Column: Alltech Prevail Carbohydrate ES, 5µm, 250 x 4.6mm. Mono-, Di-, Tri- Saccharides

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1 Carbohydrates Corn Syrup Oligomers. Dextrose. Maltose. Maltotriose. Maltotetraose. Maltopentaose. Maltohexaose. Maltoheptaose. Maltooctaose Column: Alltech Prevail Carbohydrate ES, µm, x mm Rocket (Part No. 0) Gradient: Time: 0 %B: 0 Flow Rate:.0mL/min 0 Corn Syrup Solids. Dextrose. Maltose. Maltotriose. Maltotetraose. Maltopentaose. Maltohexaose. Maltoheptaose. Maltooctaose. Maltononaose 0. Maltodecaose. Maltoundecaose. Maltododecaose. Maltotridecaose Column: Alltech Prevail Carbohydrate ES, µm, 0 x.mm (Part No. 0) Gradient: Time: 0 %B: 0 Flow Rate:.0mL/min 0 Mono-, Di-, Tri- Saccharides 0. iso-erythritol. Fructose. Sorbitol. Mannitol. Glucose. Inositol. Sucrose. Maltitol. Maltose Raffinose. DP. DP. DP. DP. DP. DP. DP. DP0. DP 0. DP. DP. DP Sugars. Fructose. Glucose. Sucrose Min. Column: Alltech Prevail Carbohydrate ES, µm, 0 x.mm (Part No. 0) Mobile Phase: A: Acetonitrile B: 0.0% Ammonium Hydroxide in Water Gradient: Time: %B: Flow Rate:.0mL/min Beer Standards Unmodified Mobile Phase. Fructose. Glucose. Sucrose. Maltose. Maltotriose. Maltotetraose. Maltopentaose 0 Min. Column: Alltech Prevail Carbohydrate ES, µm, x mm Rocket (Part No. 0) Mobile Phase: Acetonitrile:Water (:) Flow Rate:.0mL/min Column Temp: 0 C Beer Standards Modified Mobile Phase 0 0. Fructose. Glucose. Sucrose. Maltose. Maltotriose. Maltotetraose. Maltopentaose Column: Alltech Prevail Carbohydrate ES, 0 x.mm (Part No. 0) Gradient: Time: 0 0 %B: 0 Flow Rate:.0mL/min Column: Alltech Prevail Carbohydrate ES, 0 x.mm (Part No. 0) Mobile Phase: A: Acetonitrile:Acetone (:) B: Water Gradient: Time: 0 %B: 0 Flow Rate:.0mL/min more applications View our complete searchable chromatogram database at ww.discoverysciences.com

2 Carbohydrates Sugar Alcohols Column: Alltech Prevail Carbohydrate ES, 0 x.mm (Part No. 0) Mobile Phase: Acetonitrile:Water (0:0) Flow Rate:.0mL/min. iso-erythritol. Xylitol. Mannitol. Maltitol Wine Analysis Sipaska Rosé. Fructose. Sorbitol. Glucose. Maltose Min. Column: Alltech Prevail Carbohydrate ES, µm, 0 x.mm (Part No. 0) Gradient: Time: 0 0 %B: Flow Rate:.0mL/min Imported Ale. Fructose. Glucose. Maltose. Maltotriose. Maltopentaose. Maltohexaose. Maltoheptaose Beverage Additives. Ascorbic Acid. Saccharin. Benzoic Acid. Aspartame. Vanillin Column: Alltech Prevail Carbohydrate ES, µm, 0 x.mm (Part No. 0) Gradient: Time: 0 0 %B: 0 Flow Rate:.0mL/min 0 Min. Column: Alltech Prevail C, µm, 0 x.mm (Part No. ) Mobile Phase: Acetonitrile:0.0M Ammonium Acetate, ph., (0:0) Flow Rate: 0.mL/min Detector: UV at 0 Wine Analysis by Ion Exclusion Partial Digest: Complex Polysaccharide from Plant Cell Wall 0. Citric Acid. Tartaric Acid. Glucose. Malic Acid. Fructose. Acetic Acid. Glycerol. Lactic Acid. Methanol 0. Ethanol Min. Column: Alltech IOA-000, mm, 00 x.mm (Part No. ) Mobile Phase: 0.00N Sulfuric Acid Flow Rate: 0.mL/min Column Temp: 0 C Detector: RI Column: Gradient: Flow Rate: Detector: Vydac C, µm, 0 x.mm (Part No. TP) to 0% Methanol over 0 min., then to % Methanol at 0 min.0ml/min ELSD 0

3 Conquistador Tequila 0 0 Min.. Fructose. Mannitol. Glucose. Sucrose. Unknown 0 Column: Alltech Prevail Carbohydrate ES, µm, 0 x.mm (Part No. 0) Mobile Phase: Acetonitrile:Water (:) Flow Rate:.0mL/min Splenda Sweetener Min.. Sucralose. Glucose. Maltose. Maltodextrins 0 Column: Alltech Prevail Carbohydrate ES, µm, 0 x.mm (Part No. 0) Gradient: Time: 0 0 %B: Flow Rate:.0mL/min Pepsi One Cola. Sucralose. Unknown. Fructose. Glucose. Unknown. Sucrose. Maltose. Maltodextrins 00 Infant Formula. Sucrose. Lactose Min. Column: Alltech Prevail Carbohydrate ES, µm, 0 x.mm (Part No. 0) Gradient: Time: 0 0 %B: Flow Rate:.0mL/min Min. Column: Alltech Prevail Carbohydrate ES, µm, 0 x.mm (Part No. 0) Gradient: Time: 0 0 %B: Flow Rate:.0mL/min Flavor Sample Solution Chromatogram courtesy of Charles Stewart, Firmenich Inc. 0 Spiked Urine Chromatogram courtesy of Rosemary Rose, Monash University, Dept. of Gastroenterology 0. Fructose. Glucose. Sucrose. Sucralose. Rhamnose. Cellobiose Min. Column: Alltech Prevail Carbohydrate ES, 0 x.mm (Part No. 0) Gradient: Time: 0 0 %B: 0 Flow Rate:.0mL/min 0 Min. Column: Alltech Prevail Carbohydrate ES, µm, 0 x.mm (Part No. 0) Mobile Phase: Acetonitrile:Water (0:0) Flow Rate:.0mL/min more applications View our complete searchable chromatogram database at ww.discoverysciences.com

4 Carbohydrates Robitussin Flu Syrup 0 Cough Syrup Min.. Sucralose. Fructose. Sorbitol. Glucose. Sucrose. Maltose Column: Alltech Prevail Carbohydrate ES, µm, 0 x.mm (Part No. 0) Gradient: Time: 0 0 %B: 0 Flow Rate:.0mL/min Min.. Fructose. Glucose. Sucrose. Maltose Column: Alltech Prevail Carbohydrate ES, µm, 0 x.mm (Part No. 0) Gradient: Time: 0 0 %B: Flow Rate:.0mL/min Tobacco. Fructose. Glucose. Sucrose. Unknown 0 Kellogg's Frosted Flakes Cereal Regular vs. / less sugar Min. Regular. Fructose 0. Glucose. Sucrose. Maltose. Oligosaccharides / Less Sugar 0 Column: Alltech Prevail Carbohydrate ES, µm, 0 x.mm (Part No. 0) Gradient: Time: 0 0 %B: Flow Rate:.0mL/min Column: Alltech Prevail Carbohydrate ES, µm, 0 x.mm (Part No. 0) Gradient: Time: 0 0 %B: Flow Rate:.0mL/min Rosenta Analysis Min. Column: Grom Sil 00 ODS- FE, µm, 0 x mm Mobile Phase: A: Water B: Acetonitrile Gradient: Time: 0 0 %B: 00 Flow Rate: 0.mL/min Detector: UV at nm

5 Organic Acids 0 0 Min. Column: Mobile Phase: Flow Rate: Detector: Organic Acid Mix. Oxalic Acid. Tartaric Acid. Formic Acid. Malic Acid. Lactic Acid. Acetic Acid. Diglycolic Acid. Maleic Acid. Citric Acid 0. Succinic Acid. Fumaric Acid Alltech Prevail Organic Acid, µm, 0 x.mm (Part No. 0) 0.0M KHPO, ph..ml/min UV at 0nm 0 0 Min. Column: Mobile Phase: Flow Rate: Detector: Rye Bread Extract. Tartaric Acid. Malic Acid. Lactic Acid. Citric Acid. Fumaric Acid Alltech Prevail Organic Acid, µm, 0 x.mm (Part No. 0) 0.0M KHPO, ph..0ml/min UV at 0nm Underivatized Fatty Acids. Lauric Acid. Myristic Acid. Palmitic Acid. Stearic Acid. Arachidic Acid. Behenic Acid Organic Acid Mix. Tartaric Acid. Malic Acid. Lactic Acid. Diglycolic Acid. Maleic Acid. Succinic Acid. Fumaric Acid Column: Alltech Prevail Organic Acid, µm, 0 x.mm (Part No. 0) Mobile Phase: Acetonitrile:Methanol (:) Flow Rate:.0mL/min Short-Chain Aromatic Carboxylic Acids 0 0. Oxalic Acid. Citric Acid. Shikimic Acid. Fumaric Acid. Butyric Acid. Homoprotocatechuic Acid. Gallic Acid. Protocatechuic Acid. Gentisic Acid 0. p-hydroxybenzoic Acid. Benzoic Acid. Salicylic Acid Min. Column: Alltech OA-000,.µm, 00 x.mm (Part No. 0) Mobile Phase: 0.0N Sulfuric Acid Column Temp: C Flow Rate: 0.mL/min Detector: UV at nm Column: Alltech Platinum EPS C, µm, 0 x.mm (Part No. 0) Mobile Phase: 0.0M KHPO, ph.:methanol (:) Flow Rate: 0.mL/min Detector: UV at 0nm 0 Fatty Acids Using UV and ELSD in Tandem. Caproic Acid. Caprylic Acid. Capric Acid. Lauric Acid. Linolenic Acid. Myristic Acid 0 UV 0 ELSD 0 Min.. Linoleic Acid. Palmitic Acid. Oleic Acid 0. Stearic Acid 00 Column: Alltech Alltima HP C HiLoad, µm, 0 x.mm (Part No. ) Mobile Phase: A: 0.% Trifluoroacetic Acid in Water B: 0.% Trifluoroacetic Acid in Acetonitrile Gradient: Time: %B: Flow Rate:.0mL/min more applications View our complete searchable chromatogram database at ww.discoverysciences.com

6 Organic Acids Organic Acids 00 Long Chain Fatty Acids 0 Min.. Tartaric Acid. Malic Acid. Lactic Acid.Maleic Acid. Fumaric Acid Column: GraceSmart C, µm, 0 x.mm (Part No. 0) Mobile Phase: 0.0M KHPO, ph.:methanol (:) Flow Rate: 0.mL/min Detector: UV at 0 0 Min.. Capric Acid. Lauric Acid. Myristic Acid. Palmitic Acid. Stearic Acid Column: Alltech Prevail C, µm, x mm Rocket (Part No. ) Mobile Phase: Acetonitrile:Methanol (:) Flow Rate:.mL/min Iso--Acids in Beer Oils / Lipids Olive Oil. Iso--Acid. Iso--Acid. Iso--Acid. Tetra-hydro iso--acid. Tetra-hydro iso--acid. Tetra-hydro iso--acid. Tetra-hydro iso--acid. LLO. LLP. OOL. POL. PPL. OOO. OOP. PPO. OOS Column: Jones Genesis C, µm, 0 x.mm + 0mm guard (Part No. FM0E + FH0-) Mobile Phase: Methanol: 0.% Phosphoric Acid, 0.mM EDTA (:) Flow Rate:.0mL/min Detector: UV at 0nm Olive Oil 0. LLO. OOLn. PLnO. LOO. PoOO. PLO. PoOP. OOO. POO+SOL 0. POP. SOO. POS+SLS. PPS. C Min. Column: Alltech Alltima C, µm, 0 x.mm (Part No. ) Mobile Phase: A: Dichloromethane B: Acetonitrile Gradient: Time: %B: Flow Rate:.mL/min Acid Whey. LACCER. PA. PE. PI. PS. PC. SM. SM Min. Column: Alltech Alltima HP C Hi-Load, µm, 0 x.0mm (Part No. 0) Gradient: Time: 0 %B: Flow Rate: 0.mL/min Min. Column: Alltech Prevail Silica, µm, 0 x.0mm (Part No. ) Mobile Phase: A: Chloroform; B: Methanol; C: Triethylamine buffer ph Gradient: Time: 0 %B: 0 %C: Flow Rate: 0.mL/min

7 Oils / Lipids Sesame Seed Oil Sesame Seed Oil Min. 0 Column: Alltech Alltima C, µm, 0 x.mm (Part No. ) Mobile Phase: A: Dichloromethane B: Acetonitrile Gradient: Time: %B: Flow Rate:.mL/min Min. Column: Alltech Alltima C, µm, 0 x.mm (Part No. 0) Gradient: Time: 0 0 %B: 0 0 Flow Rate:.0mL/min. LLL. LLO. LLP. OOL. POL. PPL. OOO. OOP. PPO 0. OOS Evening Primrose Oil Corn Oil. LGG. LGL. LLL. OGL. PGL. OLL. OGO + PLL. OOO. C. LLLn. LLL. LLO. PLL. LOO. PLO PLP. OOO 0. SLO. POO. POP. SOO/PPP C Min. 0 0 Min. 0. LLL. LLO. LLP. OOL. POL. PPL. OOO. OOP. PPO 0. OOS Column: Alltima HP C Hi-Load, µm, 0 x.mm (Part No. ) Gradient: Time: 0 %B: Flow Rate:.0mL/min Walnut Oil. Trilaurin (LaLaLa). Trilinolein (LLL).,-Dilinoleyl--oleyl-rac-glycerol (LLO).,-Dilinoleyl--palmitin-rac-glycerol (LLP). -Palmitin--olein--Linolein rac-glycerol (POL).,-Dipalmytyl--linolein-rac glycerol (PPL) Column: Alltech Alltima C, µm, 0 x.mm (Part No. ) Mobile Phase: A: Dichloromethane B: Acetonitrile Gradient: Time: %B: Flow Rate:.mL/min Lecithin, 0.mg/mL 0. PA. PE. PI. LPE. PC. LPC Min. Column: Alltech Alltima HP C Hi-Load, µm, 0 x.0mm (Part No. 0) Gradient: Time: 0 %B: Flow Rate: 0.mL/min 0 Column: 0 0 Min. Alltech Prevail Silica, µm, 0 x.0mm (Part No. ) Mobile Phase: A: Chloroform B: Methanol C: Triethylamine buffer ph Gradient: Time: 0 %B: 0 %C: Flow Rate: 0.mL/min more applications View our complete searchable chromatogram database at ww.discoverysciences.com

8 Oils / Lipids Palm Kernel Olein Fraction 0 Butter Min. Column: Alltech Alltima HP C Hi-Load, µm, 0 x.0mm (Part No. 0) Gradient: Time: 0 %B: Flow Rate: 0.mL/min Coconut Oil Min.. CCLa. C. CLaLa. CCM. LaLaLa. CLaM. LaLaM. LaLaO. LaMM. CCLa. C. CLaLa. CCM. LaLaLa. CLaM 0. LaMO. LaMP/MMM. MMO/LaPO. MMP/LaPP/MPO. PLP. POO. POP. C 0. LaLaM. LaLaO. LaMM 0. LaMO. LaMP/MMM. MMP/LaPP/MPO. C Column: Alltech Alltima HP C Hi-Load, µm, 0 x.0mm (Part No. 0) Gradient: Time: 0 %B: Flow Rate: 0.mL/min Sunflower Oil. LLL. LLO. PLL. LOO. LLS. PLO. OOO. SLO. POO Min. Column: Alltech Alltima HP C Hi-Load, µm, 0 x.0mm (Part No. 0) Gradient: Time: 0 %B: Flow Rate: 0.mL/min Cocoa Butter Min C. PLO. PLP. POO. PLS. POP. SOO/PPP. SLS. POS 0. PPS. SOS. PSS. SOA. C 0 Column: Alltech Alltima HP C Hi-Load, µm, 0 x.0mm (Part No. 0) Gradient: Time: 0 %B: Flow Rate: 0.mL/min Refined Sunflower Oil. C. LLL. LLO. PLL. LOO. LLS. PLO. OOO. SLO 0. POO. C Min. Column: Alltech Alltima HP C Hi-Load, µm, 0 x.0mm (Part No. 0) Gradient: Time: 0 %B: Flow Rate: 0.mL/min Min. Column: Alltech Alltima HP C Hi-Load, µm, 0 x.0mm (Part No. 0) Gradient: Time: 0 %B: Flow Rate: 0.mL/min

9 Oils / Lipids Palm Oil Min. Column: Alltech Alltima HP C Hi-Load, µm, 0 x.0mm (Part No. 0) Gradient: Time: 0 %B: Flow Rate: 0.mL/min Min. Column: Alltech Alltima HP C Hi-Load, µm, 0 x.0mm (Part No. 0) Gradient: Time: 0 %B: Flow Rate: 0.mL/min Polar Lipid Standards Soybean Oil. C. OLL. PLL. LOO. PLO. PLP. MOP. OOO. C. LLnLn. LLLn. LLL. OLnL. PLLn. LLO. OOLn. PLL 0. LOO. GLUCCER. LACCER. PE. PI. PS. PC. SM. SM 0. POO 0. PLS. POP. SOO/PPP. POS. PPS. SOS. C 00. LLS. PLO. PLP. OOO. SLO. POO. POP. SOO/PPP. C Min. Column: Alltech Prevail Silica, µm, 0 x.0mm (Part No. ) Mobile Phase: A: Chloroform B: Methanol C: Triethylamine buffer ph Gradient: Time: 0 %B: 0 %C: Flow Rate: 0.mL/min Min. Column: A Alltech lltima HP C Hi-Load, µm, 0 x.0mm (Part No. 0) Gradient: Time: 0 %B: Flow Rate: 0.mL/min Min. Column: Alltech Prevail Silica, µm, 0 x.0mm (Part No. ) Mobile Phase: A: Chloroform B: Methanol; C: Triethylamine buffer ph Gradient: Time: 0 %B: 0 %C: Flow Rate: 0.mL/min Palm Kernel Stearin Fraction Butter. CCLa. C. CLaLa. CMM. LaLaLa. LaLaM. LaLaO Gouda Cheese 0 0. LaMM. LaMO 0. LaMP/MMM. MMO/LaPO. MMP/LaPP/MPO. C. PE. PI. PS. PC. SM. SM. LACCER. U. PA. PE. PI. PS. PC. SM. SM 0. LPC Min. Column: Alltech Prevail Silica, µm, 0 x.0mm (Part No. ) Mobile Phase: A: Chloroform B: Methanol C: Triethylamine buffer ph Gradient: Time: 0 %B: 0 %C: Flow Rate: 0.mL/min more applications View our complete searchable chromatogram database at ww.discoverysciences.com

10 Oils / Lipids Limonene in Grapefruit Oil Additives Analysis of Food Preservatives. Limonene. p-hydroxybenzoic Acid. Methylhydroxybenzoic Acid. Propylhydroxybenzoic Acid Min. Column: Grom Sil 0 ODS- FE, µm, 0 x mm Mobile Phase: A: Water:Methanol (0:0) B: Acetonitrile Gradient: Time: 0 0 %B: 0 00 Flow Rate: 0.mL/min Detector: UV at nm Sweeteners in Beverages 0 Min. Column: Grom Sil 0 ODS- CP, µm, x mm (Part No. ) Mobile Phase: Water:Acetonitrile (0:0) Flow Rate:.mL/min Detector: UV at nm Aspartame in Soft Drinks. Sorbic Acid. Benzoic Acid. Saccharin. Benzoic Acid. Caffeine. Aspartame 0 Min. Column: Grom Sil 00 ODS- FE, µm, x mm Mobile Phase: mm Tetrabutylammonium Hydroxide, 0.M Sodium Phosphate, ph.:water:acetonitrile (:0:) Flow Rate: 0.mL/min Detector: UV at 0nm 0 0 Min. Column: Grom Sil 0 Phenyl- FE, µm, 0 x mm Mobile Phase: 0mM KHPO:Acetonitrile:Methanol (::) Flow Rate:.mL/min Detector: UV at nm Aflatoxins Aflatoxins 0 Aflatoxins. Aflatoxin B. Aflatoxin G. Aflatoxin B. Aflatoxin G. Ga. Ba. G. B 0 0 Min. Column: Alltech Alltima HP Silica, µm, 0 x.mm (Part No. ) Mobile Phase: Methylene Chloride:Methanol:Water (.:0.:0.) Flow Rate: 0.mL/min 0 Min. Column: Grom Sil 00 ODS-0 AB, µm, x mm Mobile Phase: Acetic Acid:Methanol:Water (::) Flow Rate: 0.mL/min Detector: Fluoresence at 0nm (exc.), nm (em.)

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