. *) Soxhlet, diethylether extract. Amino Acid Analyses of 999 Con-Kix Fish Meal g Amino Acid pr 16g N sample No. of samples Average Minimum Maximum Standard Deviation Lysine 18 8,4 7,7 9,8 0,59 Methionine 18 3,0 2,8 3,3 0,11 Cystine 18 1,0 0,7 1,2 0,15 Threonine 18 4,2 3,9 4,5 0,17 Tryptophan 18 1,2 0,7 1,4 0,20 Isoleucine 18 4,6 4,0 5,0 0,25 Leucine 18 7,5 7,1 7,9 0,20 Histidine 18 2,6 2,3 3,1 0,24 Phenylalanine 18 4,0 3,8 4,1 0,10 Tyrosine 18 3,2 1,6 3,7 0,59 Valine 18 5,3 4,7 5,7 0,25 Aspartic acid 18 9,6 9,2 10,4 0,33 Serine 18 4,1 3,2 4,8 0,40 Glutamic acid 18 13,6 12,7 14,8 0,63 Proline 18 3,8 3,1 4,4 0,31 Glycine 18 5,8 5,2 6,6 0,39 Alanine 18 6,1 5,8 6,5 0,18 Ornithine 18 0,1 0,0 0,1 0,04 Arginine 18 5,8 5,3 6,3 0,24 Hydroxyproline 15 0,6 0,0 0,9 0,22 The samples have been analysed at Eurofins Steins laboratory, method used: ISO HSO

9 Average Amino Acid Analyses of 999 Fish Meal g/16g N Prime Quality LT Con-Kix Lysine 7,7 8,1 8,4 Methionine 2,8 3,0 3,0 Cystine 0,9 1,0 1,0 Threonine 4,1 4,3 4,2 Tryptophan 1,1 1,2 1,2 Isoleucine 4,3 4,6 4,6 Leucine 7,2 7,5 7,5 Histidine 2,3 2,4 2,6 Phenylalanine 3,8 4,0 4,0 Tyrosine 2,8 3,1 3,2 Valine 5,1 5,4 5,3 Aspartic acid 9,1 9,5 9,6 Serine 3,9 4,2 4,1 Glutamic acid 13,4 13,6 13,6 Proline 3,7 3,8 3,8 Glycine 5,9 5,7 5,8 Alanine 6,1 6,0 6,1 Ornithine 0,1 0,1 0,1 Arginine 5,6 5,8 5,8 Hydroxyproline 0,5 0,5 0,6 The samples have been analysed at Eurofins Steins laboratory, method used: ISO HSO

10 % % X<0,25 Average particle size of 999 fish meal Accumulated 58% Individual screens 11% 7% 1,2% 0,1% 0,25<X<0,5 0,5<X<0,8 0,8<X<1,18 1,18<X<2,36 2,36<X Screen size, mm HSO

11 Mineral Analyses of 999 Fish Meal* Ash & Minerals No. of Average Minimum Maximum Standard in dry matter samples Deviation Moisture, % 115 7,3 3,8 10,5 1,2 Ash, % 78 13,4 10,5 17,8 1,7 Calcium (Ca), g/kg 24 27,9 19,0 40,0 6,4 Phosphorous (P), g/kg 36 22,1 19,0 25,4 1,5 Magnesium (Mg), g/kg 30 2,1 1,8 2,4 0,2 Sodium (Na), g/kg 23 9,6 5,8 14,1 2,1 Potassium (K), g/kg 19 16,4 9,2 19,8 2,5 Iron (Fe), mg/kg ,1 110,0 670,0 89,6 Manganese (Mn), 20 12,6 7,9 22,4 3,5 mg/kg Cupper (Cu), mg/kg 20 4,2 3,0 5,7 0,7 Zink (Zn), mg/kg ,7 64,0 146,0 25,4 Selenium (Se), mg/kg 25 2,5 1,0 4,0 0,9 Aluminium (Al), mg/kg 19 81,8 26, ,7 * The mineral analyses are representative for all the 999 Fish Meals HSO

12 Undesirable substances in 999 fishmeal TripleNine Fish Protein is screening the content of undesireable substances as defined by EU, in our products. Each year 10 samples of fishmeal and 5 samples of fishoils are analysed. Besides the below mentioned substances, TripleNine Fish Protein is following the content of dioxins and dioxinlike PCB s, to assure, that no product leaving our factory exceeds the EU limits. Substance Unit Number of analyses Average Max. Min. Level of quantification EU limit Arsenic mg/kg 87 6,4 13 1,3 25 Flour mg/kg Nitrit mg/kg 32 2,03 8,00 0,10 30 Lead mg/kg 80 0,32 6,31 0,03 10 Chromium mg/kg 20 1,3 0,42 1,60 Cadmium mg/kg 80 0,15 0,90 0,03 2 Mercury mg/kg 86 0,08 0,27 0,01 0,5 Aldrin ng/g 43 2,7 5,0 0,004 5 sum Dieldrin ng/g 43 3,5 5,0 0,09 5 0,01 Toxaphen 26 ng/g 43 1,4 4,8 0,04 Lod=20 50 ng/g 43 2,0 20 0,03 Lod=20 sum 62 ng/g 43 3,1 5,6 0,09 Lod=20 20 Sum ng/g 42 5,7 15 0,2 Chlordan Gamma/trans ng/g 43 2,7 5 0,03 5 Alpha/cis ng/g 43 2,9 5 0,06 5 sum Oxi ng/g 43 2,7 5 0, Sum ng/g 43 8,4 15 0,1 15 DDD O,p ng/g 43 2,6 5 0,06 5 P,p ng/g 43 2,2 5 0,23 5 DDE O,p ng/g 43 2,7 5 0,02 5 sum P,p ng/g 43 4,0 11 0, DDT O,p ng/g 43 2,7 5 0,03 5 P,p ng/g 43 2,3 5 0,06 5 DDD+DDT+DDE Sum ng/g 47 16,5 30 1,5 30 Endosulfan Alfa ng/g 43 2,7 5 0,10 5 Beta ng/g 43 3,2 5 0,70 5 sum Sulfate ng/g 43 2,8 5 0, Sum ng/g 43 8,7 15 0,9 15 Endrin ng/g 43 2,7 5 0, Heptachlor ng/g 43 2,7 5 0, HCB ng/g 43 3,1 5 0, HCH Alfa ng/g 43 2,7 5 0, Beta ng/g 43 2,7 5 0, Gamma/lindan ng/g 43 5,8 10 0, Chloramphenicol μg/kg 13 Nd LOD=0, HSO

13 Specifications of 999 Fish Oil 999 Fish Oil is crude oil made of fresh raw material. The fish oil is in general customer tailor-made, i.e. 999 Fish Oil is produced and delivered according to the customer s individual demand. 999 Fish Oil is used for feed production and technical usages. Guarantees: Guarantees are determined in the individual contract. In general 999 Fish Oil will be within the values shown below: Free Fatty Acids : 3-7 % Iodine Value : Unsaponifiable matter : 2 6 % Moisture & Impurities : < 1% Further we are willing to discuss the content of the individual fatty acids peroxide, anisidine values and dioxin levels lower than the EU regulation. Antioxidants can be added according to customers demands, but normally ethoxyquin or BHT is added. Packings: 200 litre new metal drums, minimum 10 tonnes per delivery litre new bulk container, minimum 10 tonnes per delivery. bulk: 20 container, truck and ship HSO

14 Vitamin Analyses of 999 Fish Meal and Fishoil* Vitamines in 999 fishoil Vitamin A Vitamin D3 Vitamin E IU/kg IU/kg mg/kg average max min std dev number Vitamines in 999 fish meal Vitamin A Vitamin D3 Vitamin E Vitamin B1 Vitamin B2 B6 B12 IU/kg IU/kg mg/kg mg/kg mg/kg mg/kg μg/kg average max ,24 13,4 7, min ,59 0,1 1 1,58 83 std dev number * The vitamin analyses are representative for all the 999 Fish Meals and fishoils HSO

15 Undesirable substances in 999 fishoil TripleNine Fish Protein is screening the content of undesireable substances as defined by EU, in our products. Each year 10 samples of fishmeal and 5 samples of fishoils are analysed. Besides the below mentioned substances, TripleNine Fish Protein is following the content of dioxins and dioxinlike PCB s, to assure, that no product leaving our factory exceeds the EU limits. Substance Unit Number of analyses Average Max. Min. Level of quantification Arsenic mg/kg 67 7,4 11 5,1 0,03 15 Lead mg/kg 44 0,06 0,1 0,02 0,05 10 Cadmium mg/kg 44 0,01 0,05 0,01 0,01 2 Mercury mg/kg 44 0,01 0,02 0,005 0,005 0,5 Aldrin ng/g 37 3,1 5 0,02 5 sum Dieldrin ng/g , ng/g 37 5,8 19 2,0 5 Toxaphen 50 ng/g 37 8,4 33 3,0 5 sum 62 ng/g 37 3,6 18 0, Gamma/trans ng/g 30 2,7 5 0,5 5 Chlordan Alpha/cis ng/g 30 6,2 15 2,4 5 sum Oxi ng/g 30 2,8 6 1, DDD O,p ng/g 37 4,9 38 1,1 3 P,p ng/g 37 22,9 61 5,0 5 DDE O,p ng/g 37 4,3 19 0,5 5 P,p ng/g 37 54, ,0 5 sum DDT O,p ng/g 37 5,0 11 1, P,p ng/g 37 12,6 31 4,2 5 DDD+DDT+DDE ng/g Alfa ng/g 30 3,0 5 0,2 5 Endosulfan Beta ng/g 30 5,1 16 2,0 5 sum Sulfate ng/g 30 3,7 5 0, Endrin ng/g 30 3,2 5 0, Heptachlor ng/g 30 3,1 10 0, HCB ng/g 30 11,6 22 5, Alfa ng/g 30 3,2 6 1, HCH Beta ng/g 30 5,5 20 1, Gamma/lindan ng/g 30 5,1 10 1, EU limit HSO

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