MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI

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1 MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI << MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI SRM1845 SRM1544 Whole egg powder Diet composite 3x8 g 4x15 g Certified Values* (g/kg, unless otherwise stated) Cholesterol 18,64 0,1483 FATTY ACIDS Caprylic acid (C8:0) (0,3) Capric acid (C10:0) (0,3) Lauric acid (C12:0) 1,31 Myristic acid (C14:0) 1,01 Palmitic acid (C16:0) 5,77 Palmitoleic acid (C16:1) (0,4) Stearic acid (18:0) 2,00 Oleic acid (C18:1) 11,64 Linoleic acid (C18:2) 6,56 Linolenic acid (C18:3) (0,6) Arachidic acid (C20:0) (0,1) Eicosenoic acid (C20:1) (0,1) Arachidonic acid (C20:4) (0,1) PROXIMATES Behenic acid (C22:0) (0,1) Protein (5,28)% Moisture (73,12)% Total fat (3,68)% Ash (0,97)% Carbohydrate (16,9)% Calories (1221) cal/kg ELEMENTS Calcium (0,52) Potassium (1,5) Sodium (1,7) * Values in brackets are noncertified values for reference (Proximates) or information (Fatty acids and elements). 351

2 >> MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI RM8415 Whole egg powder 35 g Constituent Reference Value* (mg/kg) FATTY ACIDS (as Triglycerides) Lauric acid (C12:0) (55) Myristic acid (C14:0) 1840 Myristoleic acid (C14:1) (480) Pentadecanoic acid (C15:0) 480 Palmitic acid (C16:0) Palmitoleic acid (C16:1) Margaric acid (C17:0) 1510 Stearic acid (C18:0) Oleic acid (C18:1) Elaidic acid (C18:1) (3300) Linoleic acid (C18:2) Linolenic acid (C18:3) (2700) γ-linolenic acid (C18:3) (290) Gadoleic acid (C20:1) (1400) γ-eicosadienoic acid (C20:2) 620 Arachidonic acid (C20:4) 4780 Docosapentaenoic acid (C22:5) (370) Docosahexaenoic acid (C22:6) 2570 VITAMINS Vitamin B 1 (2,8) Vitamin B 2 (12) Vitamin B 6 (3,7) Vitamin B 12 (0,068) Biotin (1,3) Folic acid (1,8) Inositol (860) Niacin (2,4) Pantothenic acid (91) PROXIMATES Moisture 3,53% Solids 96,47% Ash 4,78% Protein 37,8% Carbohydrate 7,5% Fat 46,4% Calories (598) k cal/100g 352

3 MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI << Constituent ELEMENTS RM8415 Whole egg powder 35 g Reference Value* (mg/kg) Aluminium 540 Antimony (0,002) Arsenic (0,01) Barium (3) Boron 0,41 Cadmium (0,005) Calcium 2480 Chlorine 5080 Chromium 0,37 Cobalt 0,012 Copper 2,70 Iodine 1,97 Iron 112 Lead 0,061 Magnesium 305 Manganese 1,78 Mercury 0,004 Molybdenum 0,247 Nitrogen Phosphorus Potassium 3190 Selenium 1,39 Sodium 3770 Strontium 5,63 Sulphur 5120 Vanadium 0,459 Zinc 67,5 * Reference values are noncertified values given for reference and provided with uncertainties that may not include all sources of uncertainty or may reflect a lack of sufficient statistical agreement among multiple methods. Values in brackets are only information values provided without uncertainty. 353

4 >> MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI ELEMENTS SRM1548a Typical diet 2x6,5 g Certified Value* (mg/kg, unless otherwise stated) Aluminium 72,4 Antimony (0,009) Arsenic 0,20 Barium (0,10) Boron (4,16) Bromine (9,64) Cadmium 0,035 Caesium 0,0098 Calcium 1967 Chlorine Cobalt (0,028) Copper 2,32 Iron 35,3 Iodine 0,759 Lead 0,044 Magnesium 580 Manganese 5,75 Mercury (0,005) Molybdenum (0,260) Nickel 0,369 Phosphorus 3486 Potassium 6970 Scandium (0,0008) Selenium 0,245 Silicon (78,7) Sodium 8132 Strontium (2,93) Sulphur 1928 Tin 17,2 Titanium (4,7) Zinc 24,6 PROXIMATES Ash (4,042)% Carbohydrate (58,36)% Fat (total) (19,41)% Nitrogen (3,03)% Protein (18,08)% Total dietary fiber (4,31)% Calories (481) kcal/100g * Values in brackets are noncertified values given for reference (B, Ba, Mo, Sr, Proximates) or for information (Sb, Br, Co, Hg, Si, Sc, Ti). 354

5 MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI << SRM2383 Baby food composite 4x70 g Certified Value* (mg/kg, unless otherwise stated) VITAMINS AND CAROTENOIDS Trans-Retinol 0,80 δ-tocopherol 1,51 γ- Tocopherol 5,51 α-tocopherol 25,0 α-tocopherol (free) (10,1) Lutein (includes esters) 1,16 Zexanthin (includes esters) 0,86 β-cryptoxanthin (includes esters) 1,38 Total α-carotene 0,83 Total β-carotene 3,12 Trans-α-Carotene (0,85) Trans-β-Carotene (2,40) 9-cis-β-Carotene (0,42) 13-cis-β-Carotene (0, cis-β-Carotene (0,158) cis-β-Carotene (0,321) Retinyl palmitate (1,45) Lutein (0,75) Zexanthin (0,46) β-cryptoxanthin (0,47) Trans-Lycopene (6,3) Total Lycopene (7,0) Trans-Vitamin K (0,132) cis-vitamin K (0,012) Total-Vitamin K (0,151) Vitamin B 1 (1,15) Vitamin B 2 (2,70) Vitamin B 6 (1,51) Vitamin B 12 (0,0044) Niacin (18,1) Pantothenic acid (3,7) Biotin (0,054) 355

6 >> MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI FATTY ACIDS (as Triglycerides) SRM2383 Baby food composite 4x70 g Certified Value* (mg/kg, unless otherwise stated) Capric acid (C10:0) (460) Lauric acid (C12:0) (3470) Myristic acid (C14:0) (1810) Pentadecanoic acid (C15:0) (42) Palmitic acid (C16:0) (10300) Palmitoleic acid (C16:1) (190) Stearic acid (18:0) (2060) Oleic acid (C18:1) (15200) Linoleic acid (C18:2) (7930) Linolenic acid (C18:3) (610) Behenic acid (C22:0) (100) PROXIMATES & CHOLESTEROL Solids (37,19)% Ash (1,09)% Fat (4,67)% Fat (sum of fatty acids) (4,35)% Saturated Fat (1,92)% Monounsaturated Fat (1,60)% Polyunsaturated Fat (0,86)% Protein (3,89)% Carbohydrates (27,49)% Total Dietary Fiber (0,96)% Cholesterol (22,6)% Calories (166,5)% ELEMENTS Calcium (853) Chloride (890) Copper (1,42) Iron (8,44) Magnesium (248) Manganese (1,39) Phosphorus (948) Potassium (3600) Sodium (390) Zinc (10,5) * Values in brackets are noncertified values given for reference and provided with uncertainties that may not include all sources of uncertainty or may reflect a lack of sufficient statistical agreement among multiple methods. Information values for 4 additional vitamins, 10 additional fatty acids, 3 additional elements and 4 sugar are also given in the cerrtificate of analysis. 356

7 MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI << SRM2384 Baking chocolate 5x91 g Certified Value* (g/100g, unless otherwise stated) FAT AND FATTY ACIDS Fat (extarctable) 51,4 Fat (sum of fatty acids) 50,3 Lauric acid (C12:0) (0,022) Myristic acid (C14:0) 0,080 Pentadecanoic acid (C15:0) (0,018) Palmitic acid (C16:0) 13,06 Palmitoleic acid (C16:1) 0,133 Margaric acid(c17:0) (0,115) Stearic acid (C18:0) 18,01 Oleic acid (C18:1) 16,44 Vaccenic acid (C18:1) 0,180 Linoleic acid (C18:2) 1,524 Linolenic acid (C18:3) 0,097 Arachidic acdi(c20:0) 0,521 Gadoleic acid (C20:1) (0,023) Behenic acid (C22:0) 0,091 Lignoceric acid (C24:0) 0,050 VITAMINS & ORGANIC ANALYTES δ-tocopherol (3,42) mg/kg γ-tocopherol (108,2) mg/kg α-tocopherol (7,2) mg/kg Vitamins B 2 (1,21) mg/kg Niacin (12,1) mg/kg Caffeine 0,1060 Theobromine 1,1600 Theophylline (0,0151) Total Procyanidins (1,0300) (+)-Catechin 0,0245 (-)-Epicatechin 0,1220 Catechin monomers 0,1490 PROXIMATES Solids (98,37) Ash (2,78) Protein (13,18) Carboydrate (by difference) (32,4) Total Dietary Fiber (14,5) Calories (631,0) kcal/100 g 357

8 >> MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI ELEMENTS Calcium Copper Iron Magnesium Manganese Phosphorus Potassium Sodium Zinc SRM2384 Baking chocolate 5x91 g Certified Value* (g/100g, unless otherwise stated) 840 mg/kg (23,2) mg/kg 132 mg/kg (2570) mg/kg (20,3) mg/kg (3330) mg/kg (8200) mg/kg (40) mg/kg (36,6) mg/kg * Values in brackets are noncertified values given for reference and provided with uncertainties that may not include all sources of uncertainty or may reflect a lack of sufficient statistical agreement among multiple methods. AGRICULTURAL RESEARCH CENTRE ARC/CL-2 Total diet 20 g Concentration (µg/g, unless otherwise stated) Cadmium 21 ng/g Calcium 2,86 mg/g Copper 3,18 Iron 30,4 Lead 43 ng/g Mercury 6,6 ng/g Magnesium 785 Manganese 12,9 Molybdenum 262 ng/g Potassium 9,42 mg/g Nickel 271 ng/g Selenium 181 ng/g Sodium 7,87 mg/g Zinc 28,9 Standard non inclusi nel catalogo sono disponibili su richiesta. Contattateci! 358

9 MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI << IRMM, EUROPEAN COMMISSION BCR-273 BCR-274 Single cell protein Single cell protein 10 g 10 g Concentrations* (mg/kg, unless otherwise stated) Arsenic 132 µg/kg Cadmium 30 µg/kg Calclum 11,97 g/kg Cobalt 39 µg/kg Copper 13,1 Fluorine (17,6) Iodine (21) µg/kg Iron 156 Lead 44 µg/kg Magnesium (2,7) g/kg Manganese 51,9 Nickel (0,3) Nitrogen (Kjeldahl) (121) g/kg Nitrogen 121,6 g/kg Phosphorus 26,8 g/kg Potassium 2,22 g/kg Selenium 1,03 Sodium (44) Sulphur (10,2) g/kg Zinc 42,7 * Values in brackets are not certified. BCR-302 Microcrystalline cellulose 1 Unit of lssue 20 g Nominal water Specified saturated Certified Value activity (a w at 25 C) salt aqueous solution (equilibrium water content, wt%) 0,1105 Lithium chloride 2,13 0,2245 Potassium acetate 3,24 0,3300 Magnesium chloride 4,15 0,4276 Potassium carbonate 5,16 0,5286 Magnesium nitrate 5,97 0,5770 Sodium bromide 6,48 0,7083 Strontium carbonate 8,25 0,7528 Sodium chloride 8,90 0,8426 Potassium chloride 11,00 0,9019 Barium chloride 13,27 1 The water content of the material when in equilibrium with the atmosphere above each saturated salt solution specified in the table was determined at 25 C by the method recommended by COST 90. The CRM is specifically intended to check the correct application of the COST procedure for determination of water sorption isotherms of foods. 359

10 >> MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI KEURINGSDIENST VAN WAREN KVW-PS260 KVW-PS277* KVW-PS247 Ice cream Chines food Curry soup 100 g 60 g 80 g Acesulfam-k Glutamic acid Saccarin Sodium p-toluensulfonamid 0,159 mg/kg Concentrations 1,11 g/100 g * At this moment the concentration of the certified component (Glutamic acid) of KVW-PS277 is not known, since this reference material is still in preparation. KVW-PS273 KVW-PS267 Salad souce Energy drink 100 g 120 g Concentrations Acesulfam Aspartam Benzoic acid Cafeine Sorbic acid Crude fat 1 At this moment the concetrations of the certified components (Sorbic acid, Benzoic acid, Crude Fat) of KVW-PS273 are not known, since this reference materials is still in preparation. 2 At this moment the concetrations of the certified components (Acesulfam, Aspartam, Benzoic acid, Cafeine, Sorbic acid) of KVW-PS267 are not known, since this reference material is still in preparation. KVW-PS257a KVW-PS257b Dietary lemonade Dietary lemonade 75 g 75 g Concentrations (g/100g) Fructose 3,4 3,5 Glucose 5,97 4,08 Saccharose 5,25 5,44 Sorbital 5,88 6,08 Xylitol 3,01 3,13 360

11 MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI << LGC PROMOCHEM LGC7016 Chocolate confectionery 15 g Mass fractions* (%) Fructose (0,2) Glucose (0,2) Lactose 7,8 Maltose Sucrose 44,8 Nitrogen 1,25 Total fat 29,5 Butyric acid in fat 0,8 * Values in brackets are not certified. LGC7130 LGC7131 LGC7140 Soft drink Soft drink Soft drink Unit of lssue 5x20 ml 5x20 ml 5x60 ml Concentrations (mg/l) Aspartame Acessulphame-k Saccharin Poncean 4R (E124) 18,7 Sunset yellow (E110) 19,6 Tartrazine (E102) 29,9 2 Permissible levels of sweeteners in foodstuffs are regulated by European legislation (EU Directive 94/35/EC). LGC7176 Canned pet food 200 g Certified constituent Mass fractions* (%) Moisture 84,1 Ash 2,20 Fat 4,46 Chloride (1200) Nitrogen 1,32 Potassium (3340) Sodium (1800) * Values in brackets are not certified. 361

12 >> MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI LGC PROMOCHEM LGC7105 LGC7107 Rice pudding Madeira cake* 5x200 g 160 g Assessed values (mg/kg, unless otherwise stated) Ash 0,22% 1,76% Moisture 71,3% 25,9% Nitrogen 0,17% 0,66% Total fat 8,4% 13,4% Lactose 0,9% Sucrose 7,2% 28,1% Calcium 78 Magnesium 30 Manganese 0,7 Phosphorus 346 Potassium 558 Sodium 344 Zinc 1,5 * Indicative value of starch is also given in the certificate of this RM. (Food additive) Certified Property Value 2,6-Di-t-butyl-4-methylphenol (BHT) Purity 99,8% 0,5 g LGC t-Butyl-4-hydroxyanisole (BHA) Purity 99,2% 0,5 g LGC7301 Saccharin Purity 99,6% 0,5 g LGC7302 Potassium Sorbate Purity 99,8% 0,5 g LGC LGC7172 LGC7173 Dairy cattle feed Poultry feed 5x50 g 5x50 g Certified values (mg/kg, unless otherwise stated) Ash 8,1 % 7,5 % Crude fibre 7,5 % 5,0 % Moisture 5,8 % 8,3 % Nitrogen 2,72 % 2,72 % Oil 7,8 % 3,8 % Starch 41,4 % Calcium 1,05 % 1,90 % Chlorine 0,66 % 0,25 % Copper Iron Magnesium 0,60 % 0,18 % Manganese Phosphorus 0,72 % 0,68 % Potassium 1,07 % 0,74 % Sodium 0,15 % Zinc

13 MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI << NATIONAL FOOD ADMIRATION SLV-Diet A SLV-Diet B SLV-Diet C Simulated Simulated Simulated diet A diet B diet C 10 g 10 g 10 g Certified constituent Certified Value (mg/kg) Aluminium (0,74) (1,13) (1,43) Arsenic (<0,050) (<0,050) (<0,050) Cadmium 0,029 0,099 0,205 Calcium Chromium (0,174) 0,149 0,054 Cobalt (0,021) (0,035) (0,038) Copper 2,60 6,64 20,8 Iron 81, Lead 0,041 0,059 0,114 Magnesium Manganese 5,69 6,36 9,58 Mercury (0,00087) (0,0043) (0,015) Nickel (0,126) (0,093) 0,108 Potassium Rubidium (8,85) (10,5) (8,5) Selenium (0,050) (1,52) (0,119) Sodium Zinc 95,0 91,9 40,6 SLV-Diet D SLV-Diet E SLV-Diet F Simulated Simulated Simulated diet D diet E diet F 10 g 10 g 10 g Certified constituent Certified Value (mg/kg) Aluminium (1,25) (2,49) (3,13) Arsenic (<0,050) (<0,050) (<0,050) Cadmium 0,478 0,536 0,877 Calcium Chromium 0,036 0,061 (0,054) Cobalt 0,072 0,083 0,136 Copper 40,8 46,5 72,7 Iron Lead 0,218 0,273 0,439 Magnesium Manganese 10,2 11,0 11,1 Mercury (0,052) (0,040) (0,071) Nickel 0,0100 0,124 0,102 Potassium Rubidium (11,6) (12,2) (19,7) Selenium (0,214) (0,232) (0,391) Sodium Zinc 37,2 39,5 55,8 363

14 >> MISCELLANEA DI STANDARD IN MATRICI ALIMENTARI NRCCRM GBW10001 GBW10002 GBW10003 GBW10004 GBW10005 Synthetic Dystuffs for Food Additives Amaranth Ponceau 4R Tartrazine Brillant Blue Sunset Yellow 0,3 g 0,3 g 0,3 g 0,3 g 0,3 g Certified Purity (%) 97,2 93,3 99,3 97,3 97,3 GBW10006 GBW10007 GBW10008 GBW10009 Refined salt Refined salt Refined salt Refined salt 50 g 50 g 50 g 50 g Concentrations (mg/kg) Iodine

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